METHOD FOR PREPARING HETEROATOM-DOPED CNHS
    1.
    发明公开

    公开(公告)号:US20230286805A1

    公开(公告)日:2023-09-14

    申请号:US18304316

    申请日:2023-04-20

    CPC classification number: C01B32/18 B01J21/18 B01J23/42 B01J35/0013 B01J37/08

    Abstract: A method includes the following steps: a first step: the material containing heteroatom and graphite powder are mixed for a preset time by grinding, and the molar ratio of heteroatom to carbon atom is 1%-10%, then the heteroatom precursors are obtained; a second contact step: the heteroatom precursor is filled into a graphite rod with holes and compacted, then the graphite rod is dried for a preset time to obtain a plasma anode and using a DC arc plasma device to prepare the graphite anode into heteroatom-doped CNHs; a third contact step: the heteroatom-doped CNHs are dispersed in a reducing solution, a platinum salt is added to stir evenly, the reduction reaction is carried out by heating and stirring, and after centrifugation, washing and drying, a catalyst with platinum loading is obtained.

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