公开(公告)号：US10195590B2

公开(公告)日：2019-02-05

申请号：US14413136

申请日：2013-07-05

申请人： Teknologisk Institut

发明人： Christian Kallesøe ,  Henrik Fanø Clausen ,  Leif Højslet Christensen ,  Torsten Lund-Olesen ,  Mohammad Aref Hasen Mamakhel ,  Bo Brummerstedt Iversen ,  Jacob Becker-Christensen ,  David Friis Aarup ,  Jan Hales

IPC分类号： H01M4/92 ,  B01J21/18 ,  B01J23/42 ,  B01J23/46 ,  B01J37/00 ,  B01J37/04 ,  B01J37/34 ,  B01J35/00 ,  B01J35/02 ,  B01J35/10 ,  H01M8/1018

摘要： A method of preparing a catalytic structure the method including the steps of: providing a solution of a precursor compound in a solvent at ambient conditions; providing a suspension of a support material having a specific surface area of at least 1 m2/g in a solvent at ambient conditions; mixing the solution of the precursor compound and the suspension of the support material; providing a reactive solvent in a supercritical or subcritical state; admixing the mixture of the solution of the precursor compound and the suspension of the support material in the supercritical or subcritical reactive solvent to form a reaction solution; injecting the reaction solution into a reactor tube via an inlet; allowing a reaction of the precursor compound in the supercritical or subcritical reactive solvent in the reactor tube to form the catalyst nanoparticles on the support material to provide the catalytic structure.

公开(公告)号：US20150202598A1

公开(公告)日：2015-07-23

申请号：US14413136

申请日：2013-07-05

申请人： Teknologisk Institut

发明人： Christian Kallesøe ,  Henrik Fano Clausen ,  Leif Hojslet Christensen ,  Torsten Lund-Olesen ,  Mohammed Aref Hasen Mamakhe ,  Bo Brummerstedt Iversen ,  Jacob Becker-Christensen ,  David Friss Aarup ,  Jan Hales

IPC分类号： B01J23/46 ,  B01J37/00 ,  B01J35/00 ,  H01M4/92 ,  B01J23/42 ,  B01J21/18 ,  B01J35/02 ,  B01J37/34 ,  B01J37/04 ,  B01J35/10

CPC分类号： B01J23/462 ,  B01J21/18 ,  B01J21/185 ,  B01J23/42 ,  B01J35/0013 ,  B01J35/026 ,  B01J35/1009 ,  B01J37/0072 ,  B01J37/04 ,  B01J37/343 ,  H01M4/926 ,  H01M2008/1095

摘要： A method of preparing a catalytic structure the method including the steps of: providing a solution of a precursor compound in a solvent at ambient conditions; providing a suspension of a support material having a specific surface area of at least 1 m2/g in a solvent at ambient conditions; mixing the solution of the precursor compound and the suspension of the support material; providing a reactive solvent in a supercritical or subcritical state; admixing the mixture of the solution of the precursor compound and the suspension of the support material in the supercritical or subcritical reactive solvent to form a reaction solution; injecting the reaction solution into a reactor tube via an inlet; allowing a reaction of the precursor compound in the supercritical or subcritical reactive solvent in the reactor tube to form the catalyst nanoparticles on the support material to provide the catalytic structure.

摘要翻译： 一种制备催化结构的方法，该方法包括以下步骤：在环境条件下提供前体化合物在溶剂中的溶液; 在环境条件下在溶剂中提供具有至少1m 2 / g比表面积的载体材料的悬浮液; 混合前体化合物的溶液和载体材料的悬浮液; 提供超临界或亚临界状态的反应性溶剂; 将前体化合物的溶液和载体材料的悬浮液的混合物混合在超临界或亚临界反应性溶剂中以形成反应溶液; 通过入口将反应溶液注入反应器管中; 允许前体化合物在反应器管中的超临界或亚临界反应性溶剂中反应以在载体材料上形成催化剂纳米颗粒以提供催化结构。