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公开(公告)号：US5851505A
公开(公告)日：1998-12-22
申请号：US935204
申请日：1997-09-22
IPC分类号： B01J20/26 , C01B15/013 , C01B15/01
CPC分类号： C01B15/013
摘要： A purified aqueous solution of hydrogen peroxide is produced by contacting an aqueous solution of hydrogen peroxide containing organic impurities with a hydrophilic porous resin (the product under a tradename "WOFATIT EP63", etc.) having a specific surface area of not less than 800 m.sup.2 /g to remove the organic impurities in the aqueous solution of hydrogen peroxide.
摘要翻译： 通过使含有有机杂质的过氧化氢水溶液与比表面积不小于800m 2的亲水性多孔树脂（商品名“WOFATIT EP63”等的产品等））接触，得到纯化的过氧化氢水溶液 以除去过氧化氢水溶液中的有机杂质。
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公开(公告)号：US5942202A
公开(公告)日：1999-08-24
申请号：US094484
申请日：1998-06-10
申请人： Yoshio Nishimura , Yoshitsugu Minamikawa , Jun Kokubu , Chiharu Nishizawa , Satoshi Okabe , Naoko Matsuya
发明人： Yoshio Nishimura , Yoshitsugu Minamikawa , Jun Kokubu , Chiharu Nishizawa , Satoshi Okabe , Naoko Matsuya
IPC分类号： C01B15/037
CPC分类号： C01B15/037
摘要： A stabilized aqueous solution of hydrogen peroxide comprising at least one metal element selected from the group consisting of tantalum, zirconium, and niobium.The aqueous solution of hydrogen peroxide has excellent storage stability and heat stability.
摘要翻译： 稳定的过氧化氢水溶液，其包含选自钽，锆和铌中的至少一种金属元素。 过氧化氢水溶液具有优异的储存稳定性和热稳定性。
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3.发明授权
公开(公告)号：US5456898A
公开(公告)日：1995-10-10
申请号：US303834
申请日：1994-09-09
IPC分类号： C01B15/013 , C01B15/01
CPC分类号： C01B15/013 , C01B15/0135
摘要： Proposed is an improvement in a method for the preparation of an enriched and purified aqueous hydrogen peroxide solution from a crude aqueous hydrogen peroxide solution comprising the steps of evaporating the crude aqueous hydrogen peroxide solution in an evaporator into vapor with accompanying liquid in the form of a mist, separating the vapor from the mist of liquid in a gas-liquid separator and subjecting the vapor to fractionating distillation in a fractionating distillation column in order to greatly upgrade the product solution relative to the impurity content. The improvement is achieved by subjecting the crude aqueous hydrogen peroxide solution, prior to introduction into the evaporator, to a contacting treatment with a porous synthetic adsorbent resin to remove organic impurities from the crude aqueous hydrogen peroxide solution to such an extent that the crude aqueous hydrogen peroxide solution after the contacting treatment contains organic impurities in an amount not exceeding 50 ppm by weight calculated as organic carbon. Although the mechanism is not well understood, the preliminary removal of organic impurities from the crude aqueous hydrogen peroxide solution has an effect of greatly increasing the efficiency of gas-liquid separation of the vapor accompanied by a mist of liquid in the gas-liquid separator to decrease the amount of contaminant impurities introduced into the distillation column as carried by the mist.
摘要翻译： 提出了从粗制过氧化氢水溶液制备富集和纯化的过氧化氢水溶液的方法的改进，包括以下步骤：将蒸发器中的粗过氧化氢水溶液蒸发成蒸汽，伴随液体为 在气 - 液分离器中分离蒸气与液雾的蒸气，并在分馏蒸馏塔中对蒸汽进行分馏，以相对于杂质含量大大提升产物溶液。 改进之处在于，将粗水过氧化氢溶液在引入蒸发器之前，与多孔合成吸附剂树脂进行接触处理以从粗过氧化氢水溶液中除去有机杂质，使得粗制氢水 接触处理后的过氧化物溶液含有不超过作为有机碳计算的50重量ppm的有机杂质。 虽然机理尚不清楚，但是从粗过氧化氢水溶液中初步除去有机杂质具有大大提高伴随气液分离器中的液体雾气的气液分离效率， 减少由雾气引入到蒸馏塔中的污染物杂质的量。
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公开(公告)号：US08039022B2
公开(公告)日：2011-10-18
申请号：US11914802
申请日：2006-05-16
IPC分类号： A01N59/00
CPC分类号： C01B15/037 , A01N59/00 , A61L2/208 , A61L2202/18 , A61L2202/23 , B65B55/10 , A01N59/26 , A01N25/22 , A01N2300/00
摘要： The present invention provides a hydrogen peroxide solution for sterilization which has a hydrogen peroxide concentration of 30 to 45% by weight, an Fe concentration of 2 ppb or less and an Al concentration of at least 15 ppb and in which a concentration of a stabilizer comprising orthophosphoric acid is 40 ppm at the most. The above hydrogen peroxide solution for sterilization is used for sterilizing vessels filled with beverages and foods and packaging materials in an aseptic filling equipment. The above hydrogen peroxide solution for sterilization has less evaporation residue, does not clog a narrow piping part such as a spray nozzle and therefore makes it possible to stably operate an aseptic filling equipment. Further, an austenite base stainless material can be used as a material for the transporting facilities and the tanks.
摘要翻译： 本发明提供过氧化氢浓度为30〜45重量％，Fe浓度为2ppb以下，Al浓度为15ppb以上的绝育用过氧化氢溶液，其中，稳定剂浓度为 正磷酸最多为40ppm。 上述用于灭菌的过氧化氢溶液用于在无菌灌装设备中对装有饮料，食品和包装材料的容器进行灭菌。 上述用于灭菌的过氧化氢溶液具有较少的蒸发残留，不会堵塞诸如喷嘴之类的狭窄管道部分，因此能够稳定地操作无菌填充设备。 此外，可以使用奥氏体基础不锈钢材料作为输送设备和罐的材料。
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公开(公告)号：US20090175760A1
公开(公告)日：2009-07-09
申请号：US11914802
申请日：2006-05-16
CPC分类号： C01B15/037 , A01N59/00 , A61L2/208 , A61L2202/18 , A61L2202/23 , B65B55/10 , A01N59/26 , A01N25/22 , A01N2300/00
摘要： The present invention provides a hydrogen peroxide solution for sterilization which has a hydrogen peroxide concentration of 30 to 45% by weight, an Fe concentration of 2 ppb or less and an Al concentration of at least 15 ppb and in which a concentration of a stabilizer comprising orthophosphoric acid is 40 ppm at the most. The above hydrogen peroxide solution for sterilization is used for sterilizing vessels filled with beverages and foods and packaging materials in an aseptic filling equipment. The above hydrogen peroxide solution for sterilization has less evaporation residue, does not clog a narrow piping part such as a spray nozzle and therefore makes it possible to stably operate an aseptic filling equipment. Further, an austenite base stainless material can be used as a material for the transporting facilities and the tanks.
摘要翻译： 本发明提供过氧化氢浓度为30〜45重量％，Fe浓度为2ppb以下，Al浓度为15ppb以上的绝育用过氧化氢溶液，其中，稳定剂浓度为 正磷酸最多为40ppm。 上述用于灭菌的过氧化氢溶液用于在无菌灌装设备中对装有饮料，食品和包装材料的容器进行灭菌。 上述用于灭菌的过氧化氢溶液具有较少的蒸发残留，不会堵塞诸如喷嘴之类的狭窄管道部分，因此能够稳定地操作无菌填充设备。 此外，可以使用奥氏体基础不锈钢材料作为输送设备和罐的材料。
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公开(公告)号：US5733521A
公开(公告)日：1998-03-31
申请号：US733799
申请日：1996-10-18
IPC分类号： B01J41/04 , B01J41/12 , C01B15/013 , C01B15/023 , C01B15/01
CPC分类号： B01J41/04 , C01B15/0135
摘要： A process for producing a purified aqueous hydrogen peroxide solution comprising bringing an aqueous hydrogen peroxide solution containing impurities into contact with an anion exchange resin in the fluoride form is disclosed. According to the process, impurities in the aqueous hydrogen peroxide solution, particularly impurities containing silicon, such as silicates and silicic acid, can efficiently be removed, and a purified aqueous hydrogen peroxide solution having a high purity can be obtained.
摘要翻译： 公开了一种纯化的过氧化氢水溶液的制造方法，其包括使含有杂质的过氧化氢水溶液与氟化物形式的阴离子交换树脂接触。 根据该方法，可以有效地除去过氧化氢水溶液中的杂质，特别是含有硅的杂质，例如硅酸盐和硅酸，并且可以获得纯度高的纯化的过氧化氢水溶液。
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