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公开(公告)号：US5250396A
公开(公告)日：1993-10-05
申请号：US954411
申请日：1992-09-30
CPC分类号： G03C7/44
摘要： A method of continuously processing an imagewise exposed silver halide photographic material using an automatic processor which has a color development bath, comprising the steps of a) developing with a color developer containing an organic preservative, and b) adding to the color developer during the continuous processing (i) a replenisher for the color developer containing a development agent and other components for the development in an amount of from 20 ml to 600 ml per m.sup.2 of the photographic material processed, and (ii) a water solution in an amount of from 0.1 to 1.2 times the amount of the developer which has evaporated from the bath at a frequency of about once per week or more often.
摘要翻译： 使用具有显色浴的自动处理器连续处理成像曝光的卤化银照相材料的方法，包括以下步骤：a）用含有机防腐剂的彩色显影剂显影，和b）在连续的期间向彩色显影剂添加 处理（i）含有显影剂的显影剂和其它用于显影的成分的补充剂，其量为每毫升加工的照相材料为20ml至600ml，和（ii）水溶液的量为 以每周约一次或更频繁地从浴中蒸发的显影剂的量的0.1至1.2倍。
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102.发明授权Silicon substrate having porous oxidized silicon layers and its production method 失效具有多孔氧化硅层的硅衬底及其生产方法
公开(公告)号：US5156896A
公开(公告)日：1992-10-20
申请号：US556777
申请日：1990-07-24
申请人： Masakazu Katoh , Takatoshi Ishikawa
发明人： Masakazu Katoh , Takatoshi Ishikawa
IPC分类号： B41J2/335 , C25D11/32 , H01L21/762
CPC分类号： B41J2/33525 , B41J2/3357 , B41J2/3359 , C25D11/32 , H01L21/76245 , Y10S438/96 , Y10T428/24777 , Y10T428/24802 , Y10T428/249987 , Y10T428/249988 , Y10T428/31681
摘要： In the silicon substrate having porous oxidized silicon layers of this invention, which consists of a silicon substrate the one surface of which is dotted with porous oxidized silicon dots, the residual internal stress (compression stress) is dispersedly distributed in the porous oxidized silicon dots. Therefore, the entire silicon substrate having porous oxidized silicon dots of this invention is only minimally warped.Adopting a method for producing the silicon substrate of this invention which consists of covering with a mask the surface of a silicon substrate except its dotting areas to be treated, subjecting the silicon substrate to anodic formation in an aqueous hydrofluoric acid solution to form porous silicon layers in the areas to be treated and not covered with the mask and then oxidizing the formed porous silicon layers enables secured production of a silicon substrate provided with a plurality of polygonal shaped dots of porous oxidized silicon.
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公开(公告)号：US5153108A
公开(公告)日：1992-10-06
申请号：US789541
申请日：1991-11-08
CPC分类号： G03C7/3003 , G03C7/413
摘要： A method for processing a silver halide color photographic material comprising at least one silver halide emulsion layer, which comprises developing the silver halide color photographic material with a color developer containing at least one aromatic primary amine color developing agent, wherein the photographic material contains (a) at least one high silver chloride content emulsion layer with a silver chloride content of 80 mol % or more, and (b) a compound of formula (I): ##STR1## wherein R.sub.1 and R.sub.2 each represents --COOR.sub.5, ##STR2## --COR.sub.5 --CN or a halogenated methane R.sub.3 and R.sub.4 each represents a hydrogen atom or an unsubstituted or substituted alkyl group; R.sub.5 and R.sub.6 each represents a hydrogen atom, an unsubstituted or substituted alkyl group or an unsubstituted or substituted aryl group; Q.sub.1 and Q.sub.2 each represents an aryl group; X.sub.1 and X.sub.2 each represents a chemical bond or a divalent linking group; Y.sub.1 and Y.sub.2 each represents a sulfo group or a carboxy group; L.sub.1, L.sub.2 and L.sub.3 each represents a methine group; m.sub.1 and m.sub.2 each represents 0, 1, or 2; n represents 0, 1 or 2; p.sub.1 and p.sub.2 each represents 0, 1, 2, 3 or 4; s.sub.1 and s.sub.2 each represents 1 or 2; and t.sub.1 and t.sub.2 each represents 0 or 1; provided that the total of m.sub.1, p.sub.1 and t.sub.1 and the total of m.sub.2, p.sub.2 and t.sub.2 must not be 0 at the same time;and the color developer contains a chloride ion in an amount of from 3.5.times.10.sup.-2 to 1.5.times.10.sup.-1 mol/liter and bromide ion in an amount of from 3.0.times.10.sup.-5 to 1.0.times.10.sup.-3 mol/liter.
摘要翻译： 一种用于处理卤化银彩色照相材料的方法，其包括至少一种卤化银乳剂层，其包括用含有至少一种芳族伯胺彩色显影剂的显色剂显影所述卤化银彩色照相材料，其中所述照相材料含有 ）至少一种氯化银含量为80摩尔％以上的高氯化银含量乳剂层，（b）式（I）化合物：其中R1和R2各自表示-COOR5， 图示-COR 5 -CN或卤代甲烷R3和R4各自表示氢原子或未取代或取代的烷基; R5和R6各自表示氢原子，未取代或取代的烷基或未取代或取代的芳基; Q1和Q2各自表示芳基; X1和X2各自表示化学键或二价连接基团; Y1和Y2各自表示磺基或羧基; L1，L2和L3各自表示次甲基; m1和m2各自表示0,1或2; n表示0,1或2; p1和p2各自表示0,1,2,3或4; s1和s2各自表示1或2; t1和t2各自表示0或1; 条件是m1，p1和t1以及m2，p2和t2的总和不得同时为0; 并且显色剂含有3.5×10 -2至1.5×10 -1 mol /升的氯离子和3.0×10 -5至1.0×10 -3 mol /升的溴离子。
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公开(公告)号：US5139929A
公开(公告)日：1992-08-18
申请号：US555016
申请日：1990-07-20
申请人： Takatoshi Ishikawa , Shinji Ueda
发明人： Takatoshi Ishikawa , Shinji Ueda
CPC分类号： G03C7/44
摘要： A method for processing an exposed silver halide color photographic material comprising the steps of:(a) color developing an exposed silver halide color photographic material;(b) bleach-fixing said developed material;(c) at least one of washing said bleach-fixed material with water and stabilizing said bleach-fixed material;(d) regenerating a portion of a solution from said step (b) for bleach-fixing to form a replenisher solution comprising at least a carbonyl bisulfite adduct; and(e) replenishing at least one solution in said bleach-fixing step (b) with said replenisher solution from step (d).
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公开(公告)号：US5066571A
公开(公告)日：1991-11-19
申请号：US416690
申请日：1989-10-03
CPC分类号： G03C7/413
摘要： A method for processing a silver halide color photosensitive material is disclosed.The method comprises developing a color photographic light-sensitive material composed of a support having thereon at least one light-sensitive silver halide emulsion layer containing a silver halide comprising at least 98 mol % silver chloride;in a color developer solution comprising a primary amine color developing agent, and having a chloride ion concentration of from 4.times.10.sup.-2 to 1.times.10.sup.-1 mol/l, and a bromide ion concentration of from 5.times.10.sup.-5 to 5.times.10.sup.-4 mol/l.When used in rapid processing methods, the method according to the invention prevents fogging streaks, and provides high maximum density and low minimum density images.
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公开(公告)号：US5043254A
公开(公告)日：1991-08-27
申请号：US440865
申请日：1989-11-24
CPC分类号： G03C7/413 , G03C7/3005 , G03C7/39224
摘要： A method for forming an image comprises processing a silver halide color photosensitive material comprising a nondiffusible coupler and a nondiffusible color developing agent on a support with a color developer containing a diffusible color developing agent comprising an aromatic primary amine. By this method, it is possible to reduce the processing time required when a color developer containing an ordinary aromatic primary amine as the color developing agent is used and also to provide a stable image forming method having only a slight processing dependence.
摘要翻译： 一种用于形成图像的方法包括在含有包含芳族伯胺的可扩散彩色显影剂的彩色显影剂的载体上处理包含非扩散性成色剂和非扩散性着色剂的卤化银色感光材料。 通过该方法，可以减少使用含有作为彩色显影剂的普通芳族伯胺的彩色显影剂所需的处理时间，并且还提供仅具有轻微加工依赖性的稳定的图像形成方法。
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公开(公告)号：US5002860A
公开(公告)日：1991-03-26
申请号：US313279
申请日：1989-02-21
CPC分类号： G03C7/42 , G03C7/3835
摘要： A novel process for processing a silver halide color photographic material is disclosed, which comprises color-developing a silver halide color photographic material which has been imagewise exposed to light, and then processing the silver halide color photographic material with a processing solution having a bleaching ability, wherein the silver halide color photographic material comprises at least one magenta coupler represented by formula (M-1) and the processing solution having a bleaching ability comprises as a bleaching agent (1) at least one of ferric complex salts of compounds selected from Compound Group (A) and (2) a ferric 1,3-diaminopropanetetraacetate complex salt in a molar proportion of the (1) to the (2) of 3 or less:Compound Group (A)A-1: Ethylenediaminetetraacetic acidA-2: Diethylenetriaminepentaacetic acidA-3: Cyclohexanediaminetetraacetic acidA-4: 1,2-Propylenediaminetetraacetic acid ##STR1## wherein Za and Zb each represents --CH.dbd., ##STR2## or .dbd.N--; R.sub.1 and R.sub.2 each represents a hydrogen atom or a substituent; and X represents a hydrogen atom or a group which is released upon a coupling reaction with an oxidation product of an aromatic primary amine developing agent, with the proviso that when Za.dbd.Zb is a carbon-carbon double bond, it is a portion of an aromatic ring.
摘要翻译： 公开了一种用于处理卤化银彩色照相材料的新方法，其包括对成像曝光的卤化银彩色照相材料进行彩色显影，然后用具有漂白能力的处理溶液处理卤化银彩色照相材料 ，其中所述卤化银彩色照相材料包含至少一种由式（M-1）表示的品红成色剂，并且具有漂白能力的处理溶液包含漂白剂（1）至少一种选自化合物 组分（A）和（2）以（1）〜（2）为3以下的摩尔比例的1,3-二氨基丙烷四乙酸铁配合物盐：化合物组（A）A-1：乙二胺四乙酸A-2 ：二亚乙基三胺五乙酸A-3：环己烷二胺四乙酸A-4：1,2-丙二胺四乙酸（M-1）其中Za和Zb各自表示-CH =，IMAGE或= N-; R1和R2各自表示氢原子或取代基; X表示氢原子或与芳族伯胺显影剂的氧化物进行偶联反应而释放的基团，条件是当Za = Zb为碳 - 碳双键时，其为 芳香环。
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108.发明授权
公开(公告)号：US4985347A
公开(公告)日：1991-01-15
申请号：US560493
申请日：1990-07-25
摘要： A method for processing silver halide color photographic material is disclosed which comprises processing a silver halide color photographic material with a color developer containing substantially no sulfite ion and then processing the color photographic material with a solution having bleaching capability containing an aminopolycarboxylic acid having a molecular weight of at least 300.
摘要翻译： 公开了一种用于处理卤化银彩色照相材料的方法，其包括用基本上不含亚硫酸根离子的显影剂处理卤化银彩色照相材料，然后用具有漂白能力的溶液处理彩色照相材料，该溶液含有具有分子量的氨基多羧酸 至少300。
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公开(公告)号：US4968591A
公开(公告)日：1990-11-06
申请号：US919538
申请日：1986-10-16
CPC分类号： G03C7/42 , G03C7/3046
摘要： A process for processing a silver halide color photographic material is described comprising subjecting a silver halide color photographic material comprising a support having provided thereon at least one photographic emulsion layer containing at least one kind of pyrazoloazole series magenta coupler represented by general formula (I) to photographic processing using a bath containing at least 1.times.10.sup.-4 mol/liter of a soluble iron salt as the final bath: ##STR1## wherein Za and Zb each represents .dbd.CH--, (wherein R.sub.2 represents a hydrogen atom or a substituent) or =N-; R.sub.1 represents a hydrogen atom or a substituent; X represents a hydrogen atom or a group releasably upon coupling with the oxidation product of an aromatic primary amine developing agent; when Za=Zb is a carbon-carbon double bond, the double bond may be a part of an aromatic ring; the magenta coupler may form a dimer or polymer at R.sub.1, R.sub.2 or X; when at least one of said Za and Zb is ##STR2## at least one of the R.sub.1 and R.sub.2 represents a methylene group directly bonded to the skeleton of general formula (I), at least one of the hydrogen atoms of which is substituted; when both Za and Zb are .dbd.N--, R.sub.1 is a methylene group directly bonded to the skeleton, at least one of the hydrogen atoms of which is substituted; and the R.sub.1 or R.sub.2 has at least one --NHSO.sub.2 -- as a substituent.
摘要翻译： 描述了一种用于处理卤化银彩色照相材料的方法，其包括将包含其上提供的支持体的卤化银彩色照相材料经受至少一种含有通式（I）表示的至少一种吡唑并唑系品红成色剂的照相乳剂层至 使用含有至少1×10 -4 mol /升可溶性铁盐作为最终浴的浴的照相处理：其中Za和Zb各自表示= CH-，其中R2表示氢原子 或取代基）或= N-; R1表示氢原子或取代基; X表示与芳族伯胺显影剂的氧化产物偶联时可释放的氢原子或基团; 当Za = Zb是碳 - 碳双键时，双键可以是芳环的一部分; 品红成色剂可以在R1，R2或X形成二聚体或聚合物; 当所述Za和Zb中的至少一个为“IMA”时，R 1和R 2中的至少一个表示直接键合到通式（I）的骨架上的亚甲基，其中至少一个氢原子被取代; 当Za和Zb均为= N-时，R1是与骨架直接键合的亚甲基，其中至少一个氢原子被取代; 并且R 1或R 2具有至少一个-NHSO 2 - 作为取代基。
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公开(公告)号：US4968588A
公开(公告)日：1990-11-06
申请号：US404480
申请日：1989-09-08
申请人： Takatoshi Ishikawa , Morio Yagihara
发明人： Takatoshi Ishikawa , Morio Yagihara
IPC分类号： G03C7/413
CPC分类号： G03C7/413
摘要： A method for processing a silver halide color photographic material is described, which comprises processing a silver halide color photographic material comprising a reflective support having thereon at least one silver halide emulsion layer for a period of 2 minutes and 30 seconds or less with a color devleoping solution which does not substantially contain benzyl alcohol and which contains at least one of compounds selected from the group consisting of a compound represented by formula (I), a compound represented by formula (II), hydantoic acid, allylamine, aminoguanidine, o-aminobenzoic acid, L-(+)-cysteine, benzylamine, DL-serine, morpholine, N-hydroxyethyl morpholine, o-aminobenzyl alcohol, quinuclidine, or salts thereof, tetramethylammonium acetate, choline, or choline chloride, ##STR1## wherein R.sup.1 represents a hydroxyalkyl group having from 2 to 10 carbon atoms; and R.sup.2 and R.sup.3 each represents a hydrogen atom, an alkyl group having from 1 to 10 carbon atoms, a hydroxyalkyl group having from 2 to 20 carbon atoms or a group represented by the formula ##STR2## wherein n represents an integer from 1 to 10; and X and Y each represents a hydrogen atom, an alkyl group having from 1 to 10 carbon atoms, or a hydroxyalkyl group having from 2 to 10 carbon atoms. ##STR3## wherein R.sup.4 represents an alkyl group having from 1 to 10 carbon atoms; R.sup.5 and R.sup.6 each represents a hydrogen atom or an alkyl group having from 1 to 10 carbon atoms.In accordance with this method for processing a silver halide color photographic material, color images having high coloring property can be obtained within a short period of a color developing time without substantially using benzyl alcohol, which is disadvantageous in view of environmental pollution, in the color developing solution.The effect of the present invention is particularly remarkable in the case wherein the silver halide color photographic material contains a pyrazoloazole type magenta coupler represented by formula (III) as described in the specification.
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