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公开(公告)号:US20060123842A1
公开(公告)日:2006-06-15
申请号:US10538759
申请日:2003-12-13
Applicant: Martin Sohn , Eckhard Stroefer , Filip Nevejans , Ulrich Penzel , Hans-Jurgen Pallasch , Peter Abeel , Filip Deberdt , Jan Jacobs , Wolfgang Mackenroth
Inventor: Martin Sohn , Eckhard Stroefer , Filip Nevejans , Ulrich Penzel , Hans-Jurgen Pallasch , Peter Abeel , Filip Deberdt , Jan Jacobs , Wolfgang Mackenroth
IPC: F25J3/00
CPC classification number: C01B7/0731 , B01D53/002 , B01D2257/2045 , B01D2257/2064 , C01B7/0712 , C01B32/80 , C07C263/10 , Y02P20/154 , C07C265/14 , C07C265/12 , C07C265/10
Abstract: The invention relates to a process for the partial or complete separation of a mixture comprising hydrogen chloride and phosgene, possibly solvents and possibly low boilers and inerts as are typically obtained in the preparation of isocyanates by reaction of amines with phosgene, which comprises firstly carrying out a partial or complete condensation of phosgene, then a distillation or stripping step in a column to remove the hydrogen chloride from the bottom product phosgene and subsequently a scrub of the top product hydrogen chloride by means of the process solvent to absorb the phosgene in the process solvent. An after-purification by means of adsorption on activated carbon or by another suitable method can subsequently be carried out to remove solvent residues.