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    Process for the production of aliphatic isocyanates
    1.
    发明授权
    Process for the production of aliphatic isocyanates 有权
    生产脂族异氰酸酯的方法

    公开(公告)号：US08455695B2

    公开(公告)日：2013-06-04

    申请号：US12775715

    申请日：2010-05-07

    申请人： Rory D. Daussin ,  Paula A. Cameron ,  Lao-Jer Chen ,  Jorge Jimenez ,  Joerg-Peter Gehrke

    发明人： Rory D. Daussin ,  Paula A. Cameron ,  Lao-Jer Chen ,  Jorge Jimenez ,  Joerg-Peter Gehrke

    IPC分类号： C07C263/10

    CPC分类号： C07C263/10 ,  C07C265/14 ,  C07C265/04 ,  C07C265/10

    摘要： The present invention is a process for aliphatic or cycloaliphatic isocyanate. The process comprises reacting an aliphatic or cycloaliphatic primary amine, with phosgene in the presence of an inert solvent wherein the initial reaction temperature is between 100 and 130° C. and the temperature is subsequently ramped to 150 to 180° C. during the course of the reaction, the solvent to amine weight ratio is 95:5 to 80:20, the total reaction pressure is maintained between 50 and 350 psig and the amine is rapidly dispersed in the phosgene through injection in a region of high efficiency mixing.

    摘要翻译： 本发明是脂肪族或脂环族异氰酸酯的方法。 该方法包括在惰性溶剂存在下使脂族或脂环族伯胺与光气反应，其中初始反应温度为100-130℃，然后在过程中将温度升至150-180℃ 反应，溶剂与胺的重量比为95:5至80:20，总反应压力保持在50至350psig之间，胺通过注射在高效混合区域中快速分散在光气中。

    NOVEL FULLERENE CYCLOPROPANATION REACTION
    2.
    发明申请
    NOVEL FULLERENE CYCLOPROPANATION REACTION 审中-公开
    新的富勒烯循环反应

    公开(公告)号：US20110178316A1

    公开(公告)日：2011-07-21

    申请号：US13056405

    申请日：2009-07-28

    申请人： Jing Zhang

    发明人： Jing Zhang

    IPC分类号： C07C247/10 ,  C07C265/08 ,  C07C211/31 ,  C07C229/36 ,  C07C271/12 ,  C07C275/24

    CPC分类号： C07C211/13 ,  C07C247/22 ,  C07C265/10 ,  C07C265/14

    摘要： Fullerene compounds represented by the formulae Cm[C(R)CON3]n, Cm[C(R)NCO]n, Cm[C(R)NHCORd]n, and Cm[C(R)NH2]n, wherein Cm represents a fullerene moiety having m carbon atoms, m represents an even integer from about 60 to about 200, n represents an integer of about 1 or more, R represents an electron-withdrawing group, and Rd represents an alkoxy or alkylamino group. In addition, processes for preparing these fullerene compounds involving reacting an acyl azide with a fullerene in the presence of a base.

    摘要翻译： 由式Cm [C（R）CON3] n，Cm [C（R）NCO] n，Cm [C（R）NHCORd] n和Cm [C（R）NH2] n表示的富勒烯化合物，其中Cm表示 具有m个碳原子的富勒烯部分，m表示约60至约200的偶数整数，n表示约1或更大的整数，R表示吸电子基团，Rd表示烷氧基或烷基氨基。 此外，制备这些富勒烯化合物的方法包括在碱的存在下使酰基叠氮化物与富勒烯反应。

    Polyisocyanate mixtures, a process for their production and their use for the production of polyurethanes
    4.
    发明授权
    Polyisocyanate mixtures, a process for their production and their use for the production of polyurethanes 失效
    多异氰酸酯混合物，其生产方法及其用于生产聚氨酯的方法

    公开(公告)号：US5464921A

    公开(公告)日：1995-11-07

    申请号：US156202

    申请日：1993-11-22

    申请人： Hans-Josef Laas ,  Reinhard Halpaap ,  Christian Wamprecht ,  Hans-Ulrich Meier-Westhues ,  Wolfgang Schultz ,  Lothar Kahl

    发明人： Hans-Josef Laas ,  Reinhard Halpaap ,  Christian Wamprecht ,  Hans-Ulrich Meier-Westhues ,  Wolfgang Schultz ,  Lothar Kahl

    IPC分类号： C07C265/14 ,  C07C265/04 ,  C07C265/10 ,  C07C271/10 ,  C07C271/24 ,  C07D251/34 ,  C08G18/10 ,  C08G18/73 ,  C08G18/75 ,  C08G18/76 ,  C09D5/03 ,  C09D5/46 ,  C09D175/00 ,  C09D175/04 ,  C08G18/32

    CPC分类号： C07C265/10 ,  C07C265/04 ,  C07C271/10 ,  C07C271/24 ,  C07D251/34

    摘要： The present invention relates to polyisocyanate mixtures which are solid below 40.degree. C. and liquid above 125.degree. C. and which havea) an average isocyanate functionality of at least 2.1,b) a content of free isocyanate groups bonded to tertiary (cyclo)aliphatic carbon atoms (calculated as NCO; molecular weight=42) of 5 to 22 wt. %,c) a urethane group content calculated as --NH--CO--O--; molecular weight=59) of 2 to 30 wt. %,d) an isocyanurate group content (calculated as C.sub.3 N.sub.3 O.sub.3 ; molecular weight=126) of 0 to 30 wt. % ande) a carboxylic acid ester group content (calculated as --CO--O--; molecular weight=44) of 0 to 25 wt. % and/orf) a carbonate group content (calculated as --O--CO--O--; molecular weight=60) of from 0 to 34 wt. %with the proviso that the total amount of ester groups e) and carbonate groups f) is at least 2 wt. %.The present invention also relates to a process for the production of these polyisocyanate mixtures and to their use for the production of polyurethanes, in particular as the crosslinking component in heat-curable two-component polyurethane powder coatings for coating heat-resistant substrates.

    摘要翻译： 本发明涉及固体低于40℃和高于125℃的液体的多异氰酸酯混合物，其具有a）平均异氰酸酯官能度至少为2.1，b）结合到叔（环）的游离异氰酸酯基团的含量， 脂肪族碳原子（以NCO计算;分子量= 42）为5〜22重量份。 ％，c）以-NH-CO-O-计算的氨基甲酸酯基含量; 分子量= 59）为2〜30wt。 ％，d）异氰脲酸酯基含量（以C3N3O3计算;分子量= 126）为0〜30wt。 ％和e）羧酸酯基含量（以-CO-O-计算;分子量= 44）为0〜25重量％。 ％和/或f）0至34重量％的碳酸酯基含量（以-O-CO-O-计算;分子量= 60） ％，条件是酯基e）和碳酸酯基团f）的总量为至少2重量％。 ％。 本发明还涉及生产这些多异氰酸酯混合物的方法及其用于生产聚氨酯的方法，特别是作为用于涂覆耐热基材的可热固化双组分聚氨酯粉末涂料中的交联组分。

    Aliphatic-cycloaliphatic diisocyanates
    6.
    发明授权
    Aliphatic-cycloaliphatic diisocyanates 失效
    脂肪族 - 脂环族二异氰酸酯

    公开(公告)号：US4613685A

    公开(公告)日：1986-09-23

    申请号：US691103

    申请日：1985-01-14

    申请人： Gerhard Klein ,  Dieter Arlt

    发明人： Gerhard Klein ,  Dieter Arlt

    IPC分类号： C08G18/00 ,  C07C67/00 ,  C07C211/36 ,  C07C241/00 ,  C07C265/10 ,  C07C265/14 ,  C08G18/73 ,  C08G18/75 ,  C08G18/80 ,  C07C119/045

    CPC分类号： C07C265/10 ,  C07C211/36 ,  C08G18/756 ,  C07C2101/08

    摘要： The present invention relates to diisocyanates having an isocyanate content of from about 20 to 50% by weight, optionally in the form of isomeric mixtures, characterized in that, in addition to containing a sterically unhindered isocyanate group attached to a primary aliphatic carbon atom, they contain a sterically hindered isocyanate group attached to a tertiary carbon atom which forms part of a cycloaliphatic ring system.The invention also relates to the use of the new diisocyanates, optionally blocked with blocking agents for isocyanate groups, as isocyanate component for the preparation of polyurethanes.

    摘要翻译： 本发明涉及异氰酸酯含量为约20至50重量％，任选地为异构混合物形式的二异氰酸酯，其特征在于，除了含有连接到伯脂肪族碳原子上的空间未阻碍的异氰酸酯基之外，它们 含有连接到形成脂环族环系的一部分的叔碳原子上的空间位阻异氰酸酯基团。 本发明还涉及使用任选用封端剂封端的异氰酸酯二异氰酸酯作为制备聚氨酯的异氰酸酯组分的用途。

    Process for the production of 2-chloroalkyl-(or cycloalkyl)-isocyanide dichlorides
    9.
    发明授权
    Process for the production of 2-chloroalkyl-(or cycloalkyl)-isocyanide dichlorides 失效
    生产2-氯代（2-环己基） - 异氰酸酯二氯化物的方法

    公开(公告)号：US3673254A

    公开(公告)日：1972-06-27

    申请号：US3673254D

    申请日：1968-06-17

    申请人： BAYER AG

    发明人： ARLT DIETER ,  HOLTSCHMIDT HANS

    IPC分类号： A47B53/02 ,  C07C119/00

    CPC分类号： C07C263/00 ,  C07C251/00 ,  C07C2601/14 ,  C07C265/04 ,  C07C265/10

    摘要： IN WHICH R1 to R4 are the same as defined above, including N=CCl2 as optional further substituent for said substituted radicals, and being usable as intermediates for producing plastics auxiliaries, or directly for the production of isocyanates which optionally may be converted in turn with amines into ureas in the known manner, or directly as plant protection agents.

    Production of 2-chloro-alkyl-(or cycloalkyl or aromatic)isocyanide dichlorides by reacting an olefin of the formula IN WHICH R1 to R4 each individually is hydrogen, alkyl, cycloalkyl, aromatic having up to 10 carbon atoms, or such radicals optionally substituted with NO2, halo, or alkoxy, or R1 and R2 together with the GROUP FORM AN ALICYCLIC RING SYSTEM OPTIONALLY CONTAINING AN SO2- group with hydrocyanic acid and with a chlorine-contributing compound, e.g. chlorine or sulfuryl chloride, in an amount at least equivalent to the sum total of the quantities of olefin and hydrocyanic acid used, e.g. at a temperature of about -10* to +40* C; the produced isocyanide dichlorides having the corresponding formula

    摘要翻译： 通过使式IN的化合物R1至R4各自独立地生产2-氯 - 烷基 - （或环烷基或芳族） - 异氰化物二氯化物，其各自为氢，烷基，环烷基，具有至多10个碳原子的芳族或任选地 被NO 2，卤素或烷氧基取代，或者R 1和R 2与可选择地含有-SO 2 - 基团的氢氧化合物和与氯气有关的化合物组合的基团形式的烷基环系统，例如 氯或磺酰氯，其量至少等于使用的烯烃和氢氰酸的量的总和，例如。 在约-10℃至+ 40℃的温度下; 所制备的具有相应式Ⅰ至R4的异氰化二氯化物与上述定义相同，包括-N = CCl 2，作为任选的取代基的另外的取代基，可用作生产塑料助剂的中间体，或直接用于制备 任选地可以以已知的方式或者直接作为植物保护剂将胺转化成脲类的异氰酸酯转化成脲。