PROCESS AND APPARATUS FOR PRODUCING AMMONIUM SULFATE CRYSTALS
    11.
    发明申请
    PROCESS AND APPARATUS FOR PRODUCING AMMONIUM SULFATE CRYSTALS 有权
    生产硫酸汞晶体的方法和装置

    公开(公告)号:US20160159657A1

    公开(公告)日:2016-06-09

    申请号:US14899579

    申请日:2014-06-20

    申请人: CAP III B.V.

    IPC分类号: C01C1/24 B01D9/00

    摘要: The present invention provides a continuous process for producing ammonium sulfate crystals, wherein said process comprises: (a) feeding to a first group of crystallization sections, which crystallization sections are heat integrated in series, a first aqueous ammonium sulfate solution that contains one or more impurities; (b) feeding to a second group of crystallization sections, which crystallization sections are heat integrated in series, a second aqueous ammonium sulfate solution that contains one or more impurities; (c) crystallizing ammonium sulfate crystals in each crystallization section respectively from each of said solutions of ammonium sulfate that contain one or more impurities; (d) purging a fraction of the ammonium sulfate solution that contains one or more impurities from each of said crystallization sections; and (e) discharging ammonium sulfate crystals from each crystallization section, characterized in that: (i) both the first group of crystallization sections and the second group of crystallization sections are together heat integrated in one series of crystallization sections; wherein the first group of crystallization sections operates at higher temperature than the second group of crystallization sections; and (ii) the composition of the first aqueous ammonium sulfate solution that contains one or more impurities is different to the composition of the second aqueous ammonium sulfate solution that contains one or more impurities. Further provided is apparatus suitable for producing ammonium sulfate crystals.

    摘要翻译: 本发明提供了一种用于生产硫酸铵晶体的连续方法,其中所述方法包括:(a)将第一组结晶部分进料到该第一组结晶部分,该结晶部分是串联的热积分法,第一组硫酸铵水溶液含有一种或多种 杂质; (b)将第二组结晶部分进料到该第二组结晶部分,该结晶部分串联加热一体化,含有一种或多种杂质的第二硫酸铵溶液; (c)分别从含有一种或多种杂质的所述硫酸铵溶液中分别在每个结晶段中结晶硫酸铵晶体; (d)从每个所述结晶部分清洗含有一种或多种杂质的硫酸铵溶液的一部分; 和(e)从每个结晶部分排出硫酸铵晶体,其特征在于:(i)第一组结晶部分和第二组结晶部分一起热集成在一系列结晶部分中; 其中所述第一组结晶段在比所述第二组结晶段更高的温度下操作; 和(ii)含有一种或多种杂质的第一硫酸铵水溶液的组成与含有一种或多种杂质的第二硫酸铵水溶液的组成不同。 还提供了适用于生产硫酸铵晶体的装置。