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公开(公告)号：US07153647B2
公开(公告)日：2006-12-26
申请号：US10847833
申请日：2004-05-18
CPC分类号： G03C1/005 , G03C1/498 , G03C1/49827 , G03C1/49845 , G03C1/4989 , G03C7/3041 , G03C2001/03588 , G03C2001/03594 , G03C2001/091 , G03C2001/7448 , G03C2200/16 , Y10S430/165 , Y10S430/166
摘要： A black and white thermographic recording material comprising a thermosensitive element and a support, the thermosensitive element containing at least one substantially light-insensitive organic silver salt, a binder and optionally photosensitive silver halide, characterized in that the thermosensitive element further contains deliberately added metal nano-particles in a molar ratio with respect to the total molar concentration of the at least one substantially light-insensitive organic silver salt in the range of 0.05:1 to 10−6:1; and the use for the purpose of increasing the ratio of Dmax to the quantity of said substantially light-insensitive organic silver salts per unit area of the above-mentioned thermographic recording material.
摘要翻译： 包含热敏元件和载体的黑色和白色温度记录材料，所述热敏元件含有至少一种基本上不受光敏的有机银盐，粘合剂和任选的感光卤化银，其特征在于，所述热敏元件还包含有意添加的金属纳米 相对于至少一种基本上不光敏感的有机银盐的总摩尔浓度的摩尔比在0.05:1至10-6:1范围内的颗粒; 以及用于将上述热敏记录材料的每单位面积中的D max max与所述基本上不受光敏感的有机银盐的比例增加的目的的用途。
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12.发明授权
公开(公告)号：US6096486A
公开(公告)日：2000-08-01
申请号：US982318
申请日：1997-12-10
申请人： Sabine Emmers , Bartholomeus Horsten , Ingrid Geuens , Yvan Gilliams , Andre Bellens , Dirk Bollen , Ivan Hoogmartens
发明人： Sabine Emmers , Bartholomeus Horsten , Ingrid Geuens , Yvan Gilliams , Andre Bellens , Dirk Bollen , Ivan Hoogmartens
CPC分类号： G03C1/49809 , C07C51/412 , G03C1/498 , G03C1/4989
摘要： A recording material comprising a support and a thermosensitive element containing silver behenate, an organic reducing agent therefor in thermal working relationship therewith and a binder, wherein the silver behenate is not associated with mercury and/or lead ions and when the recording material is irradiated with a copper K.alpha..sub.1 X-ray source the ratio, normalized to a quantity of silver in the recording material of 1 g per m.sup.2 thereof, of the sum of the peak heights of the X-ray diffraction lines attributable to silver behenate at Bragg angles, 2.THETA., of 6.01.degree., 7.56.degree., 9.12.degree., 10.66.degree., 12.12.degree. and 13.62.degree. to the sum of the peak heights of the X-ray diffraction lines at Bragg angles, 2.THETA., of 25.60.degree., 35.16.degree. and 43.40.degree. of NIST standard 1976, rhombohedral Al.sub.2 O.sub.3, determined with the same X-ray diffractometer in the same state of adjustment, is greater than 0.85; production processes for particles of substantially light-insensitive organic silver salt comprising silver behenate with these X-ray characteristics in the presence and substantial absence of organic solvent.
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公开(公告)号：US06962773B2
公开(公告)日：2005-11-08
申请号：US10306254
申请日：2002-11-27
CPC分类号： G03C1/005 , G03C1/498 , G03C1/49827 , G03C1/49845 , G03C1/4989 , G03C7/3041 , G03C2001/03588 , G03C2001/03594 , G03C2001/091 , G03C2001/7448 , G03C2200/16 , Y10S430/165 , Y10S430/166
摘要： A black and white thermographic recording material comprising a thermosensitive element and a support, the thermosensitive element containing at least one substantially light-insensitive organic silver salt, a binder and optionally photosensitive silver halide, characterized in that the thermosensitive element further contains deliberately added metal nano-particles in a molar ratio with respect to the total molar concentration of the at least one substantially light-insensitive organic silver salt in the range of 0.05:1 to 10−6:1; and the use for the purpose of increasing the ratio of Dmax to the quantity of said substantially light-insensitive organic silver salts per unit area of the above-mentioned thermographic recording material.
摘要翻译： 包含热敏元件和载体的黑色和白色温度记录材料，所述热敏元件含有至少一种基本上不受光敏的有机银盐，粘合剂和任选的感光卤化银，其特征在于，所述热敏元件还包含有意添加的金属纳米 相对于至少一种基本上不光敏感的有机银盐的总摩尔浓度的摩尔比在0.05:1至10-6:1范围内的颗粒; 以及用于将上述热敏记录材料的每单位面积中的D max max与所述基本上不受光敏感的有机银盐的比例增加的目的的用途。
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14.发明授权Recording materials with improved shelf-life, image tone and/or stability upon thermal development 有权记录材料，具有改善的保质期，图像色调和/或热稳定性公开(公告)号：US06579671B2
公开(公告)日：2003-06-17
申请号：US09854749
申请日：2001-05-14
申请人： Sabine Emmers , Bartholomeus Horsten , Ingrid Geuens , Yvan Gilliams , Dirk Bollen , Ivan Hoogmartens , Andre Bellens
发明人： Sabine Emmers , Bartholomeus Horsten , Ingrid Geuens , Yvan Gilliams , Dirk Bollen , Ivan Hoogmartens , Andre Bellens
IPC分类号： G03C100
CPC分类号： G03C1/00 , G03C1/49809 , G03C1/4989 , G03C2200/43
摘要： A recording material comprising a support and a thermosensitive element containing one or more of silver behenate, silver palmitate, and silver stearate, an organic reducing agent therefor in thermal working relationship therewith and a binder, wherein the silver behenate, palmitate, or stearate is not associated with mercury and/or lead ions, production processes for particles of substantially light-insensitive organic silver salt primarily comprising silver behenate, silver palmitate, or stearate, with described X-ray characteristics in the substantial absence of organic solvent.
摘要翻译： 一种记录材料，其包含载体和含有山嵛酸银，棕榈酸棕榈酯和硬脂酸银中的一种或多种的热敏元件，与其热加工关系的有机还原剂和粘合剂，其中山嵛酸银，棕榈酸酯或硬脂酸酯不是 与汞和/或铅离子相关的生物过程，主要包含山嵛酸银，棕榈酸棕榈酸酯或硬脂酸酯的基本上不受光敏的有机银盐的颗粒的生产方法，其基本上不存在有机溶剂时具有所述的X射线特性。
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15.发明授权公开(公告)号：US07348296B2
公开(公告)日：2008-03-25
申请号：US10859288
申请日：2004-06-02
IPC分类号： B41M5/30
CPC分类号： G03C1/4989 , G03C1/04 , G03C1/49863
摘要： A substantially light-insensitive monosheet thermographic recording material comprising a support and on one side of the support a thermosensitive element, the thermosensitive element comprising at least one substantially light-insensitive silver salt of a carboxylic acid, at least one reducing agent therefor in thermal working relationship therewith and at least one binder, the at least one binder comprising at least one first polymer consisting of vinyl aceto-acetal monomer units and optionally monomer units selected from the group consisting of vinyl alcohol, vinyl acetate and itaconic acid monomer units, wherein the weight ratio of the at least one binder to the light-insensitive silver salt(s) of a carboxylic acid in the thermosensitive element is greater than 1.6; and the at least one binder optionally contains less than 40% by weight of a second polymer consisting of vinyl butyral monomer units and optionally vinyl alcohol and/or vinyl acetate monomer units.
摘要翻译： 一种基本上不光敏的单片热成像记录材料，其包含支撑体，并且在支撑体的一侧上具有热敏元件，所述热敏元件包含至少一种基本上不受光敏的羧酸银盐，至少一种用于热加工的还原剂 与至少一种粘合剂，所述至少一种粘合剂包含至少一种由乙烯基乙酰 - 缩醛单体单元组成的第一聚合物和任选的选自乙烯醇，乙酸乙烯酯和衣康酸单体单元的单体单元，其中 所述至少一种粘合剂与所述热敏元件中羧酸的不敏感的银盐的重量比大于1.6; 并且所述至少一种粘合剂任选地包含小于40重量％的由乙烯醇缩丁醛单体单元和任选的乙烯醇和/或乙酸乙烯酯单体单元组成的第二聚合物。
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公开(公告)号：US06306572B1
公开(公告)日：2001-10-23
申请号：US09135637
申请日：1998-08-17
IPC分类号： G03C1498
CPC分类号： G03C1/4989 , G03C1/04 , G03C1/49863 , G03C2200/36
摘要： A substantially light-insensitive black and white thermographic material including a support and a thermosensitive element, containing a substantially light-insensitive organic silver salt, a reducing agent therefor in thermal working relationship therewith and a binder, wherein the binder is a water-dispersible film-forming polymer with covalently bonded moieties with one or more acid groups or anhydrides thereof and the thermographic material is thermally developable under substantially water-free conditions; and a process for producing the substantially light-insensitive black and white thermographic material comprising the steps of: producing an aqueous dispersion of the substantially light-insensitive organic silver salt; producing one or more aqueous coating compositions containing together the aqueous dispersion of the substantially light-insensitive organic silver salt, the reducing agent and the binder; and applying the one or more aqueous coating compositions to the support thereby forming after drying the thermosensitive element.
摘要翻译： 一种基本上不透光的黑色和白色热成像材料，包括支撑体和热敏元件，其含有基本上不受光敏的有机银盐，与其热加工关系的还原剂和粘合剂，其中粘合剂是水分散性膜 具有共价键合的部分与一个或多个酸基团或其酸酐并且热成像材料在基本上无水条件下可热显影; 以及用于生产基本上不透光的黑白热成像材料的方法，包括以下步骤：制备基本上不光敏的有机银盐的水分散体; 制备一种或多种含有基本上不光敏的有机银盐，还原剂和粘合剂的水性分散体的水性涂料组合物; 并且将一种或多种水性涂料组合物施加到载体上，从而在干燥热敏元件之后形成。
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17.发明申请Binders for use in the thermosensitive elements of substantially light-insensitive thermographic recording materials 审中-公开用于基本上不透光的热敏记录材料的热敏元件的粘合剂公开(公告)号：US20050003315A1
公开(公告)日：2005-01-06
申请号：US10859528
申请日：2004-06-02
CPC分类号： G03C1/4989 , B41M5/3372 , B41M5/44 , B41M5/443 , B41M2205/40 , G03C1/04
摘要： A substantially light-insensitive monosheet thermographic recording material comprising a support and on one side of the support a thermosensitive element, the thermosensitive element comprising at least one substantially light-insensitive silver salt of a carboxylic acid, at least one reducing agent therefor in thermal working relationship therewith and at least one binder, the at least one binder comprising at least one first polymer consisting of vinyl aceto-acetal monomer units, vinyl butyral monomer units and monomer units selected from the group consisting of, vinyl alcohol, vinyl acetate and itaconic acid monomer units, wherein the weight ratio of the at least one binder to the light-insensitive silver salt(s) of a carboxylic acid in the thermosensitive element is greater than 1.5; and the at least one binder optionally contains less than 40% by weight of a second polymer consisting of vinyl butyral monomer units and optionally vinyl alcohol and/or vinyl acetate monomer units.
摘要翻译： 一种基本上不光敏的单片热成像记录材料，其包含支撑体，并且在支撑体的一侧上具有热敏元件，所述热敏元件包含至少一种基本上不受光敏的羧酸银盐，至少一种用于热加工的还原剂 与至少一种粘合剂，所述至少一种粘合剂包含至少一种由乙烯基乙酰 - 缩醛单体单元，乙烯基缩丁醛单体单元和选自由乙烯醇，乙酸乙烯酯和衣康酸组成的组的单体单元组成的第一聚合物 单体单元，其中所述热敏元件中所述至少一种粘合剂与所述不敏感的羧酸的银盐的重量比大于1.5; 并且所述至少一种粘合剂任选地包含小于40重量％的由乙烯醇缩丁醛单体单元和任选的乙烯醇和/或乙酸乙烯酯单体单元组成的第二聚合物。
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18.发明申请公开(公告)号：US20050003298A1
公开(公告)日：2005-01-06
申请号：US10859288
申请日：2004-06-02
CPC分类号： G03C1/4989 , G03C1/04 , G03C1/49863
摘要： A substantially light-insensitive monosheet thermographic recording material comprising a support and on one side of the support a thermosensitive element, the thermosensitive element comprising at least one substantially light-insensitive silver salt of a carboxylic acid, at least one reducing agent therefor in thermal working relationship therewith and at least one binder, the at least one binder comprising at least one first polymer consisting of vinyl aceto-acetal monomer units and optionally monomer units selected from the group consisting of vinyl alcohol, vinyl acetate and itaconic acid monomer units, wherein the weight ratio of the at least one binder to the light-insensitive silver salt(s) of a carboxylic acid in the thermosensitive element is greater than 1.6; and the at least one binder optionally contains less than 40% by weight of a second polymer consisting of vinyl butyral monomer units and optionally vinyl alcohol and/or vinyl acetate monomer units.
摘要翻译： 一种基本上不光敏的单片热成像记录材料，其包含支撑体，并且在支撑体的一侧上具有热敏元件，所述热敏元件包含至少一种基本上不受光敏的羧酸银盐，至少一种用于热加工的还原剂 与至少一种粘合剂，所述至少一种粘合剂包含至少一种由乙烯基乙酰 - 缩醛单体单元组成的第一聚合物和任选的选自乙烯醇，乙酸乙烯酯和衣康酸单体单元的单体单元，其中 所述至少一种粘合剂与所述热敏元件中羧酸的不敏感的银盐的重量比大于1.6; 并且所述至少一种粘合剂任选地包含小于40重量％的由乙烯醇缩丁醛单体单元和任选的乙烯醇和/或乙酸乙烯酯单体单元组成的第二聚合物。
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公开(公告)号：US6063559A
公开(公告)日：2000-05-16
申请号：US135628
申请日：1998-08-17
IPC分类号： G03C1/498
CPC分类号： G03C1/49836 , G03C1/49863 , G03C1/49872 , G03C1/4989
摘要： A (photo)thermographic recording material according to the present invention comprising a thermosensitive element contains a substantially light-insensitive organic silver salt, a reducing agent therefor in thermal working relationship therewith and a binder (and optionally further including photosensitive silver halide), wherein the (photo)thermographic recording material is exclusive of polypyrrole/poly(styrene sulfonic acid) in an electrically-conductive layer and further contains a compound represented by formula (I) or a reaction product thereof with a polymer having active hydrogen atoms: ##STR1## where R.sup.1 and R.sup.3 independently represent hydrogen, a hydroxyalkyl group, an alkoxyalkyl group, an alkyl group, a --(C.dbd.O)R.sup.5 group or an alkenyl group; and R.sup.2 and R.sup.4 independently represent a hydroxyalkyl group, an alkoxyalkyl group, an alkyl group, a --(C.dbd.O)R.sup.5 group or an alkenyl group; or R.sup.1 and R.sup.2 together and R.sup.3 and R.sup.4 together independently represent the atoms needed to close a carbocyclic or heterocyclic ring; R.sup.5 represents an aryl, a substituted aryl, an alkyl or a substituted alkyl group; and Z represents the atoms needed to complete a 5 ring-atom or 6 ring-atom hetero-aromatic ring; and a production process therefor.
摘要翻译： 包含热敏元件的根据本发明的（照片）热成像记录材料包含基本上不光敏的有机银盐，与其热加工关系的还原剂和粘合剂（以及任选地还包括感光卤化银），其中 （光）热成像记录材料在导电层中不包含聚吡咯/聚（苯乙烯磺酸），并且还含有由式（I）表示的化合物或其与具有活性氢原子的聚合物的反应产物：其中R1和 R3独立地表示氢，羟基烷基，烷氧基烷基，烷基， - （C = O）R5基或烯基; 和R 2和R 4独立地表示羟基烷基，烷氧基烷基，烷基， - （C = O）R 5基或链烯基; 或R 1和R 2一起并且R 3和R 4一起独立地表示封闭碳环或杂环所需的原子; R5表示芳基，取代的芳基，烷基或取代的烷基; Z表示完成5环原子或6环原子杂芳环所需的原子; 及其生产工艺。
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公开(公告)号：US06774084B2
公开(公告)日：2004-08-10
申请号：US10106172
申请日：2002-03-26
申请人： Johan Loccufier , Geert Defieuw , Ivan Hoogmartens
发明人： Johan Loccufier , Geert Defieuw , Ivan Hoogmartens
IPC分类号： B41M530
CPC分类号： G03C1/4989 , G03C1/49827 , G03C1/49845
摘要： A monosheet black and white substantially light-insensitive thermographic recording material comprising a thermosensitive element and a support, the thermosensitive element containing a substantially light-insensitive organic silver salt, a 1,2-dihydroxyphenyl-compound in thermal working relationship therewith and a binder, wherein said 1,2-dihydroxyphenyl-compound is represented by formula (I): R1SO2R2, wherein R1 is an optionally substituted aryl group and R2 is selected from the group consisting of a 3,4,5-trihydroxyphenyl group, a 3-alkoxy-4,5-dihydroxyphenyl group and a 3-aryloxy-4,5-dihydroxyphenyl group; or said 1,2-dihydroxyphenyl-compound is represented by formula (II): R3COOR4, wherein R3 is a 3-alkoxy-4,5-dihydroxyphenyl group or a 3-aryloxy-4,5-dihydroxyphenyl group; and R4 is an alkyl group or an aryl group; and a thermographic recording process therefor.
摘要翻译： 包含热敏元件和载体的单片黑色和白色基本上不光敏感的热敏成像记录材料，所述热敏元件含有基本上不光敏的有机银盐，与其热处理的1,2-二羟基苯基化合物和粘合剂， 其中所述1,2-二羟基苯基化合物由式（I）表示：R 1 SO 2 R 2，其中R 1是任选取代的芳基，R 2选自 3,4,5-三羟基苯基，3-烷氧基-4,5-二羟基苯基和3-芳氧基-4,5-二羟基苯基; 或所述1,2-二羟基苯基化合物由式（II）表示：R 3 COOR 4，其中R 3为3-烷氧基-4,5-二羟基苯基或3-芳氧基-4 ，5-二羟基苯基; 和R 4是烷基或芳基; 及其热成像记录方法。
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