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公开(公告)号：US06432865B1
公开(公告)日：2002-08-13
申请号：US09657645
申请日：2000-09-07
IPC分类号： C08G6510
CPC分类号： C10M173/02 , C08G18/10 , C08G18/4837 , C08G18/4866 , C08G18/718 , C08G65/2651 , C08G65/336 , C10M107/34 , C10M145/26 , C10M145/28 , C10M145/30 , C10M2201/02 , C10M2209/103 , C10M2209/104 , C10M2209/105 , C10M2209/107 , C10N2220/02 , C10N2240/08 , C10N2250/02 , C08G18/307
摘要： The invention is a high molecular weight polyether polyol prepared by the reaction of one or more compounds having one or more active hydrogen compounds with one or more alkylene oxides in the presence of a catalyst comprising calcium having counterions of carbonate and a C6-10 alkanoate in a solvent or dispersant which does not contain active hydrogen atoms. The polyether polyol prepared preferably has an equivalent weight of from about 1000 to about 20,000, a polydispersity of 1.3 or less and a residual catalyst level of from about 0 to about 2000 parts per million (ppm). In another embodiment the invention is a process for preparing such high molecular weight polyether polyols. The process comprises first, contacting one or more compounds having one or more active hydrogen atoms with one or more alkylene oxides in the presence of a catalyst. The catalyst comprises calcium having counterions of carbonate and a C6-10 alkanoate in a solvent, wherein the solvent does not contain active hydrogen atoms. The mixture is exposed to conditions at which the alkylene oxides react with the compound containing more than one active hydrogen atoms such that a polyether polyol is prepared which has an equivalent weight of from about 1,000 to about 20,000, a polydispersity of about 1.3 or less and a residual catalyst level of from about 0 to about 1000 (ppm).
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公开(公告)号：US5021180A
公开(公告)日：1991-06-04
申请号：US432958
申请日：1989-11-07
申请人： Philip W. McGraw
发明人： Philip W. McGraw
IPC分类号： C10M105/18 , C09K5/00 , C09K5/04 , C09K5/08 , C10M105/62 , C10M107/34 , C10M169/04 , C10M171/00 , C10N20/02 , C10N40/30
CPC分类号： C10M169/041 , C09K5/041 , C10M107/34 , C10M171/008 , C10M2207/026 , C10M2209/105 , C10M2209/107 , C10M2209/108 , C10M2211/0206 , C10M2211/022 , C10M2211/0225 , C10M2211/0245 , C10M2211/06 , C10M2215/04 , C10M2215/042 , C10M2215/064 , C10M2215/065 , C10M2215/14 , C10M2215/22 , C10M2215/221 , C10M2215/224 , C10M2215/225 , C10M2215/226 , C10M2215/26 , C10M2215/30 , C10M2217/04 , C10M2219/044 , C10M2223/043 , C10N2220/02 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： A refrigeration fluid compositions for compression refrigeration which have an upper solution critical temperature equal to or greater than 60.degree. C. are composed of (A) selected hydrochlorofluorocarbons and hydrofluorocarbons and (B) polyether polyols having viscosities of greater than 80 centistokes at 38.degree. C. and having a number average molecular weight from about 400 to about 2000 wherein the polyols are the residue of an active hydrogen compound such as glycerine or ethylene diamine.
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公开(公告)号：US06423661B1
公开(公告)日：2002-07-23
申请号：US09657157
申请日：2000-09-07
IPC分类号： C08G6510
CPC分类号： C10M173/02 , C08G18/10 , C08G18/4837 , C08G18/4866 , C08G18/718 , C08G65/2651 , C08G65/336 , C10M107/34 , C10M145/26 , C10M145/28 , C10M145/30 , C10M2201/02 , C10M2209/103 , C10M2209/104 , C10M2209/105 , C10M2209/107 , C10N2220/02 , C10N2240/08 , C10N2250/02 , C08G18/307
摘要： The invention is a high molecular weight polyether polyol prepared by the reaction of one or more compounds having one or more active hydrogen compounds with one or more alkylene oxides in the presence of a catalyst comprising calcium having counterions of carbonate and a C6-10 alkanoate in a solvent or dispersant which does not contain active hydrogen atoms. The polyether polyol prepared preferably has an equivalent weight of from about 1000 to about 20,000, a polydispersity of 1.3 or less and a residual catalyst level of from about 0 to about 2000 parts per million (ppm). In another embodiment the invention is a process for preparing such high molecular weight polyether polyols. The process comprises first, contacting one or more compounds having one or more active hydrogen atoms with one or more alkylene oxides in the presence of a catalyst. The catalyst comprises calcium having counterions of carbonate and a C6-10 alkanoate in a solvent, wherein the solvent does not contain active hydrogen atoms. The mixture is exposed to conditions at which the alkylene oxides react with the compound containing more than one active hydrogen atoms such that a polyether polyol is prepared which has an equivalent weight of from about 1,000 to about 20,000, a polydispersity of about 1.3 or less and a residual catalyst level of from about 0 to about 1000 (ppm).
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公开(公告)号：US06255434B1
公开(公告)日：2001-07-03
申请号：US09300232
申请日：1999-04-27
IPC分类号： C08G5968
CPC分类号： C10M173/02 , C08G18/10 , C08G18/4837 , C08G18/4866 , C08G18/718 , C08G65/2651 , C08G65/336 , C10M107/34 , C10M145/26 , C10M145/28 , C10M145/30 , C10M2201/02 , C10M2209/103 , C10M2209/104 , C10M2209/105 , C10M2209/107 , C10N2220/02 , C10N2240/08 , C10N2250/02 , C08G18/307
摘要： The invention is a high molecular weight polyether polyol prepared by the reaction of one or more compounds having one or more active hydrogen compounds with one or more alkylene oxides in the presence of a catalyst comprising calcium having counterions of carbonate and a C6-10 alkanoate in a solvent or dispersant which does not contain active hydrogen atoms. The polyether polyol prepared preferably has an equivalent weight of from about 1000 to about 20,000, a polydispersity of about 1.3 or less and a residual catalyst level of from about 0 to about 2000 parts per million (ppm).
摘要翻译： 本发明是一种高分子量聚醚多元醇，其通过一种或多种具有一种或多种活性氢化合物与一种或多种烯化氧的化合物的反应制备，所述化合物在催化剂存在下，该催化剂包含具有与碳酸酯和C 6-10链烷酸酯的抗衡离子的钙 不含活性氢原子的溶剂或分散剂。 制备的聚醚多元醇的当量重量优选为约1000至约20,000，多分散度为约1.3或更小，残留催化剂含量为约0至约2000ppm（ppm）。
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