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公开(公告)号：US07544426B2
公开(公告)日：2009-06-09
申请号：US11329181
申请日：2006-01-11
申请人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
发明人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
CPC分类号： H01L51/0085 , C07F15/004 , C07F15/0066 , C07F15/008 , C07F15/0093 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1033 , C09K2211/1037 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1092 , C09K2211/185 , H01L27/3244 , H01L51/005 , H01L51/0059 , H01L51/0081 , H01L51/0084 , H01L51/5012 , H01L51/5016 , H01L51/5234 , H05B33/14 , Y10S428/917
摘要： A luminescence device having a layer containing a metal coordination compound which has a partial structure. MLm of formula (2) below and is preferably entirely represented by formula (3) below: MLmL′n (3) wherein M denotes a metal atom of Ir, Pt, Rh or Pd; represent mutually different bidentate ligands; m is 1 or 2 or 3; n is 0 or 1 or 2 with the proviso that m+n=2 or 3; the partial structure MLm is represented by formula (2) below (wherein B is an isoquinolyl group bonded to the metal M with its N and including a position-1 carbon atom bonded to a cyclic group A which includes the C bonded to the metal M), and the partial structure ML′n is represented by formula (4), (5) or (6) shown below. There is provided a luminescence device capable of high-efficiency luminescence and long-term high luminance and adapted to red luminescence.
摘要翻译： 一种发光装置，其具有含有部分结构的金属配位化合物的层。 优选完全由下式（3）表示的式（2）的MLm：<？in-line-formula description =“In-line formula”end =“lead”？> MLmL'n（3）<？in -line-formula description =“In-line Formulas”end =“tail”？>其中M表示Ir，Pt，Rh或Pd的金属原子; 代表相互不同的二齿配体; m为1或2或3; n为0或1或2，条件是m + n = 2或3; 部分结构MLm由下式（2）表示（其中B为与其金属M键合的含有N并且包含与环状基团A键合的位置1的碳原子的异喹啉基，其包括与金属M键合的C ），部分结构ML'n由下述式（4），（5）或（6）表示。 提供了能够高效发光和长期高亮度并适合红色发光的发光装置。
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公开(公告)号：US07078115B2
公开(公告)日：2006-07-18
申请号：US10942861
申请日：2004-09-17
申请人： Takao Takiguchi , Akira Tsuboyama , Shinjiro Okada , Jun Kamatani , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Manabu Furugori , Hidemasa Mizutani
发明人： Takao Takiguchi , Akira Tsuboyama , Shinjiro Okada , Jun Kamatani , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Manabu Furugori , Hidemasa Mizutani
CPC分类号： C07D221/16 , C07D221/10 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1018 , C09K2211/1029 , C09K2211/1044 , C09K2211/1088 , C09K2211/1092 , C09K2211/181 , C09K2211/185 , H01L27/3244 , H01L51/0059 , H01L51/0062 , H01L51/0081 , H01L51/0084 , H01L51/0085 , H01L51/0087 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： A metal coordination compound having a basic structure represented by formula: MLmL′n (1), wherein M is a metal atom of Ir, Pt, Rh or Pd; L and L′ are mutually different bidentate ligands; m is 1, 2 or 3; wherein at least one bidentate ligand has a partial structure formed by condensation via an alkylene group having 2–10 carbon atoms, is provided. In an electroluminescence device composed of one or a plurality of organic films disposed between a cathode and an anode, at least one layer is a luminescence layer which is formed by incorporating luminescence molecules constituting the metal coordination compound having a structure of the formula (1) described above as a guest material in a host material thereby to provide an electroluminescence device producing luminescence at high efficiency and stably keeping a high luminance for a long period.
摘要翻译： 具有由下式表示的基本结构的金属配位化合物：其中M是Ir，Pt，Rh或Pd的金属原子; L和L'是相互不同的二齿配体; m为1,2或3; 其中至少一个二齿配体具有通过具有2-10个碳原子的亚烷基缩合形成的部分结构。 在由设置在阴极和阳极之间的一个或多个有机膜构成的电致发光器件中，至少一层是通过掺入构成具有式（1）结构的金属配位化合物的发光分子形成的发光层， 作为主体材料中的客体材料，从而提供以高效率产生发光并且长时间稳定地保持高亮度的电致发光器件。
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23.发明申请公开(公告)号：US20050025996A1
公开(公告)日：2005-02-03
申请号：US10921917
申请日：2004-08-20
申请人： Akira Tsuboyama , Hidemasa Mizutani , Shinjiro Okada , Takao Takiguchi , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
发明人： Akira Tsuboyama , Hidemasa Mizutani , Shinjiro Okada , Takao Takiguchi , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
CPC分类号： H05B33/14 , C07F15/0033 , C07F15/006 , C07F15/0073 , C09K11/06 , C09K2211/1003 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1092 , C09K2211/185 , H01L51/0084 , H01L51/0085 , H01L51/5012 , Y10S428/917
摘要： A luminescence device that has an organic compound layer disposed between a pair of electrodes. This organic compound layer contains a metal coordination compound represented by the following formula (1): wherein M is Ir, Rh or Pd; n is 2 or 3; CyN is a substituted or unsubstituted cyclic group containing a nitrogen atom connected to M and capable of containing another nitrogen atom and/or a sulfur atom; and CyC is a substituted or unsubstituted cyclic group containing a carbon atom connected to M and capable of containing a nitrogen atom and/or a sulfur atom.
摘要翻译： 一种具有设置在一对电极之间的有机化合物层的发光装置。 该有机化合物层含有由下式（1）表示的金属配位化合物：其中M为Ir，Rh或Pd; n为2或3; CyN是含有与M连接的氮原子并且能够含有另外的氮原子和/或硫原子的取代或未取代的环状基团; CyC是含有与M连接并能够含有氮原子和/或硫原子的碳原子的取代或未取代的环状基团。
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公开(公告)号：US06824894B2
公开(公告)日：2004-11-30
申请号：US10181342
申请日：2002-07-17
申请人： Takao Takiguchi , Akira Tsuboyama , Shinjiro Okada , Jun Kamatani , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Manabu Furugori , Hidemasa Mizutani
发明人： Takao Takiguchi , Akira Tsuboyama , Shinjiro Okada , Jun Kamatani , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Manabu Furugori , Hidemasa Mizutani
IPC分类号： H05B3314
CPC分类号： C07D221/16 , C07D221/10 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1018 , C09K2211/1029 , C09K2211/1044 , C09K2211/1088 , C09K2211/1092 , C09K2211/181 , C09K2211/185 , H01L27/3244 , H01L51/0059 , H01L51/0062 , H01L51/0081 , H01L51/0084 , H01L51/0085 , H01L51/0087 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： A metal coordination compound having a basic structure represented by formula: MLmL′n (1), wherein M is a metal atom of Ir, Pt, Rh or Pd; L and L′ are mutually different bidentate ligands; m is 1, 2 or 3; wherein at least one bidentate ligand has a partial structure formed by condensation via an alkylene group having 2-10 carbon atoms, is provided. In an electroluminescence device composed of one or a plurality of organic films disposed between a cathode and an anode, at least one layer is a luminescence layer which is formed by incorporating luminescence molecules constituting the metal coordination compound having a structure of the formula (1) described above as a guest material in a host material thereby to provide an electroluminescence device producing luminescence at high efficiency and stably keeping a high luminance for a long period.
摘要翻译： 具有由式MLmL'n（1）表示的碱性结构的金属配位化合物，其中M是Ir，Pt，Rh或Pd的金属原子; L和L'是相互不同的二齿配体; m为1,2或3; 其中至少一个二齿配体具有通过具有2-10个碳原子的亚烷基缩合形成的部分结构。 在由设置在阴极和阳极之间的一个或多个有机膜构成的电致发光器件中，至少一层是通过掺入构成具有式（1）结构的金属配位化合物的发光分子形成的发光层， 作为主体材料中的客体材料，从而提供以高效率产生发光并且长时间稳定地保持高亮度的电致发光器件。
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公开(公告)号：US07527879B2
公开(公告)日：2009-05-05
申请号：US11694754
申请日：2007-03-30
申请人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
发明人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
CPC分类号： H01L51/0085 , C07F15/004 , C07F15/0066 , C07F15/008 , C07F15/0093 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1033 , C09K2211/1037 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1092 , C09K2211/185 , H01L27/3244 , H01L51/005 , H01L51/0059 , H01L51/0081 , H01L51/0084 , H01L51/5012 , H01L51/5016 , H01L51/5234 , H05B33/14 , Y10S428/917
摘要： A metal coordination compound having a structure according to formula (1) or (3), wherein ligand L is a phenylisoquinoline ligand and ligand L2 is different from L: A luminescence device and a display apparatus using this metal coordination compound are provided.
摘要翻译： 具有式（1）或（3）结构的金属配位化合物，其中配体L是苯基异喹啉配体，配体L2不同于L：发光装置和使用该金属配位化合物的显示装置。
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26.发明授权公开(公告)号：US07220495B2
公开(公告)日：2007-05-22
申请号：US10921917
申请日：2004-08-20
申请人： Akira Tsuboyama , Hidemasa Mizutani , Shinjiro Okada , Takao Takiguchi , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
发明人： Akira Tsuboyama , Hidemasa Mizutani , Shinjiro Okada , Takao Takiguchi , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
CPC分类号： H05B33/14 , C07F15/0033 , C07F15/006 , C07F15/0073 , C09K11/06 , C09K2211/1003 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1092 , C09K2211/185 , H01L51/0084 , H01L51/0085 , H01L51/5012 , Y10S428/917
摘要： A luminescence device that has an organic compound layer disposed between a pair of electrodes. This organic compound layer contains a metal coordination compound represented by the following formula (1): wherein M is Ir, Rh or Pd; n is 2 or 3; CyN is a substituted or unsubstituted cyclic group containing a nitrogen atom connected to M and capable of containing another nitrogen atom and/or a sulfur atom; and CyC is a substituted or unsubstituted cyclic group containing a carbon atom connected to M and capable of containing a nitrogen atom and/or a sulfur atom.
摘要翻译： 一种具有设置在一对电极之间的有机化合物层的发光装置。 该有机化合物层含有由下式（1）表示的金属配位化合物：其中M为Ir，Rh或Pd; n为2或3; CyN是含有与M连接的氮原子并且能够含有另外的氮原子和/或硫原子的取代或未取代的环状基团; CyC是含有与M连接并能够含有氮原子和/或硫原子的碳原子的取代或未取代的环状基团。
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公开(公告)号：US20060177694A1
公开(公告)日：2006-08-10
申请号：US11329181
申请日：2006-01-11
申请人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
发明人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
IPC分类号： H01L51/54 , H05B33/14 , C09K11/06 , C07D217/00
CPC分类号： H01L51/0085 , C07F15/004 , C07F15/0066 , C07F15/008 , C07F15/0093 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1033 , C09K2211/1037 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1092 , C09K2211/185 , H01L27/3244 , H01L51/005 , H01L51/0059 , H01L51/0081 , H01L51/0084 , H01L51/5012 , H01L51/5016 , H01L51/5234 , H05B33/14 , Y10S428/917
摘要： A luminescence device having a layer containing a metal coordination compound which has a partial structure. MLm of formula (2) below and is preferably entirely represented by formula (3) below: MLmL′n (3) wherein M denotes a metal atom of Ir, Pt, Rh or Pd; represent mutually different bidentate ligands; m is 1 or 2 or 3; n is 0 or 1 or 2 with the proviso that m+n=2 or 3; the partial structure MLm is represented by formula (2) below (wherein B is an isoquinolyl group bonded to the metal M with its N and including a position-1 carbon atom bonded to a cyclic group A which includes the C bonded to the metal M), and the partial structure ML′n is represented by formula (4), (5) or (6) shown below. There is provided a luminescence device capable of high-efficiency luminescence and long-term high luminance and adapted to red luminescence.
摘要翻译： 一种发光装置，其具有含有部分结构的金属配位化合物的层。 优选以下式（3）全部由式（3）表示：＆lt;＆RightArrow;＆CenterDot;＆CenterDot;＆CenterDot;＆CenterDot;＆CenterDot;＆CenterDot;＆CenterDot;＆CenterDot; （3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中M表示金属原子 Ir，Pt，Rh或Pd; 代表相互不同的二齿配体; m为1或2或3; n为0或1或2，条件是m + n = 2或3; 部分结构ML>由下式（2）表示（其中B是与其N键合到金属M上并包含与环状基团A键合的位置1的碳原子的异喹啉基），其中 包括与金属M键合的C），并且部分结构ML'N
由下面所示的式（4），（5）或（6）表示。 提供了能够高效发光和长期高亮度并适合红色发光的发光装置。 -
28.发明授权公开(公告)号：US06821646B2
公开(公告)日：2004-11-23
申请号：US09960285
申请日：2001-09-24
申请人： Akira Tsuboyama , Hidemasa Mizutani , Shinjiro Okada , Takao Takiguchi , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
发明人： Akira Tsuboyama , Hidemasa Mizutani , Shinjiro Okada , Takao Takiguchi , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
IPC分类号： H05B3314
CPC分类号： H05B33/14 , C07F15/0033 , C07F15/006 , C07F15/0073 , C09K11/06 , C09K2211/1003 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1092 , C09K2211/185 , H01L51/0084 , H01L51/0085 , H01L51/5012 , Y10S428/917
摘要： A luminescence device that has an organic compound layer disposed between a pair of electrodes. This organic compound layer contains a metal coordination compound represented by the following formula (1) wherein M is Ir, Rh or Pd; n is 2 or 3; CyN is a substituted or unsubstituted cyclic group containing a nitrogen atom connected to M and capable of containing another nitrogen atom and/or sulfur atom; and CyC is a substituted or unsubstituted cyclic group containing a carbon atom connected to M and capable of containing a nitrogen atom and/or a sulfur atom.
摘要翻译： 一种具有设置在一对电极之间的有机化合物层的发光装置。 该有机化合物层包含由下式（1）表示的金属配位化合物，其中M为Ir，Rh或Pd; n为2或3; CyN是含有与M连接的氮原子并且能够含有另外的氮原子和/或硫原子的取代或未取代的环状基团; CyC是含有与M连接并能够含有氮原子和/或硫原子的碳原子的取代或未取代的环状基团。
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29.发明授权公开(公告)号：US06815091B2
公开(公告)日：2004-11-09
申请号：US09961075
申请日：2001-09-24
申请人： Takao Takiguchi , Hidemasa Mizutani , Shinjiro Okada , Akira Tsuboyama , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
发明人： Takao Takiguchi , Hidemasa Mizutani , Shinjiro Okada , Akira Tsuboyama , Seishi Miura , Takashi Moriyama , Satoshi Igawa , Jun Kamatani , Manabu Furugori
IPC分类号： H05B3314
CPC分类号： C07F15/0086 , C07F15/0033 , C07F15/006 , C09K11/06 , C09K2211/1003 , C09K2211/1011 , C09K2211/1029 , C09K2211/185 , H01L51/0052 , H01L51/0059 , H01L51/0062 , H01L51/0081 , H01L51/0084 , H01L51/0085 , H01L51/0087 , H01L51/5012 , H01L51/5016 , H05B33/14 , Y10S428/917
摘要： A luminescence device comprising a pair of electrodes and an organic compound layer disposed therebetween. The layer contains a metal coordination compound represented by the following formula (1): wherein M is Ir, Rh or Pd; n is 2 or 3; and X1 to X8 is, independently, a hydrogen atom or a substituent selected from the group consisting of a halogen atom; a nitro group; a trifluoromethyl group; a trialkylsilyl group having three linear or branched alkyl groups each independently having 1-8 carbon atoms; and a linear or branched alkyl group having 2-20 carbon atoms capable of including one or at least two non-neighboring methylene groups which can be replaced with —O—, —S—, —C(O)—, —C(O)—O—, —O—C(O)—, —CH═CH— or —C≡C— and capable of including hydrogen atom which can be replaced with fluorine atom.
摘要翻译： 一种发光装置，包括一对电极和设置在其间的有机化合物层。 该层含有由下式（1）表示的金属配位化合物：其中M为Ir，Rh或Pd; n为2或3; 而X 1至X 8独立地为氢原子或选自卤素原子的取代基; 硝基; 三氟甲基; 具有三个直链或支链烷基的三烷基甲硅烷基，各自独立地具有1-8个碳原子; 和具有2-20个碳原子的直链或支链烷基能够包含一个或至少两个不相邻的亚甲基，可以被-O - ， - S - ， - C（O） - ， - C ）-O-，-OC（O） - ， - CH = CH-或-C = C-，并且能够包括可被氟原子替代的氢原子。
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公开(公告)号：US08920943B2
公开(公告)日：2014-12-30
申请号：US12371104
申请日：2009-02-13
申请人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
发明人： Jun Kamatani , Shinjiro Okada , Akira Tsuboyama , Takao Takiguchi , Seishi Miura , Koji Noguchi , Takashi Moriyama , Satoshi Igawa , Manabu Furugori
CPC分类号： H01L51/0085 , C07F15/004 , C07F15/0066 , C07F15/008 , C07F15/0093 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1033 , C09K2211/1037 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1092 , C09K2211/185 , H01L27/3244 , H01L51/005 , H01L51/0059 , H01L51/0081 , H01L51/0084 , H01L51/5012 , H01L51/5016 , H01L51/5234 , H05B33/14 , Y10S428/917
摘要： A metal coordination compound represented by the formula: An organic luminescence device including an anode, a cathode, and an organic layer, which contains the metal coordination compound, disposed between the anode and the cathode.
摘要翻译： 由下式表示的金属配位化合物：设置在阳极和阴极之间的包含阳极，阴极和有机层的含有金属配位化合物的有机发光器件。
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