摘要:
The invention concerns a magnet configuration comprising a superconducting magnet coil (1) within which a gradient system is to be switched. All low temperature oscillation systems (R1) with a temperature T1 10K within the magnet coil (1) has worse electrical conducting properties and has a considerably different mechanical resonance frequency (separation approximately 500 Hz or more) than at least one of the low temperature oscillation systems (R1). This reduces the undesired heating power supplied to the low temperature oscillation systems due to mechanical oscillations and induced eddy currents.
摘要:
A cryostat (1) with a magnet coil system including superconductors for the production of a magnet field B0 in a measuring volume (3) within a room temperature bore (2) of the cryostat has a plurality of radially nested solenoid-shaped coil sections (4, 5, 6) which surround the room temperature bore and which are electrically connected in series, at least one of which being an LTS section (5, 6) with a conventional low temperature superconductor (LTS) and at least one of which being an HTS section (4) including a high temperature superconductor (HTS), wherein the LTS section (5, 6) is located in a helium tank (9) of the cryostat (1) along with liquid helium at a helium temperature TL. The apparatus is characterized in that the HTS section (4) is disposed radially within the LTS section (5, 6) in a vacuum portion of the cryostat and is separated from the LTS section (5, 6) by the helium tank (9) wall (9a) facing the room temperature bore. The HTS coil section can be reliably used in the cryostat over a long period of time (FIG. 1a).
摘要:
A magnetic resonance apparatus comprising a superconducting magnet coil disposed in a cryostat, and a refrigerator for cooling same comprising a compressor (1) for compressing a working gas, and a high-pressure line (2) and a low-pressure line (3) disposed between the compressor (1) and a control valve (5), which periodically connects the high-pressure line (2) and the low-pressure line (3) to at least one connecting line (6) between the control valve (5) and a cold head (4) of the refrigerator, thereby producing pressure pulses through the switched working gas, wherein the control valve (5) and/or connecting line (6) and cold head (4) components are rigidly mechanically coupled to the cryostat, is characterized in that at least one of the above-mentioned lines (2, 3, 6) is branched on the compressor side upstream of the rigidly coupled components, and is symmetrically joined at one of the coupled components in such a manner that the pressure pulses through the working gas are vectorially compensated for at the component where the branched line is joined, thereby minimizing vibrations of the cryostat. The inventive magnetic resonance apparatus greatly reduces transmission of oscillations to the magnet coil and thereby the number and strength of artefacts in the spectra or images acquired with this magnetic resonance apparatus, to ensure high-quality magnetic resonance recordings.
摘要:
A MAS (magic angle spinning) NMR (nuclear magnetic resonance) apparatus, with automatic sample supply by a supply unit (45), is characterized in that an automatic preparation station (44) for samples is provided, with a rotor storage (49) having several rotors (1) for receiving sample material (53) soaked with NMR solution (55), a cap storage (48) with several caps (3), each cap (3) being suited for closing a rotor (1), wherein each cap (3) has a central axial bore (4), several movable pins (5), each being insertable into the central axial bore (4) of a cap (3) to close the bore (4) in the inserted state, a cap handling unit (46b) which can grip a cap (3) from the cap storage (48), move it, and dispose it onto a rotor (1), a plunger (61) for inserting a pin (5) into the bore (4) of the cap (3), and a suctioning device (62) for suctioning excess NMR solution (55) that escapes from the bore (4). The apparatus provides simple and automatic preparation of sample units, in particular, closure of rotors with caps.
摘要:
An apparatus for analyzing a measuring substance which is dissolved in a solvent, comprising a conduit (4) for transporting the dissolved measuring substance from a feed means (3) to a measuring location (12), wherein the feed means (3) is designed to optionally feed a solvent or dissolved measuring substance into the conduit (4), is characterized in that the conduit (4) is designed, at least partially, as a polycapillary area (9) which has N parallel connected capillaries (21a, 21b, 21c; 62a, 62b), such that the individual capillaries (21a, 21b, 21c; 62a, 62b) have identical flow times from the feed means (3) to the measuring location (12) and wherein N≧2. The apparatus improves the signal-to-noise ratio of the analysis.
摘要:
A superconducting magnet configuration with a magnet coil (1) of inductance L which is disposed in a cryostat (7) at a cryogenic temperature, for generating a temporally stable magnetic field, in a working volume, which is suitable for NMR measurements, and with current feed lines to an external current source (3) via which a current of a current strength IPS can be supplied, wherein, at a cryogenic temperature, the magnet coil (1) can be exclusively short-circuited via a switch (5), is characterized in that the switch (5) is normally conducting and comprises a mechanically operable bridge (6) with an ohmic resistance R1 which can be predetermined. The inventive magnet configuration ensures straightforward stable permanent operation via a mains supply even at high currents (>1000A) and also effective discharge of the energy released during a quench.
摘要:
The invention concerns a superconducting high-field magnet system (1) for a high-resolution magnetic resonance spectrometer, comprising a magnet coil (4) which is superconductingly short-circuited during operation, and generates a homogeneous temporally stable magnetic field during operation that meets the requirements for taking a high-resolution magnetic resonance spectrum. The magnet coil (4) comprises an LTS partial coil (4b, 4c) and an HTS partial coil (4a, 4d). The LTS partial coil (4b, 4c) can be separately short-circuited in a pure LTS circuit (14b) via an LTS switch (15b), and the HTS partial coil (4a, 4d) can be separately short-circuited in a pure HTS circuit (14) via an HTS switch (15a) and both partial coils (4a, 4d; 4b, 4c) are connected via an LTS-HTS joint (20) and are charged by the same power supply.
摘要:
A probe head for nuclear magnetic resonance measurements in an area of a surface of a measuring object is disclosed. The probe head comprises first means for generating a static magnetic field extending at least partially parallel to the surface, second means for generating a radio frequency magnetic field having components extending perpendicular to the surface, and third means for amplifying a radio frequency magnetic field effective within the measuring object. The third means are configured as an aperture and are located between the second means and the surface.
摘要:
An apparatus for determining a quantitative property of a sample substance by means of magnetic resonance is disclosed. The apparatus comprises a conveyor for conveying sample containers containing the sample substance through a measuring station. The measuring station comprises a magnet system for generating a constant magnetic field of high homogeneity. The measuring station, further, comprises a probe head adapted for letting sample containers be conveyed therethrough and for generating a high frequency magnetic field. A magnetic resonance measuring unit determines the quantitative property of the sample substance contained in the probe head. The probe head excites and detects, resp., the magnetic resonance essentially only within that section of the sample container which contains the sample substance. The probe head comprises a split-ring resonator which, as seen in a conveying direction of the conveyor, has a passage cross-section for letting run the sample containers therethrough. The high frequency magnetic field is generated essentially only in an area of the passage cross-section through which the sample containers run during conveying.
摘要:
A superconducting magnet coil configuration has at least one section containing a superconducting strip conductor which is wound in several layers like a solenoid in a cylindrical winding chamber (1) between two end flanges (2, 3), characterized in that the radially innermost layers of the section consist of metallic low-temperature superconductors (LTS) (LTS layers (8)) and radially adjacent layers of the section are formed from high-temperature superconductor (HTS) material (HTS layers (9)). The invention proposes a magnet coil configuration using HTS material which has a notch structure for correcting inhomogeneities and homogenizing a compact high-field magnet, wherein the mechanical load on the HTS strip conductor is minimized.