DETERMINATION OF PORE SIZE IN POROUS MATERIALS BY EVAPORATIVE MASS LOSS
    3.
    发明申请
    DETERMINATION OF PORE SIZE IN POROUS MATERIALS BY EVAPORATIVE MASS LOSS 有权
    通过蒸发质量损失确定多孔材料中的孔尺寸

    公开(公告)号:US20130042670A1

    公开(公告)日:2013-02-21

    申请号:US13695251

    申请日:2011-05-02

    IPC分类号: G01N15/08

    摘要: A method for determination of pore-size distribution in a porous material called evapo porometry (EP) is capable of determining pore sizes from approximately the nanometer scale up to the micron scale. EP determines the pore size based on the evaporative mass loss at constant temperature from porous materials that have been pre-saturated with either a wetting or non-wetting volatile liquid. The saturated porous material is placed in an appropriate test cell on a conventional microbalance to measure liquid mass loss at a constant temperature as a function of time. The mass-loss rate is then related to the pore-size distribution. The microbalance permits measuring the mass as a function of time. The slope of the mass versus time curve is the evaporation rate. The evaporation rate is related to the vapor pressure at the interface between the liquid in the porous material and the ambient gas phase. The vapor pressure in turn is related to the pore diameter.

    摘要翻译: 用于测定称为蒸发孔隙率(EP)的多孔材料中的孔径分布的方法能够确定从大约纳米级至微米级的孔径。 EP基于已经用润湿或非润湿挥发性液体预饱和的多孔材料在恒定温度下基于蒸发质量损失来确定孔径。 将饱和多孔材料放置在常规微量天平上的合适的测试池中,以在恒定温度下测量作为时间的函数的液体质量损失。 然后质量损失率与孔径分布有关。 微量天平允许测量质量作为时间的函数。 质量对时间曲线的斜率是蒸发速率。 蒸发速率与多孔材料中的液体与环境气相之间的界面处的蒸气压有关。 蒸气压又与孔径有关。