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    Ionic conducting gels, preparation method thereof and use of same
    1.
    发明申请
    Ionic conducting gels, preparation method thereof and use of same 有权
    离子导电凝胶及其制备方法及用途

    公开(公告)号：US20070007137A1

    公开(公告)日：2007-01-11

    申请号：US10562680

    申请日：2004-07-02

    申请人： Andre Vioux ,  Jean Le Bideau ,  Marie-Alexandra Neouze ,  Fabrics Leroux

    发明人： Andre Vioux ,  Jean Le Bideau ,  Marie-Alexandra Neouze ,  Fabrics Leroux

    IPC分类号： C07D233/14 ,  C07D213/20 ,  C07K1/26

    CPC分类号： H01B1/122 ,  C08K5/3432 ,  C08K5/3445 ,  C08L83/02

    摘要： A method of preparing an ionic conducting gel in solid form, known as ionogel. The method includes a step of mixing an ionic liquid with at least one molecular precursor containing at least one hydrolyzable group, if necessary in the presence of an acid, such as a carboxylic acid. The mixture is subsequently left to stand for one or more days until a gel is formed by polycondensation of the molecular precursor(s). The gel contains the aforementioned ionic liquid and can be set, in particular in transparent monolithic solid form.

    摘要翻译： 制备固体形式的离子导电凝胶的方法，称为离子凝胶。 该方法包括将离子液体与至少一种含有至少一个可水解基团的分子前体混合的步骤，如有必要，在酸例如羧酸存在下。 然后将混合物静置一天或多天，直至通过分子前体的缩聚形成凝胶。 凝胶含有上述离子液体，特别是以透明的整体固体形式设置。

    Process for the preparation of optionally alkoxylated polyorganosiloxane resin by non-hydrolytic condensation
    2.
    发明授权
    Process for the preparation of optionally alkoxylated polyorganosiloxane resin by non-hydrolytic condensation 失效
    通过非水解缩合制备任选烷氧基化聚有机硅氧烷树脂的方法

    公开(公告)号：US5767216A

    公开(公告)日：1998-06-16

    申请号：US594398

    申请日：1996-01-31

    申请人： Jean-Marc Frances ,  Hubert Pierre Mutin ,  Laurence Bourget ,  Dominique LeClercq ,  Andre Vioux

    发明人： Jean-Marc Frances ,  Hubert Pierre Mutin ,  Laurence Bourget ,  Dominique LeClercq ,  Andre Vioux

    IPC分类号： C08G77/06 ,  C08G77/08 ,  C08G77/18 ,  C08G77/22 ,  C08G77/48 ,  C08G77/60

    CPC分类号： C08G77/18 ,  C08G77/06 ,  C08G77/08

    摘要： The present invention relates to the synthesis of optionally alkoxylated polyorganosiloxane (POS) resins by non-hydrolytic condensation. The object is to provide a process which offers the possibility of controlling the crosslinking. This object, inter alia, is achieved by the process according to the invention, which makes provision for carrying out a non-hydrolytic condensation reaction between alkoxysilyl units (Mo1) and halogenosilyl units (Mo2), both of which are carried by identical or different silanes, in the presence of a catalyst of the Lewis acid type, said condensation reaction generating essentially .tbd.Si--O--Si.tbd. linkages and coproducts XR (X=halogen). In this process, the target POS comprise siloxy units D, T and/or Q, or perhaps M, the catalyst is selected from metal compounds or mixtures thereof based on at least one metal belonging to group IIIB, IVB or VB of the periodic table, and the reaction temperature and the initial ratio OR/X are adjusted so that condensation takes place substantially exclusively between the units Mo1 and Mo2, with extreme minimization of secondary condensation between two alkoxy units OR to give the by-product R.sub.2 O.

    摘要翻译： 本发明涉及通过非水解缩合合成任选的烷氧基化聚有机硅氧烷（POS）树脂。 目的是提供一种提供控制交联的可能性的方法。 该目的尤其通过根据本发明的方法实现，其提供了在烷氧基甲硅烷基单元（Mo1）和卤代甲硅烷基单元（Mo2）之间进行非水解缩合反应，两者均由相同或不同的载体 硅烷，在路易斯酸型催化剂存在下，所述缩合反应产生基本上为3BOND Si-O-Si 3BOND键和副产物XR（X =卤素）。 在该方法中，目标POS包含基于至少一种属于元素周期表IIIB，IVB或VB族金属的金属化合物或其混合物的甲硅烷氧基单元D，T和/或Q，或者也许M ，并且调节反应温度和初始比例OR / X，使得冷凝仅在单元Mo1和Mo2之间发生，极端地最小化两个烷氧基单元之间的二次缩合或得到副产物R2O。