公开(公告)号：US20100305342A1

公开(公告)日：2010-12-02

申请号：US12850016

申请日：2010-08-04

申请人： Alfred Wong ,  Hugh Sven Oscar Norman ,  Angus Kirke MacMillan

发明人： Alfred Wong ,  Hugh Sven Oscar Norman ,  Angus Kirke MacMillan

IPC分类号： C07J9/00

CPC分类号： C07J9/00 ,  C07G1/00 ,  C11B13/005 ,  Y02W30/74

摘要： A method of preparing phytosterols from tall oil pitch containing steryl esters comprises the steps of converting the steryl esters to free phytosterols while in the pitch to produce a modified pitch containing the free phytosterols; removing light ends from the modified pitch by evaporation to produce a bottom fraction containing the free phytosterols; evaporating the bottom fraction to produce a light phase distillate containing the free phytosterols; dissolving the light phase distillate in a solvent comprising an alcohol to produce a solution containing the free phytosterols; cooling the solution to produce a slurry with the free phytosterols crystallized in the slurry; and, washing and filtering the slurry to isolate the crystallized phytosterols.

摘要翻译： 从含有甾醇酯的妥尔油沥青制备植物甾醇的方法包括以下步骤：在沥青中将甾酯转化为游离植物甾醇，以产生含有游离植物甾醇的改性沥青; 通过蒸发从改性沥青中除去轻馏分以产生含有游离植物甾醇的底部馏分; 蒸发底部馏分以产生含有游离植物甾醇的轻质馏出物; 将轻相馏出物溶解在包含醇的溶剂中以产生含有游离植物甾醇的溶液; 冷却溶液以产生具有在浆液中结晶的游离植物甾醇的浆料; 并洗涤并过滤浆料以分离出结晶的植物甾醇。

公开(公告)号：US20090131697A1

公开(公告)日：2009-05-21

申请号：US12233392

申请日：2008-09-18

申请人： Alfred Wong ,  Hugh Sven Oscar Norman ,  Angus Kirke MacMillan

发明人： Alfred Wong ,  Hugh Sven Oscar Norman ,  Angus Kirke MacMillan

IPC分类号： C07J9/00

CPC分类号： C07J9/00 ,  C07G1/00 ,  C11B13/005 ,  Y02W30/74

摘要： A method of preparing phytosterols from tall oil pitch containing steryl esters comprises the steps of converting the steryl esters to free phytosterols while in the pitch to produce a modified pitch containing the free phytosterols; removing light ends from the modified pitch by evaporation to produce a bottom fraction containing the free phytosterols; evaporating the bottom fraction to produce a light phase distillate containing the free phytosterols; dissolving the light phase distillate in a solvent comprising an alcohol to produce a solution containing the free phytosterols; cooling the solution to produce a slurry with the free phytosterols crystallized in the slurry; and, washing and filtering the slurry to isolate the crystallized phytosterols.

摘要翻译： 从含有甾醇酯的妥尔油沥青制备植物甾醇的方法包括以下步骤：在沥青中将甾酯转化为游离植物甾醇，以产生含有游离植物甾醇的改性沥青; 通过蒸发从改性沥青中除去轻馏分以产生含有游离植物甾醇的底部馏分; 蒸发底部馏分以产生含有游离植物甾醇的轻质馏出物; 将轻相馏出物溶解在包含醇的溶剂中以产生含有游离植物甾醇的溶液; 冷却溶液以产生具有在浆液中结晶的游离植物甾醇的浆料; 并洗涤并过滤浆料以分离出结晶的植物甾醇。

公开(公告)号：US08338564B2

公开(公告)日：2012-12-25

申请号：US12850016

申请日：2010-08-04

申请人： Alfred Wong ,  Hugh Sven Oscar Norman ,  Angus Kirke MacMillan

发明人： Alfred Wong ,  Hugh Sven Oscar Norman ,  Angus Kirke MacMillan

IPC分类号： C11B13/00 ,  C11B7/00 ,  A61K31/56

CPC分类号： C07J9/00 ,  C07G1/00 ,  C11B13/005 ,  Y02W30/74

摘要： A method of preparing phytosterols from tall oil pitch containing steryl esters comprises the steps of converting the steryl esters to free phytosterols while in the pitch to produce a modified pitch containing the free phytosterols; removing light ends from the modified pitch by evaporation to produce a bottom fraction containing the free phytosterols; evaporating the bottom fraction to produce a light phase distillate containing the free phytosterols; dissolving the light phase distillate in a solvent comprising an alcohol to produce a solution containing the free phytosterols; cooling the solution to produce a slurry with the free phytosterols crystallized in the slurry; and, washing and filtering the slurry to isolate the crystallized phytosterols.

摘要翻译： 从含有甾醇酯的妥尔油沥青制备植物甾醇的方法包括以下步骤：在沥青中将甾酯转化为游离植物甾醇，以产生含有游离植物甾醇的改性沥青; 通过蒸发从改性沥青中除去轻馏分以产生含有游离植物甾醇的底部馏分; 蒸发底部馏分以产生含有游离植物甾醇的轻质馏出物; 将轻相馏出物溶解在包含醇的溶剂中以产生含有游离植物甾醇的溶液; 冷却溶液以产生具有在浆液中结晶的游离植物甾醇的浆料; 并洗涤并过滤浆料以分离出结晶的植物甾醇。