摘要:
A method of operating a high-resolution NMR spectrometer comprising a DDS generator containing an NCOL for generating an LO frequency, wherein the frequency of the NCOL is defined by inputting a numerical value Z, is characterized in that this numerical value Z may assume only values which satisfy the equation Z=n·N/m, wherein Z, n, N, and m are integer and positive numbers, N is a power of 2 with a positive integer exponent, wherein said exponent represents the maximum number of bits during the calculation process, m is approximately 2·fs/&Dgr;B, n approximately m·fout/fs and m additionally a common integer divisor of n·N and fs is the clock frequency of the NCOL, &Dgr;B is the desired bandwidth with high spectral purity and fout is the output frequency of the NCOL. This method allows the use of a DDS generator even in the case where very high spectral purity is required, wherein in particular quantization noise is largely eliminated over the frequency range relevant for NMR measurements.
摘要:
A device has a first control loop (28) with which a frequency RF of an RF generator is synchronized with a resonance frequency F0 of an NMR line. A phase shifter (22) is provided to rotate the radio frequency phase of the NMR receiver system in the first control loop. The phase shifter is controlled by a second control loop (27) whose input signal comes from a signal extraction stage.
摘要:
A device that comprises an RF generator (29), an NMR transmission (20) and reception system (21) and a first control loop (28), with which the frequency fRF of the RF generator is synchronized with the resonance frequency f0 of an NMR line, wherein, from the signal of the RF generator, a train of excitation pulses (EX) of the repetition frequency fm is generated, with which nuclear spins of a certain resonance frequency of an associated NMR line are excited quasi-continuously (CW) and, in the times between the excitation pulses, the NMR signal is received (AQ), wherein the period time 1/fm is chosen to be much smaller than the relaxation time of the NMR line, preferably shorter than 1/10 of the relaxation time, and the NMR signal UD mixed down into the low-frequency range is used, with the help of the first control loop, to closed-loop-control the value of the transmission frequency (=frequency lock) or the value of the B0 field (=field lock) in such a way that the frequency and phase of the RF generator and the NMR line match as precisely as possible, characterized in that a phase shifter (22) that rotates the radio-frequency phase of the NMR transmission and reception system in the first control loop by the value Δφ is controlled by a second control loop (27) whose input signal comes from a signal extraction stage (25, 26) that extracts the saw-tooth AC component of the signal UD and maintains this input signal at zero by closed-loop control. In this way, the influence of the RF phase on the synchronization process can be taken into consideration to improve the precision with which the resonance frequency of an NMR line is synchronized.
摘要:
A magnetic resonance (MR) detection configuration comprising at least one RF resonant circuit with an inductance, a preamplifier module and an RF receiver, wherein a reactive transformation circuit is connected between a high-impedance point of the inductance and a low-impedance connecting point of the RF resonant circuit, which acts as an impedance transformer and wherein the low-impedance connecting point is connected to the preamplifier module via an RF line having a characteristic impedance, is characterized in that at least one passive damping impedance is provided in the preamplifier module downstream of the RF line, wherein the passive damping impedance can be connected to the resonant circuit by a switching means during a damping and/or transmitting process, and wherein the respective amount of the complex reflection factor of passive damping impedance relative to the characteristic impedance of the RF line exceeds a value of 0.5. This presents an MR detection configuration with an extensive damping concept, wherein all three processes (transmitting, damping and receiving processes) are optimized.
摘要:
A magnetic resonance (MR) detection configuration comprising at least one RF resonant circuit (1) with an inductance (L), a preamplifier module (2) and an RF receiver (7), wherein a reactive transformation circuit is connected between a high-impedance point (M) of the inductance (L) and a low-impedance connecting point (A) of the RF resonant circuit (1), which acts as an impedance transformer and wherein the low-impedance connecting point (A) is connected to the preamplifier module (2) via an RF line (15) having a characteristic impedance RW), is characterized in that at least one passive damping impedance (ZDV, ZSV, ZDV′, ZSV′) is provided in the preamplifier module (2) downstream of the RF line (15), wherein the passive damping impedance (ZDV, ZSV, ZDV′, ZSV′) can be connected to the resonant circuit (1) by a switching means during a damping and/or transmitting process, and wherein the respective amount of the complex reflection factor of passive damping impedance (ZDV, ZSV, ZDV′, ZSV′) relative to the characteristic impedance RW) of the RF line (15) exceeds a value of 0.5. This presents an MR detection configuration with an extensive damping concept, wherein all three processes (transmitting, damping and receiving processes) are optimized.
摘要翻译:一种包括具有电感(L)的至少一个RF谐振电路(1),前置放大器模块(2)和RF接收器(7))的磁共振(MR)检测配置,其中, 作为阻抗变换器的RF谐振电路(1)的电感(L)的阻抗点(M)和低阻抗连接点(A),其中低阻抗连接点(A)连接到 前置放大器模块(2)经由具有特征阻抗R W W的RF线路(15))的特征在于,至少一个被动阻尼阻抗(Z Z DV,Z 在RF线路(15)的下游的前置放大器模块(2)中提供有SV SV,Z SV,Z SV, 可以连接被动阻尼阻抗(Z DV DV>,>>>,,Z Z Z,,,,,,connected connected connected connected connected connected connected connected connected connected connected>>>>>>>>>>>>>>>>> 在阻尼和/或发送过程中通过开关装置耦合到谐振电路(1) ,并且其中无源阻尼阻抗(Z N DV,Z SV),Z V DV',Z W>的相位> SV'<>>超过0.5的值。 这提出了具有广泛的阻尼概念的MR检测配置,其中所有三个过程(发射,阻尼和接收过程)被优化。
摘要:
In a method for compensation of time variant field disturbances in magnetic fields of electromagnets with high field-homogeneity, in particular in sample volumes of superconducting electromagnets for measurements of magnetic resonance, the dispersion signal u.sub.x of the nuclear signal of a reference substance is acquired and taken into consideration for compensation by generation of a current dependent on the dispersion signal in a field correction coil of the electromagnet. The method is characterized in that the absorption signal u.sub.y of the reference substance is additionally acquired and that the compensation is carried out in dependence on the quantity u.sub.x /u.sub.y and/or (1/u.sub.y)(du.sub.x /dt). These are substantially independent of many influencing quantities.