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公开(公告)号：US06899782B1
公开(公告)日：2005-05-31
申请号：US10031963
申请日：1999-09-07
CPC分类号： B60C11/00 , B29C47/0004 , B29C47/0021 , B29C47/12 , B29D2030/665 , B29K2021/00 , B29K2105/06 , B29K2105/14 , B29L2030/002 , Y10T152/10513
摘要： A method and apparatus for continuously processing fiber into an elastomeric component uses an expanding die (11, 11a) for orienting fibers in other than the processing direction of the extrusion. In one embodiment, an injection mold (50) is used with the expanding die (11), and in another embodiment, an extruder (30) is used with expanding die (11a). Processing parameters may be alteredto control the direction of orientation of fibers (20) in the elastomer component. Orientation of fibers (20) in an extrudate (17) is dependent on the processing speed viscosity of the elastomer, pressure of extrusion, the length l1 and l2 and height h1 and h2 of gate (12) and expansion cavity (14), respectively, of the expansion die (11, 11a).
摘要翻译： 用于将纤维连续地加工成弹性体组分的方法和设备使用扩展模具（11,11a）来定向不同于挤出的加工方向的纤维。 在一个实施例中，注塑模具（50）与膨胀模具（11）一起使用，在另一个实施例中，挤出机（30）与膨胀模具（11a）一起使用。 可以改变加工参数以控制弹性体组分中的纤维（20）的取向方向。 挤出物（17）中的纤维（20）的取向取决于弹性体的加工速度粘度，挤出压力，长度l 1和1 2 2和高度 分别为膨胀模具（11,11a）的浇口（12）和膨胀腔（14）的h 1/2和2 H 2。
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公开(公告)号：US6106752A
公开(公告)日：2000-08-22
申请号：US194417
申请日：1998-11-28
CPC分类号： B29C45/0005
摘要： A method for molding short fiber/rubber composite articles having enhanced mechanical properties by aligning short reinforcing fibers during an injection molding process. The method comprises injecting a molding mixture through an injection gate arranged in a predetermined relationship to the molding cavity. The injection gate has a relatively small thickness in comparison to the thickness of the molding cavity. The fibers are associated with a first direction, generally parallel to the flow of the molding mixture as the molding mixture moves through the gate. As the molding mixture passes through the gate and into the cavity, the fiber direction is altered as the molding material fills the cavity.
摘要翻译： PCT No.PCT / US96 / 15237 Sec。 371日期：1998年11月27日 102（e）1998年11月27日PCT PCT 1996年9月24日PCT公布。 公开号WO98 / 13185 日期：1998年4月2日在注射成型工序中，通过对准短增强纤维，对具有增强的机械性能的短纤维/橡胶复合制品进行成型。 该方法包括通过以预定关系布置成模腔的注入口注入模制混合物。 与模腔的厚度相比，注射门具有相对较小的厚度。 当模制混合物通过浇口时，纤维与第一方向相关联，大致平行于模制混合物的流动。 当模制混合物通过浇口并进入空腔时，纤维方向随着模制材料填充空腔而改变。
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公开(公告)号：US06825302B1
公开(公告)日：2004-11-30
申请号：US10648180
申请日：2003-08-26
IPC分类号： C08F414
CPC分类号： C08F240/00 , C08F210/14
摘要： This invention is based upon the unexpected discovery that the reactivity of the most important monomers commonly used in synthesizing tackifier resins with aluminum halide catalysts can be enhanced by conducting the polymerization in the presence of an allylic halide. For instance, the conversions of 2-methyl-2-butene, cis-piperylene, and cyclopentene that are attained in polymerizations that are catalyzed with aluminum halide catalysts are increased by conducting the polymerization in the presence of an allylic halide, such as allyl chloride. Increased monomer conversion is of great commercial importance because it leads to an increased level of efficiency and reactor capacity. The present invention more specifically discloses a process for synthesizing a resin having characteristics that make it particularly useful as a tackifier resin, said process comprising the polymerization of an unsaturated hydrocarbon monomer mixture in the presence of aluminum halide and an allylic halide, wherein the unsaturated hydrocarbon monomer mixture is comprised of unsaturated hyrdocarbon monomers containing from about 4 to about 18 carbon atoms, and wherein said process is conducted in the absence of tantalum compounds. The subject invention further reveals a process for synthesizing a resin having characteristics that make it particularly useful as a tackifier resin, said process comprising the polymerization of an unsaturated hydrocarbon monomer mixture in the presence of aluminum halide and an allylic halide, wherein the unsaturated hydrocarbon monomer mixture is comprised of monomers including but not limited to 2-methyl-2-butene, cis-piperylene, trans-piperylene, cyclopentene, and additional unsaturated hyrdocarbon monomers containing from about 4 to about 18 carbon atoms, wherein said process is conducted in the absence of tantalum compounds.
摘要翻译： 本发明基于意想不到的发现，通过在烯丙基卤化物存在下进行聚合可以提高通常用于合成增粘树脂与卤化铝催化剂的最重要的单体的反应性。 例如，在用卤化铝催化剂催化的聚合中获得的2-甲基-2-丁烯，顺 - 戊间二烯和环戊烯的转化率通过在烯丙基卤化物如烯丙基氯的存在下进行聚合而增加 。 增加的单体转化率具有很大的商业重要性，因为它导致提高的效率和反应器容量水平。 本发明更具体地公开了一种具有使其特别用作增粘树脂的特性的树脂的方法，所述方法包括在卤化铝和烯丙基卤的存在下聚合不饱和烃单体混合物，其中不饱和烃 单体混合物由含有约4至约18个碳原子的不饱和羧基碳单体组成，并且其中所述方法在不存在钽化合物的情况下进行。 本发明还揭示了一种具有使其特别用作增粘树脂的特性的树脂的方法，所述方法包括在卤化铝和烯丙基卤化物存在下聚合不饱和烃单体混合物，其中不饱和烃单体 混合物由包括但不限于2-甲基-2-丁烯，顺式 - 戊间二烯，反式 - 戊间二烯，环戊烯和含有约4至约18个碳原子的其它不饱和羧基碳单体组成的单体组成，其中所述方法在 没有钽化合物。
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公开(公告)号：US06387313B1
公开(公告)日：2002-05-14
申请号：US09461907
申请日：1999-12-15
IPC分类号： B29C4500
CPC分类号： B29C45/0005 , B29C45/2701 , B29C2045/0006 , B29K2021/00
摘要： A combination rubber injection gate system (24) and method of injection molding rubber to produce desired flow patterns in the rubber is disclosed. The combination gate (24) directs rubber through a first region (26) to flow at cross angles (38, 40) through the injection gate (24), relative to the direction of flow of the rubber (22) through the injection gate (24). The rubber (22) is then directed through an adjacent region (28) to flow through the injection gate (24) at a direction parallel to the direction of flow of the rubber (22) through the entire injection gate (24). The combination gate (24) yields a highly mixed and uniform flow of rubber (22) that is particularly useful when injection molding fiber-loaded rubber where it is desired to orient the fibers in a particular direction.
摘要翻译： 公开了一种组合橡胶注射门系统（24）和注射橡胶的方法以在橡胶中产生所需的流动模式。 组合门24引导橡胶穿过第一区域26相对于橡胶（22）通过喷射门（22）的流动方向通过喷射浇口（24）以交叉角（38,40）流动 24）。 然后，橡胶（22）被引导通过相邻区域（28），以通过整个喷射门（24）沿与橡胶（22）的流动方向平行的方向流过喷射门（24）。 组合门（24）产生高度混合且均匀的橡胶流动（22），当注射成型纤维负载的橡胶时，其需要在特定方向上定向纤维时特别有用。
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