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公开(公告)号：US20130114369A1
公开(公告)日：2013-05-09
申请号：US13807009
申请日：2011-06-23
申请人： Fumihiko Ishiyama , Takeshi Hizawa , Kiyoo Kamei
发明人： Fumihiko Ishiyama , Takeshi Hizawa , Kiyoo Kamei
CPC分类号： B01F5/0256 , B01F13/0059 , B01F15/065 , B81B1/00
摘要： Disclosed is a micro mixer which includes a mixing plate (14) with a first channel-forming section and a second channel-forming section. The first channel-forming section has a first channel formed for a first fluid to flow therethrough, while the second channel-forming section has a second channel formed for a second fluid to flow therethrough. Between the first channel-forming section and the second channel-forming section, there is provided a combined channel in which the first fluid and the second fluid merge with each other. The outlet of the first channel and the outlet of the second channel are opposed to each other with the combined channel disposed therebetween. The position of the outlet of the first channel facing the center axis of the combined channel is included in or the same as the position of the outlet of the second channel facing the center axis.
摘要翻译： 公开了一种微型混合器，其包括具有第一通道形成部分和第二通道形成部分的混合板（14）。 第一通道形成部分具有形成为用于第一流体流过其中的第一通道，而第二通道形成部分具有形成为用于使第二流体流过其中的第二通道。 在第一通道形成部分和第二通道形成部分之间设置有第一流体和第二流体彼此合并的组合通道。 第一通道的出口和第二通道的出口彼此相对，其中组合的通道设置在它们之间。 面向组合通道的中心轴的第一通道的出口的位置包括在与第二通道的出口相对于中心轴线的位置相同的位置上。
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公开(公告)号：US20110087041A1
公开(公告)日：2011-04-14
申请号：US12922207
申请日：2009-03-12
IPC分类号： C07C269/02
CPC分类号： C07C269/02 , C07C271/28
摘要： An object of the present invention is to provide a process for producing a urethane (meth)acrylate safely with good productivity, and for achieving the object, the invention provides a process for continuously producing a urethane (meth)acrylate, containing causing a mixed liquid of a compound (A) having a hydroxyl group and a (meth)acryloyl group and a compound (B) having an isocyanate group to pass continuously and densely through a tubular microchannel formed in a heat-conducting reaction device, and reacting the hydroxyl group of the compound (A) with the isocyanate group of the compound (B), in which the tubular microchannel in the reaction device has a space size making a fluid cross-sectional area, through which the mixed liquid passes densely, of from 0.1 to 4.0 mm2, and the process contains heating the heat-conducting reaction device to a temperature of from 100 to 250° C., reacting the mixed liquid to provide a Reynolds number of a reaction liquid passing through the tubular microchannel in a range of from 0.2 to 300, and after completing reaction, cooling continuously a reaction product discharged from the heat-conducting reaction device.
摘要翻译： 本发明的目的在于提供一种以高生产率安全地制备氨基甲酸酯（甲基）丙烯酸酯的方法，为了达到上述目的，本发明提供一种连续生产聚氨酯（甲基）丙烯酸酯的方法， 具有羟基和（甲基）丙烯酰基的化合物（A）和具有异氰酸酯基的化合物（B）连续密集地通过形成在导热反应装置中的管状微通道，并使羟基 化合物（A）与化合物（B）的异氰酸酯基的化合物（B）的反应，其中反应装置中的管状微通道具有使混合液体密集通过的流体截面的空间尺寸为0.1〜 4.0mm 2，并且该方法包括将导热反应装置加热至100至250℃的温度，使混合液体反应以提供通过管状物的反应液的雷诺数 微通道在0.2至300的范围内，并且在完成反应之后，连续冷却从导热反应装置排出的反应产物。
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公开(公告)号：US08759551B2
公开(公告)日：2014-06-24
申请号：US12922193
申请日：2009-03-12
IPC分类号： C07D303/04 , C07D301/02
CPC分类号： C07C269/02 , C07C271/28
摘要： The invention provides a process for continuously producing a urethane (meth)acrylate, containing causing a mixed liquid of a compound (A) having a hydroxyl group and a (meth) acryloyl group and a compound (B) having an isocyanate group to pass continuously and densely through a tubular microchannel formed in a heat-conducting reaction device, and reacting the hydroxyl group of the compound (A) with the isocyanate group of the compound (B).
摘要翻译： 本发明提供连续制造氨基甲酸酯（甲基）丙烯酸酯的方法，其中含有具有羟基和（甲基）丙烯酰基的化合物（A）和具有异氰酸酯基的化合物（B）的混合液体连续通过 并密集地通过在导热反应装置中形成的管状微通道，并使化合物（A）的羟基与化合物（B）的异氰酸酯基反应。
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公开(公告)号：US09073018B2
公开(公告)日：2015-07-07
申请号：US13807009
申请日：2011-06-23
申请人： Fumihiko Ishiyama , Takeshi Hizawa , Kiyoo Kamei
发明人： Fumihiko Ishiyama , Takeshi Hizawa , Kiyoo Kamei
CPC分类号： B01F5/0256 , B01F13/0059 , B01F15/065 , B81B1/00
摘要： Disclosed is a micro mixer which includes a mixing plate (14) with a first channel-forming section and a second channel-forming section. The first channel-forming section has a first channel formed for a first fluid to flow therethrough, while the second channel-forming section has a second channel formed for a second fluid to flow therethrough. Between the first channel-forming section and the second channel-forming section, there is provided a combined channel in which the first fluid and the second fluid merge with each other. The outlet of the first channel and the outlet of the second channel are opposed to each other with the combined channel disposed therebetween. The position of the outlet of the first channel facing the center axis of the combined channel is included in or the same as the position of the outlet of the second channel facing the center axis.
摘要翻译： 公开了一种微型混合器，其包括具有第一通道形成部分和第二通道形成部分的混合板（14）。 第一通道形成部分具有形成为用于第一流体流过其中的第一通道，而第二通道形成部分具有形成为用于使第二流体流过其中的第二通道。 在第一通道形成部分和第二通道形成部分之间设置有第一流体和第二流体彼此合并的组合通道。 第一通道的出口和第二通道的出口彼此相对，其中组合的通道设置在它们之间。 面向组合通道的中心轴的第一通道的出口的位置包括在与第二通道的出口相对于中心轴线的位置相同的位置上。
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公开(公告)号：US08148567B2
公开(公告)日：2012-04-03
申请号：US12922207
申请日：2009-03-12
IPC分类号： C07C269/00
CPC分类号： C07C269/02 , C07C271/28
摘要： An object of the present invention is to provide a process for producing a urethane (meth)acrylate safely with good productivity, and for achieving the object, the invention provides a process for continuously producing a urethane (meth)acrylate, containing causing a mixed liquid of a compound (A) having a hydroxyl group and a (meth)acryloyl group and a compound (B) having an isocyanate group to pass continuously and densely through a tubular microchannel formed in a heat-conducting reaction device, and reacting the hydroxyl group of the compound (A) with the isocyanate group of the compound (B), in which the tubular microchannel in the reaction device has a space size making a fluid cross-sectional area, through which the mixed liquid passes densely, of from 0.1 to 4.0 mm2, and the process contains heating the heat-conducting reaction device to a temperature of from 100 to 250° C., reacting the mixed liquid to provide a Reynolds number of a reaction liquid passing through the tubular microchannel in a range of from 0.2 to 300, and after completing reaction, cooling continuously a reaction product discharged from the heat-conducting reaction device.
摘要翻译： 本发明的目的在于提供一种以高生产率安全地制备氨基甲酸酯（甲基）丙烯酸酯的方法，为了达到上述目的，本发明提供一种连续生产聚氨酯（甲基）丙烯酸酯的方法， 具有羟基和（甲基）丙烯酰基的化合物（A）和具有异氰酸酯基的化合物（B）连续密集地通过形成在导热反应装置中的管状微通道，并使羟基 化合物（A）与化合物（B）的异氰酸酯基的化合物（B）的反应，其中反应装置中的管状微通道具有使混合液体密集通过的流体截面的空间尺寸为0.1〜 4.0mm 2，并且该方法包括将导热反应装置加热至100至250℃的温度，使混合液体反应以提供通过管状物的反应液的雷诺数 微通道在0.2至300的范围内，并且在完成反应之后，连续冷却从导热反应装置排出的反应产物。
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公开(公告)号：US20110071307A1
公开(公告)日：2011-03-24
申请号：US12922193
申请日：2009-03-12
IPC分类号： C07D303/16
CPC分类号： C07C269/02 , C07C271/28
摘要： An object of the present invention is to provide a process for producing an epoxy (meth)acrylate safely with good productivity, and the invention provides a process for continuously producing an epoxy (meth)acrylate, containing causing a mixed liquid of a compound (A) having a carboxyl group and a (meth)acryloyl group and a compound (B) having an epoxy group to pass continuously and densely through a tubular microchannel formed in a heat-conducting reaction device, and reacting the carboxyl group of the compound (A) with the epoxy group of the compound (B), in which the tubular microchannel in the reaction device has a space size making a fluid cross-sectional area, through which the mixed liquid passes densely, of from 0.1 to 4.0 mm2, and the process contains heating the heat-conducting reaction device to a temperature of from 150 to 260° C., reacting the mixed liquid to provide a Reynolds number of a reaction liquid passing through the tubular microchannel in a range of from 0.4 to 100, and after completing reaction, cooling continuously a reaction product discharged from the heat-conducting reaction device.
摘要翻译： 本发明的目的在于提供一种以高生产率安全地生产环氧（甲基）丙烯酸酯的方法，本发明提供一种连续制备环氧（甲基）丙烯酸酯的方法，该方法含有使化合物（A） ）具有羧基和（甲基）丙烯酰基的化合物（B）和具有环氧基的化合物（B）连续密集地通过形成在导热反应装置中的管状微通道，并使化合物（A ）与化合物（B）的环氧基的反应，其中反应装置中的管状微通道具有使混合液体密集通过的流体截面积为0.1〜4.0mm 2的空间尺寸， 该方法包括将导热反应装置加热至150-260℃的温度，使混合液体反应，以提供穿过管状微通道的反应液体的雷诺数在0.4至 100，反应完成后，连续冷却从导热反应装置排出的反应物。
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