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公开(公告)号：US20130137883A1
公开(公告)日：2013-05-30
申请号：US13816778
申请日：2011-08-19
申请人： Kohjiro Hashizume , Takuo Tsuno , Koji Kato , Hisahiro Morita
发明人： Kohjiro Hashizume , Takuo Tsuno , Koji Kato , Hisahiro Morita
CPC分类号： C07J53/004 , C07J9/00 , C07J53/00 , C07J63/008 , C11B3/006 , C11C3/06
摘要： A process for producing triterpene alcohol, comprising sequentially conducting the following steps (A) to (C): (A) subjecting γ-oryzanol to alkaline hydrolysis; (B) mixing the alkaline hydrolysate with a low polarity organic solvent, and extracting triterpene alcohol to obtain a triterpene alcohol-containing low polarity organic solvent; and (C) adding water to the triterpene alcohol-containing low polarity organic solvent thus obtained, removing the low polarity organic solvent, and then melting triterpene alcohol in hot water, followed by cooling.
摘要翻译： 一种制备三萜醇的方法，包括依次进行下列步骤（A）至（C）：（A）使γ-谷维素进行碱水解; （B）将碱性水解产物与低极性有机溶剂混合，萃取三萜醇得到含三萜醇的低极性有机溶剂; 和（C）向由此得到的三萜烯醇低极性有机溶剂中加入水，除去低极性有机溶剂，然后在热水中熔融三萜烯醇，然后冷却。
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公开(公告)号：US09200029B2
公开(公告)日：2015-12-01
申请号：US13816778
申请日：2011-08-19
申请人： Kohjiro Hashizume , Takuo Tsuno , Koji Kato , Hisahiro Morita
发明人： Kohjiro Hashizume , Takuo Tsuno , Koji Kato , Hisahiro Morita
CPC分类号： C07J53/004 , C07J9/00 , C07J53/00 , C07J63/008 , C11B3/006 , C11C3/06
摘要： A process for producing triterpene alcohol, comprising sequentially conducting the following steps (A) to (C): (A) subjecting γ-oryzanol to alkaline hydrolysis; (B) mixing the alkaline hydrolysate with a low polarity organic solvent, and extracting triterpene alcohol to obtain a triterpene alcohol-containing low polarity organic solvent; and (C) adding water to the triterpene alcohol-containing low polarity organic solvent thus obtained, removing the low polarity organic solvent, and then melting triterpene alcohol in hot water, followed by cooling.
摘要翻译： 一种制备三萜醇的方法，包括依次进行以下步骤（A）至（C）：（A）使γ-谷维素进行碱水解; （B）将碱性水解产物与低极性有机溶剂混合，萃取三萜醇得到含三萜醇的低极性有机溶剂; 和（C）向由此得到的三萜烯醇低极性有机溶剂中加入水，除去低极性有机溶剂，然后在热水中熔融三萜烯醇，然后冷却。
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