公开(公告)号：US08492409B2

公开(公告)日：2013-07-23

申请号：US12990193

申请日：2009-07-03

Applicant: Bin Li ,  Huibin Yang ,  Junfeng Wang ,  Haibo Yu ,  Hong Zhang ,  Zhinian Li ,  Yuquan Song

Inventor： Bin Li ,  Huibin Yang ,  Junfeng Wang ,  Haibo Yu ,  Hong Zhang ,  Zhinian Li ,  Yuquan Song

IPC: A01N43/40 ,  C07D401/04

CPC classification number: C07D401/04 ,  A01N43/56

Abstract: The present invention discloses a kind of 1-substituted pyridyl-pyrazolyl amide compounds and uses thereof. The compounds have structures as represented by the general formula I, wherein the definitions of each substituent showed in the specification. The compounds of formula I are novel and have excellent insecticidal and fungicidal activities and can be used for controlling insect pest and diseases.

Abstract translation: 本发明公开了一种1-取代的吡啶基吡唑基酰胺化合物及其用途。 化合物具有由通式I表示的结构，其中每个取代基的定义在说明书中显示。 式I化合物是新颖的，具有优异的杀虫和杀真菌活性，可用于防治害虫和疾病。

公开(公告)号：US08217179B2

公开(公告)日：2012-07-10

申请号：US12918133

申请日：2009-03-30

Applicant: Bin Li ,  Hongfei Wu ,  Haibo Yu ,  Huibin Yang

Inventor： Bin Li ,  Hongfei Wu ,  Haibo Yu ,  Huibin Yang

IPC: C07D401/04

CPC classification number: C07D401/04

Abstract: A preparation method of phenylcarboxamides of formula (I), the reaction scheme of which is as follows: wherein the groups are defined in the description. In this method, 3-halo-1-(3-chloro-2-pyridinyl)-4,5-dihydro-1H-pyrazole-5-carboxylic acid esters (V) as the raw materials are hydrolyzed to obtain carboxylic acids of formula (IV) under a basic condition, and carboxylic acids (IV) are simultaneously acyl halogenated and oxidated to get acyl halide of formula (III), and then without the presence of a acid binging agent, acyl chlorides (III) are reacted with substituted anilines (II) to get phenylcarboxamides of formula (I) in high yield.

Abstract translation: 式（I）的苯甲酰胺的制备方法，其反应方案如下：其中这些基团在说明书中定义。 在该方法中，将作为原料的3-卤代-1-（3-氯-2-吡啶基）-4,5-二氢-1H-吡唑-5-羧酸酯（V）水解，得到式 （Ⅳ），羧酸（Ⅳ）同时进行酰基卤化和氧化，得到式（Ⅳ）的酰卤，然后不存在酸性起始剂，酰基氯（III）与取代的 苯胺（II）以高产率得到式（I）的苯基甲酰胺。

公开(公告)号：US20110046186A1

公开(公告)日：2011-02-24

申请号：US12990193

申请日：2009-07-03

Applicant: Bin Li ,  Huibin Yang ,  Junfeng Wang ,  Haibo Yu ,  Hong Zhang ,  Zhinian Li ,  Yuquan Song

Inventor： Bin Li ,  Huibin Yang ,  Junfeng Wang ,  Haibo Yu ,  Hong Zhang ,  Zhinian Li ,  Yuquan Song

IPC: A01N43/56 ,  C07D401/04 ,  A01P3/00 ,  A01P7/04

CPC classification number: C07D401/04 ,  A01N43/56

Abstract: The present invention discoses a kind of 1-substituted pyridyl-pyrazolyl amide compounds and uses thereof. The compounds have structures as represented by the general formula I, wherein the definitions of each substituent showed in the specification. The compounds of formula I are novel and have excellent insecticidal and fungicidal activities and can be used for controlling insect pest and diseases.

Abstract translation: 本发明涉及一种1-取代的吡啶基吡唑基酰胺化合物及其用途。 化合物具有由通式I表示的结构，其中每个取代基的定义在说明书中显示。 式I化合物是新颖的，具有优异的杀虫和杀真菌活性，可用于防治害虫和疾病。

公开(公告)号：US09764363B2

公开(公告)日：2017-09-19

申请号：US14362051

申请日：2012-06-18

Applicant: Huacheng Zhang ,  Zeheng Li ,  Yunfeng He ,  Huibin Yang

Inventor： Huacheng Zhang ,  Zeheng Li ,  Yunfeng He ,  Huibin Yang

IPC: D06F37/26 ,  B08B3/02 ,  D06F39/08 ,  D06F39/14 ,  D06F37/28 ,  D06F35/00

CPC classification number: B08B3/02 ,  D06F35/008 ,  D06F37/28 ,  D06F39/088 ,  D06F39/14

Abstract: A drum washing machine is provided with a double spraying system used for washing the window and the window gasket ring respectively. A first spraying nozzle is connected with the inlet solenoid valve of the washing machine to wash the outer surface of the watching window and the window gasket ring, and a second spraying nozzle to wash the folded inner wall of the window gasket ring. The spraying nozzles are connected to the solenoid valve through a three-way pipe, or connected to the solenoid valve of the washing machine through respective pipes. The double spraying system intakes water and soaks the clothes in the washing process, and/or intakes water and sprays the watching window and the window gasket ring simultaneously, and/or sprays the watching window and the window gasket ring when dehydrating the clothes in the dehydrating process.

公开(公告)号：US20140299164A1

公开(公告)日：2014-10-09

申请号：US14362051

申请日：2012-06-18

Applicant: Huacheng Zhang ,  Zeheng Li ,  Yunfeng He ,  Huibin Yang

Inventor： Huacheng Zhang ,  Zeheng Li ,  Yunfeng He ,  Huibin Yang

IPC: B08B3/02

CPC classification number: B08B3/02 ,  D06F35/008 ,  D06F37/28 ,  D06F39/088 ,  D06F39/14

Abstract: A drum washing machine is provided with a double spraying system used for washing the window and the window gasket ring respectively. A first spraying nozzle is connected with the inlet solenoid valve of the washing machine to wash the outer surface of the watching window and the window gasket ring, and a second spraying nozzle to wash the folded inner wall of the window gasket ring. The spraying nozzles are connected to the solenoid valve through a three-way pipe, or connected to the solenoid valve of the washing machine through respective pipes. The double spraying system intakes water and soaks the clothes in the washing process, and/or intakes water and sprays the watching window and the window gasket ring simultaneously, and/or sprays the watching window and the window gasket ring when dehydrating the clothes in the dehydrating process.

Abstract translation: 滚筒洗衣机设有双重喷涂系统，分别用于清洗窗户和窗垫圈。 第一喷嘴与洗衣机的入口电磁阀连接以洗涤观察窗和窗垫圈的外表面，以及第二喷嘴，用于洗涤窗垫圈环的折叠内壁。 喷嘴通过三通管连接到电磁阀，或者通过相应的管连接到洗衣机的电磁阀。 双重喷洒系统在洗涤过程中吸入水并浸泡衣服，和/或进水并同时喷洒观察窗和窗垫圈，和/或在衣服脱水时喷洒观察窗和窗垫圈 脱水过程。

公开(公告)号：US20100317864A1

公开(公告)日：2010-12-16

申请号：US12918133

申请日：2009-03-30

Applicant: Bin Li ,  Hongfei Wu ,  Haibo Yu ,  Huibin Yang

Inventor： Bin Li ,  Hongfei Wu ,  Haibo Yu ,  Huibin Yang

IPC: C07D401/04

CPC classification number: C07D401/04

Abstract: A preparation method of phenylcarboxamides of formula (I), the reaction scheme of which is as follows: wherein the groups are defined in the description.In this method, 3-halo-1-(3-chloro-2-pyridinyl)-4,5-dihydro-1H-pyrazole-5-carboxylic acid esters (V) as the raw materials are hydrolyzed to obtain carboxylic acids of formula (IV) under a basic condition, and carboxylic acids (IV) are simultaneously acyl halogenated and oxidated to get acyl halide of formula (III), and then without the presence of a acid binging agent, acyl chlorides (III) are reacted with substituted anilines (II) to get phenylcarboxamides of formula (I) in high yield.

Abstract translation: 式（I）的苯甲酰胺的制备方法，其反应方案如下：其中这些基团在说明书中定义。 在该方法中，将作为原料的3-卤代-1-（3-氯-2-吡啶基）-4,5-二氢-1H-吡唑-5-羧酸酯（V）水解，得到式 （Ⅳ），羧酸（Ⅳ）同时进行酰基卤化和氧化，得到式（Ⅳ）的酰卤，然后不存在酸性起始剂，酰基氯（III）与取代的 苯胺（II）以高产率得到式（I）的苯基甲酰胺。