Process for the preparation of N-alkypolyhydroxyalkylamines from monoalkylamine and reducing sugar
    1.
    发明授权
    Process for the preparation of N-alkypolyhydroxyalkylamines from monoalkylamine and reducing sugar 失效
    从单烷基胺和还原糖制备N-烷基多羟基烷基胺的方法

    公开(公告)号:US06365778B1

    公开(公告)日:2002-04-02

    申请号:US09521480

    申请日:2000-03-09

    IPC分类号: C07C209116

    摘要: Aqueous, alcoholic or aqueous-alcoholic solutions of a monoalkylamine and a reducing sugar are simultaneously injected into a mixing unit and the two solutions are mixed under turbulence in the mixing unit for 6 seconds to 5 minutes at a temperature of 25 to 60° C. and a pressure of 50 to 90 bar. The mixture is then added to a hydrogenation reactor and hydrogenated with hydrogen in the presence of a hydrogenation catalyst. An alkylpolyhydroxyalkylamine is obtained in high yield and with high purity.

    摘要翻译: 将单烷基胺和还原糖的水溶液,醇或水溶液同时注入混合单元中,并将两种溶液在混合单元中在湍流下在25至60℃的温度下混合6秒至5分钟。 压力为50至90巴。 然后将混合物加入氢化反应器中,并在氢化催化剂存在下用氢气氢化。 以高产率和高纯度获得烷基聚羟基烷基胺。