公开(公告)号：US4582591A

公开(公告)日：1986-04-15

申请号：US637934

申请日：1984-08-06

申请人： Heinrich Hoermeyer ,  Juergen Stadelhofer ,  Heinrich Louis ,  Wolfgang Brueggemann

发明人： Heinrich Hoermeyer ,  Juergen Stadelhofer ,  Heinrich Louis ,  Wolfgang Brueggemann

IPC分类号： C10C1/18 ,  C10B55/00 ,  C10C3/08 ,  C10G21/02 ,  C10G53/06 ,  C10L5/16 ,  C10C3/00

CPC分类号： C10G53/06 ,  C10B55/00 ,  C10G21/02 ,  C10L5/16

摘要： Heavy oil derived from coal is diluted with organic solvent to a content of less than 10 weight percent of toluene-insoluble material. The mixture is then mixed with a non-aromatic solvent in a ratio of 1:3 to 5:1. With slow stirring of the heavy phase at a temperature of between 50.degree. and 200.degree. C., this mixture is separated into a pumpable TI-poor and a pumpable TI-rich fraction under the action of gravity, with a settling-surface load of up to 1 metric ton/m.sup.2 hour. No .beta.-resins are precipitated from these fluid fractions. No tacky, rubber-like sediment is formed from the TI-rich fraction. The fractions are distillatively separated from the solvents, which can be reused. The TI-poor fraction can be used, for example, as a carbon-black oil component or can be processed further to an impregnating agent for carbon shapes. Binders for carbon shapes or cokes are obtained from the TI-rich fraction.

摘要翻译： 来自煤的重油用有机溶剂稀释至小于10重量％的甲苯不溶物质的含量。 然后将混合物与非芳族溶剂以1:3至5:1的比例混合。 在50至200℃的温度下缓慢搅拌重相，将该混合物在重力作用下分离成可泵送的TI-贫和可泵送的富含TI的级分，其沉降面负荷 高达1公吨/平方米小时。 没有β-残基从这些流体组分中沉淀出来。 由富含TI的部分形成不粘的橡胶状沉淀物。 馏分与溶剂蒸馏分离，可以重复使用。 TI不良部分可以用作例如炭黑油组分，或者可以进一步加工成用于碳形状的浸渍剂。 用于碳形状或焦炭的粘合剂可从富含TI的部分获得。