公开(公告)号：US20100272623A1

公开(公告)日：2010-10-28

申请号：US12763618

申请日：2010-04-20

申请人： Alexander LUKACS, III ,  Leonard Macadams ,  Kevin Christmas

发明人： Alexander LUKACS, III ,  Leonard Macadams ,  Kevin Christmas

IPC分类号： C01B35/14 ,  C07F5/02

CPC分类号： C07F5/027 ,  C01B35/14

摘要： A method of preparing an ammonia borane compound selected from the group consisting of: ammonia borane, ammonia alkyl borane, ammonia aryl borane and mixtures thereof, the method including the steps of: a) incorporating a reaction mixture into a pressure vessel, the reaction mixture including anhydrous liquid ammonia and a boron containing compound that can react under pressure with the liquid ammonia to form the ammonia borane compound; and, b) causing the reaction mixture to warm from a first temperature greater than or equal to −33° C. to a second temperature under pressure to form the ammonia borane compound.

摘要翻译： 一种制备选自氨硼烷，氨烷基硼烷，氨基芳基硼烷及其混合物的氨硼烷化合物的方法，所述方法包括以下步骤：a）将反应混合物加入压力容器中，将反应混合物 包括无水液氨和可在压力下与液氨反应形成氨硼烷化合物的含硼化合物; 和b）使反应混合物在大于或等于-33℃的第一温度下加热至加压的第二温度以形成氨硼烷化合物。