公开(公告)号：US07491299B2

公开(公告)日：2009-02-17

申请号：US10473993

申请日：2002-04-04

Applicant: Mélanie Hebert ,  Jean Ollivier ,  Georges Fremy

Inventor： Mélanie Hebert ,  Jean Ollivier ,  Georges Fremy

IPC: C07C1/00 ,  C07F1/00 ,  C07B45/00

CPC classification number: C07C319/18 ,  B01J19/123 ,  B01J19/2465 ,  C07C321/14

Abstract: In the photochemical synthetic process in semi-continuous mode according to the invention, a reactor comprising two zones is used, the radiating portion of the lamp(s) being totally immersed in a first zone which is completely filled with reaction medium and spills off via an overflow into a second zone whose volume is sufficient to contain the volume of reaction medium originating from the first zone and corresponding substantially to the volume of the reagent(s) gradually introduced.

Abstract translation: 在根据本发明的半连续模式的光化学合成方法中，使用包括两个区域的反应器，所述灯的散热部分完全浸没在完全填充有反应介质的第一区域中并且通过 溢出到第二区域，其体积足以容纳源自第一区域的反应介质的体积并且基本上对应于逐渐引入的试剂的体积。