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1.发明授权公开(公告)号：US07423160B2
公开(公告)日：2008-09-09
申请号：US11846630
申请日：2007-08-29
IPC分类号： C07D207/00
CPC分类号： C07D207/333 , C07F5/02
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
摘要翻译： 一种制备金属络合物的方法包括将1-单酰基二吡咯甲烷与式R 1 R 2 MX的化合物组合，其中M是硼，R 1， R 2和R 2各自独立地为有机取代基; X为阴离子离去基团; 以制备其中DH是1-单酰基二吡咯甲烷的式DMR 1 R 2的金属络合物。 该方法和配合物可用于双嘧磺隆和卟啉的纯化和合成。
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2.发明申请BORON COMPLEXATION STRATEGY FOR USE IN MANIPULATING 1-ACYLDIPYRROMETHANES 有权用于操作1-ACYLDIPYRROMETHANES的BORON复合策略公开(公告)号：US20070088158A1
公开(公告)日：2007-04-19
申请号：US11559138
申请日：2006-11-13
IPC分类号： C07D487/22 , C07F5/02
CPC分类号： C07D207/333 , C07F5/02
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
摘要翻译： 一种制备金属络合物的方法包括将1-单酰基二吡咯甲烷与式R 1 R 2 MX的化合物组合，其中M是硼，R 1， R 2和R 2各自独立地为有机取代基; X为阴离子离去基团; 以制备其中DH是1-单酰基二吡咯甲烷的式DMR 1 R 2的金属络合物。 该方法和配合物可用于双嘧磺隆和卟啉的纯化和合成。
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公开(公告)号：US07317108B2
公开(公告)日：2008-01-08
申请号：US10956781
申请日：2004-10-01
IPC分类号： C07D207/00
CPC分类号： C07D207/335 , C07D487/22 , C07F5/02 , C07F5/022
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
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公开(公告)号：US20050282779A1
公开(公告)日：2005-12-22
申请号：US10956781
申请日：2004-10-01
IPC分类号： A61K31/69 , C07D487/22 , C07F5/02
CPC分类号： C07D207/335 , C07D487/22 , C07F5/02 , C07F5/022
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
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5.发明申请公开(公告)号：US20050282778A1
公开(公告)日：2005-12-22
申请号：US10872321
申请日：2004-06-18
IPC分类号： A61K31/69 , C07D487/22 , C07F5/02
CPC分类号： C07D207/333 , C07F5/02
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
摘要翻译： 一种制备金属络合物的方法包括将1-单酰基二吡咯甲烷与式R 1 2 R 2 MX的化合物组合，其中M是硼，R 1， R 2和R 2各自独立地为有机取代基; X为阴离子离去基团; 以制备其中DH是1-单酰基二吡咯甲烷的式DMR 1 R 2的金属络合物。 该方法和配合物可用于双嘧磺隆和卟啉的纯化和合成。
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公开(公告)号：US07947829B2
公开(公告)日：2011-05-24
申请号：US12780151
申请日：2010-05-14
IPC分类号： C07B47/00 , C07D487/22
CPC分类号： C07D487/04
摘要： A method of making a compound of Formula I: is carried out by condensing a pair of compounds of Formula II (which pair may be the same or different), or by condensing a compound of Formula III with a compound Formula IV, to produce a compound of Formula I. The condensing step may be carried out with a metal salt under basic conditions.
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公开(公告)号：US07745618B2
公开(公告)日：2010-06-29
申请号：US12036395
申请日：2008-02-25
IPC分类号： C07B47/00 , C07D487/22
CPC分类号： C07D487/04
摘要： A method of making a compound of Formula I: is carried out by condensing a pair of compounds of Formula II (which pair may be the same or different), or by condensing a compound of Formula III with a compound Formula IV, to produce a compound of Formula I. The condensing step may be carried out with a metal salt under basic conditions.
摘要翻译： 制备式I化合物的方法是通过将一对式II化合物（其可以相同或不同）的化合物或通过将式III化合物与式IV化合物缩合来制备式 式I化合物。缩合步骤可以在碱性条件下用金属盐进行。
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8.发明授权公开(公告)号：US07595407B2
公开(公告)日：2009-09-29
申请号：US11846646
申请日：2007-08-29
IPC分类号： C07D207/00
CPC分类号： C07D207/335 , C07D487/22 , C07F5/02 , C07F5/022
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
摘要翻译： 制备金属络合物的方法包括将1-单酰基二吡咯甲烷与式R1R2MX化合物组合，其中M为硼，R 1和R 2各自为有机取代基; X为阴离子离去基团; 以制备式DMR1R2的金属络合物，其中DH是1-单酰基二吡咯甲烷。 该方法和配合物可用于双嘧磺隆和卟啉的纯化和合成。
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9.发明授权公开(公告)号：US07153975B2
公开(公告)日：2006-12-26
申请号：US10872321
申请日：2004-06-18
IPC分类号： C07F5/02
CPC分类号： C07D207/333 , C07F5/02
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
摘要翻译： 一种制备金属络合物的方法包括将1-单酰基二吡咯甲烷与式R 1 2 R 2 MX的化合物组合，其中M是硼，R 1， R 2和R 2各自独立地为有机取代基; X为阴离子离去基团; 以制备其中DH是1-单酰基二吡咯甲烷的式DMR 1 R 2的金属络合物。 该方法和配合物可用于双嘧磺隆和卟啉的纯化和合成。
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公开(公告)号：US07964720B2
公开(公告)日：2011-06-21
申请号：US12960057
申请日：2010-12-03
IPC分类号： C07D487/22 , C07B47/00
CPC分类号： C07D487/04
摘要： A method of making a compound of Formula I: is carried out by condensing a pair of compounds of Formula II (which pair may be the same or different), or by condensing a compound of Formula III with a compound Formula IV, to produce a compound of Formula I. The condensing step may be carried out with a metal salt under basic conditions.
摘要翻译： 制备式I化合物的方法是通过将一对式II化合物（其可以相同或不同）的化合物或通过将式III化合物与式IV化合物缩合来制备式 式I化合物。缩合步骤可以在碱性条件下用金属盐进行。
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