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1.发明申请公开(公告)号：US20140044598A1
公开(公告)日：2014-02-13
申请号：US13961012
申请日：2013-08-07
CPC分类号： G01R33/305 , B23G1/02 , G01R3/00 , G01R33/307 , Y10T29/49996 , Y10T409/300112
摘要： Re-usable ceramic magic angle spinning (MAS) NMR rotors constructed of high-mechanic strength ceramics are detailed that include a sample compartment that maintains high pressures up to at least about 200 atmospheres (atm) and high temperatures up to about least about 300° C. during operation. The rotor designs minimize pressure losses stemming from penetration over an extended period of time. The present invention makes possible a variety of in-situ high pressure, high temperature MAS NMR experiments not previously achieved in the prior art.
摘要翻译： 详细描述了由高机械强度陶瓷构成的可重复使用的陶瓷魔角旋转（MAS）NMR转子，其包括保持高达至少约200大气压（atm）的高压和至多约300°的高温的样品室 C.操作期间 转子设计可以最大限度地减少长时间内渗透引起的压力损失。 本发明使现有技术中以前未实现的各种原位高压，高温MAS NMR实验成为可能。
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2.发明授权公开(公告)号：US09151813B2
公开(公告)日：2015-10-06
申请号：US13961012
申请日：2013-08-07
CPC分类号： G01R33/305 , B23G1/02 , G01R3/00 , G01R33/307 , Y10T29/49996 , Y10T409/300112
摘要： Re-usable ceramic magic angle spinning (MAS) NMR rotors constructed of high-mechanic strength ceramics are detailed that include a sample compartment that maintains high pressures up to at least about 200 atmospheres (atm) and high temperatures up to about least about 300° C. during operation. The rotor designs minimize pressure losses stemming from penetration over an extended period of time. The present invention makes possible a variety of in-situ high pressure, high temperature MAS NMR experiments not previously achieved in the prior art.
摘要翻译： 详细描述了由高机械强度陶瓷构成的可重复使用的陶瓷魔角旋转（MAS）NMR转子，其包括保持高达至少约200大气压（atm）的高压和至多约300°的高温的样品室 C.操作期间 转子设计可以最大限度地减少长时间内渗透引起的压力损失。 本发明使现有技术中以前未实现的各种原位高压，高温MAS NMR实验成为可能。
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