公开(公告)号：US06787633B2

公开(公告)日：2004-09-07

申请号：US10065062

申请日：2002-09-13

申请人： Rudy Francois Alain Jos Peemans ,  Wiebe Knol ,  Peter Groefsema

发明人： Rudy Francois Alain Jos Peemans ,  Wiebe Knol ,  Peter Groefsema

IPC分类号： C08G6538

CPC分类号： C08G65/46

摘要： A method of precipitating a poly(arylene ether) includes preparing a poly(arylene ether) solution comprising a poly(arylene ether) and a solvent, combining the poly (arylene ether) solution with an antisolvent to form a poly(arylene ether) dispersion comprising a poly(arylene ether) solid, separating the poly(arylene ether) solid from the poly(arylene ether) dispersion to form an isolated poly(arylene ether) solid, determining a particle size distribution of the poly(arylene ether) solid prior to separating the poly(arylene ether) solid from the poly(arylene ether) dispersion, and adjusting a precipitation parameter in response to the particle size distribution. Although the measured particle size distribution is very different from the particle size distribution of the solid poly(arylene ether) ultimately isolated, it is useful for controlling the process. The method may be automated to rapidly adjust precipitation conditions in response to the particle size distribution measurements. An apparatus for carrying out the method is also described.

摘要翻译： 沉淀聚（亚芳基醚）的方法包括制备包含聚（亚芳基醚）和溶剂的聚（亚芳基醚）溶液，将聚（亚芳基醚）溶液与抗溶剂结合以形成聚（亚芳基醚）分散体 包括聚（亚芳基醚）固体，从聚（亚芳基醚）分散体中分离聚（亚芳基醚）固体以形成分离的聚（亚芳基醚）固体，以前测定聚（亚芳基醚）固体的粒度分布 从聚（亚芳基醚）分散体中分离聚（亚芳基醚）固体，并根据粒度分布调节沉淀参数。 虽然测量的粒度分布与最终分离的固体聚（亚芳基醚）的粒度分布非常不同，但是对于控制该方法是有用的。 该方法可以自动化以响应于粒度分布测量快速调节沉淀条件。 还描述了用于执行该方法的装置。