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    Process for producing oligomers
    1.
    发明授权
    Process for producing oligomers 有权
    生产低聚物的方法

    公开(公告)号：US08507424B2

    公开(公告)日：2013-08-13

    申请号：US11171207

    申请日：2005-07-01

    申请人： Tian Lye Ooi ,  Salmiah Ahmad ,  Shoot Kian Yeong ,  Chun Ming Teoh

    发明人： Tian Lye Ooi ,  Salmiah Ahmad ,  Shoot Kian Yeong ,  Chun Ming Teoh

    IPC分类号： C10M129/70

    CPC分类号： C10M145/22 ,  C10M2207/2815 ,  C10M2209/102 ,  C10N2220/023 ,  C10N2220/08

    摘要： The present invention relates to a process for producing oligomers and a method for improving the low temperature properties of fatty alkyl esters by using these oligomers. The oligomers according to the present invention are used as pour point depressant and cloud point reducer to improve the pour point and cloud point of fatty alkyl esters such as isopropyl, butyl, ethyl, ethylhexyl esters particularly fatty acid methyl esters at low temperature.

    摘要翻译： 本发明涉及一种制备低聚物的方法和一种通过使用这些低聚物改进脂肪烷基酯的低温性能的方法。 根据本发明的低聚物用作倾点降低剂和浊点还原剂，以改善脂肪烷基酯如异丙基，丁基，乙基，乙基己基酯，特别是脂肪酸甲酯在低温下的倾点和浊点。

    PROCESS TO PRODUCE POLYOLS
    2.
    发明申请
    PROCESS TO PRODUCE POLYOLS 有权
    制造多元醇的方法

    公开(公告)号：US20080293913A1

    公开(公告)日：2008-11-27

    申请号：US12057444

    申请日：2008-03-28

    申请人： Hazimah ABU HASSAN ,  Tuan Noor Maznee Tuan Ismail ,  Mohd Norhisham Sattar ,  Seng Soi Hoong ,  Tian Lye Ooi ,  Salmiah Ahmad ,  Kosheela Devi a/p Poo Palam ,  Mei Yee Cheong

    发明人： Hazimah ABU HASSAN ,  Tuan Noor Maznee Tuan Ismail ,  Mohd Norhisham Sattar ,  Seng Soi Hoong ,  Tian Lye Ooi ,  Salmiah Ahmad ,  Kosheela Devi a/p Poo Palam ,  Mei Yee Cheong

    IPC分类号： C08G59/00 ,  C07D301/32

    CPC分类号： C07D301/32 ,  C08G18/36 ,  C08G59/025 ,  C08G59/027

    摘要： A process for producing oleochemical polyols comprises the steps of epoxidizing unsaturated oil using an organic acid together with oxygenated water or a per-acid to obtain epoxidized oil; washing the epoxidized oil with salt water to remove unused organic acid together with oxygenated water or a per-acid; neutralizing acidic condition of the washed epoxidized oil with a base; washing the neutralized epoxidized oil with a salt solution until the pH of the neutralized epoxidized oil reaching 6.5 to 7.5 to removed the base residue; drying the washed neutralized epoxidized oil under vacuum; and reacting the washed neutralized dried epoxidized oil with polyhydric alcohol in the presence of boron trifluoride-diethylether complex to produce the oleochemical polyols. The oleochemical polyols are then subjected to the same washing, neutralizing, washing and drying process as in preparing the washed neutralized dried epoxidized oil.

    摘要翻译： 一种制备油化多元醇的方法包括以下步骤：使用有机酸与含氧水或过酸环氧化不饱和油，得到环氧化油; 用盐水洗涤环氧化油，除去未使用的有机酸与氧化水或过酸; 用碱中和洗涤后的环氧化油的酸性条件; 用盐溶液洗涤中和的环氧化油直到中和的环氧化油的pH达到6.5-7.5以除去碱残渣; 在真空下干燥洗涤的中和的环氧化油; 并在三氟化硼 - 二乙醚络合物的存在下使洗涤的中和的干燥的环氧化油与多元醇反应，以产生油化学多元醇。 然后将油化多元醇进行与制备洗涤的中和的干燥的环氧化油相同的洗涤，中和，洗涤和干燥过程。

    Process to produce polyols
    5.
    发明授权
    Process to produce polyols 有权
    生产多元醇的方法

    公开(公告)号：US07932409B2

    公开(公告)日：2011-04-26

    申请号：US12057444

    申请日：2008-03-28

    申请人： Hazimah Abu Hassan ,  Tuan Noor Maznee Tuan Ismail ,  Mohd Norhisham Sattar ,  Seng Soi Hoong ,  Tian Lye Ooi ,  Salmiah Ahmad ,  Kosheela Devi a/p Poo Palam ,  Mei Yee Cheong

    发明人： Hazimah Abu Hassan ,  Tuan Noor Maznee Tuan Ismail ,  Mohd Norhisham Sattar ,  Seng Soi Hoong ,  Tian Lye Ooi ,  Salmiah Ahmad ,  Kosheela Devi a/p Poo Palam ,  Mei Yee Cheong

    IPC分类号： C07D301/32 ,  C08G65/02

    CPC分类号： C07D301/32 ,  C08G18/36 ,  C08G59/025 ,  C08G59/027

    摘要： A process for producing oleochemical polyols comprises the steps of epoxidizing unsaturated oil using an organic acid together with oxygenated water or a per-acid to obtain epoxidized oil; washing the epoxidized oil with salt water to remove unused organic acid together with oxygenated water or a per-acid; neutralizing acidic condition of the washed epoxidized oil with a base; washing the neutralized epoxidized oil with a salt solution until the pH of the neutralized epoxidized oil reaching 6.5 to 7.5 to removed the base residue; drying the washed neutralized epoxidized oil under vacuum; and reacting the washed neutralized dried epoxidized oil with polyhydric alcohol in the presence of boron trifluoride-diethylether complex to produce the oleochemical polyols. The oleochemical polyols are then subjected to the same washing, neutralizing, washing and drying process as in preparing the washed neutralized dried epoxidized oil.

    摘要翻译： 一种制备油化多元醇的方法包括以下步骤：使用有机酸与含氧水或过酸环氧化不饱和油，得到环氧化油; 用盐水洗涤环氧化油，除去未使用的有机酸与氧化水或过酸; 用碱中和洗涤后的环氧化油的酸性条件; 用盐溶液洗涤中和的环氧化油直到中和的环氧化油的pH达到6.5-7.5以除去碱残渣; 在真空下干燥洗涤的中和的环氧化油; 并在三氟化硼 - 二乙醚络合物的存在下使洗涤的中和的干燥的环氧化油与多元醇反应，以产生油化学多元醇。 然后将油化多元醇进行与制备洗涤的中和的干燥的环氧化油相同的洗涤，中和，洗涤和干燥过程。