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    Process for producing fire resistant organic textile materials
    1.
    发明授权
    Process for producing fire resistant organic textile materials 失效
    生产耐火有机纺织材料的工艺

    公开(公告)号：US3949108A

    公开(公告)日：1976-04-06

    申请号：US365895

    申请日：1973-06-01

    申请人： Darrell J. Donaldson ,  Floyd L. Normand ,  George L. Drake, Jr. ,  Wilson A. Reeves

    发明人： Darrell J. Donaldson ,  Floyd L. Normand ,  George L. Drake, Jr. ,  Wilson A. Reeves

    IPC分类号： D06M11/47 ,  D06M15/252 ,  D06M15/423 ,  C09K3/28

    CPC分类号： D06M15/423 ,  D06M11/47 ,  D06M15/252 ,  Y10S428/921

    摘要： Organic fibrous materials especially cellulosic and other textiles are rendered flame resistant upon treatment with an emulsion containing either (1) an organic bromine containing material having at least 65% bromine such as polyvinylbromide, (2) polyvinylbromide and an N-methylol agent such as trimethylolmethylglycoluril, (3) polyvinylbromide and a metal oxide such as antimony oxide, and (4) polyvinylbromide, N-methylol agent and metal oxide. The emulsions are applied to various fibers by the pad-dry-cure technique. The finish contained the added quality of wrinkle resistance and rot resistance. The treated textiles, including polyester/cotton blends remain highly flame resistant through innumerable laundry cycles.

    摘要翻译： 有机纤维材料，特别是纤维素和其它纺织品在用含有（1）含有至少65％溴的有机溴物质如聚溴乙烯，（2）聚乙烯基溴和N-羟甲基试剂如三羟甲基甲基甘脲 ，（3）聚溴乙烯和金属氧化物如氧化锑，和（4）聚乙烯基溴，N-羟甲基试剂和金属氧化物。 乳液通过垫 - 干固化技术施加到各种纤维上。 整理含有抗皱和抗腐蚀的附加品质。 被处理的纺织品，包括聚酯/棉混纺，经过无数的洗衣循环，保持高度的阻燃性。

    Process for reducing agent migration during treatment of knitted cotton fabric
    2.
    发明授权
    Process for reducing agent migration during treatment of knitted cotton fabric 失效
    针织棉织物处理过程中减少剂迁移的方法

    公开(公告)号：US3947613A

    公开(公告)日：1976-03-30

    申请号：US495461

    申请日：1974-08-07

    申请人： Bethlehem K. Andrews ,  John G. Frick, Jr. ,  Wilson A. Reeves

    发明人： Bethlehem K. Andrews ,  John G. Frick, Jr. ,  Wilson A. Reeves

    IPC分类号： D06M15/423 ,  B05D3/12 ,  B05D3/02

    CPC分类号： D06M15/423

    摘要： Knitted cotton fabrics in tubular form are impregnated to 20 to 35% wet add-on of crosslinking agent by any of several techniques including sprinkling, spraying, printing, or slop padding the solution of crosslinking agent to the outer surfaces of the fabric tube, or transferring the solution of crosslinking agent from impregnated material to the outer surfaces of the fabric tube, followed by a mechanical agitation step wherein the impregnated tubes are mechanically agitated at elevated temperatures under closed conditions, thereby eliminating agent migration toward fabric surfaces during drying of the cotton containing knitted fabrics in chemical treatments for smooth-drying properties and dimensional stabilization.

    摘要翻译： 管状的针织棉织物通过以下几种技术中的任何一种技术浸渍到20至35％的湿附加交联剂中，包括喷洒，喷涂，印刷或将交联剂溶液倾斜到织物管的外表面，或 将交联剂的溶液从浸渍材料转移到织物管的外表面，然后进行机械搅拌步骤，其中浸渍的管在封闭条件下在升高的温度下机械搅拌，从而在棉花干燥过程中消除了向织物表面的迁移 包含针织物在化学处理中的平滑干燥性能和尺寸稳定性。

    Phosphorus, nitrogen, bromin containing polymers and process for producing flame retardant textiles
    4.
    发明授权
    Phosphorus, nitrogen, bromin containing polymers and process for producing flame retardant textiles 失效
    磷，氮，溴化聚合物和制造阻燃纺织品的方法

    公开(公告)号：US3954400A

    公开(公告)日：1976-05-04

    申请号：US499810

    申请日：1974-08-22

    申请人： Wilson A. Reeves ,  Darrell J. Donaldson ,  Donald J. Daigle ,  George L. Drake, Jr. ,  John V. Beninate

    发明人： Wilson A. Reeves ,  Darrell J. Donaldson ,  Donald J. Daigle ,  George L. Drake, Jr. ,  John V. Beninate

    IPC分类号： D06M15/431 ,  C08G51/24 ,  D06M13/32 ,  D06M13/38

    CPC分类号： D06M15/431 ,  Y10S428/921

    摘要： Textile treating compositions containing the elements phosphorus, nitrogen, and bromine and the processes for imparting flame resistance to organic fibrous materials have been prepared. This is accomplished by impregnating the textile treating compositions consisting of (1) tris(hydroxymethyl)phosphine mixed with nitrogenous compounds containing at least two members of the group hydrogen and methylol radicals (--CH.sub.2 OH) attached to trivalent nitrogen atoms, or (2) soluble methylol phosphine adducts which contain one or more methylol phosphine radicals (P--CH.sub.2 OH) prepared by reacting tris(hydroxymethyl)phosphine with an amide or amine which contains one or more hydrogens attached to a trivalent nitrogen with an organic bromine containing material with at least 10% bromine in the form of bromine atoms attached to carbon atoms, in proportions selected so that generally the phosphorus contained in structures of the group (--CH.sub.2).sub.3 P amounts to a small portion of the total weight of the mixture, and heating to cause insolubilization in or on the fibrous structure.

    摘要翻译： 已经制备了含有磷，氮和溴元素的纺织品处理组合物和赋予有机纤维材料阻燃性的方法。 这是通过浸渍由（1）三（羟甲基）膦混合的纺织品处理组合物实现的，所述组合物与含有至少两个连接到三价氮原子的氢和羟甲基（-CH 2 OH）的成员的含氮化合物混合，或（2）可溶的 含有一个或多个羟甲基膦加成物的羟甲基膦加合物（P-CH 2 OH），其通过使三（羟甲基）膦与含有一个或多个与三价氮连接的氢的酰胺或胺与含有有机溴的材料与至少10 以溴原子连接碳原子的形式的溴，以选定的比例，使得通常基团（-CH 2）3 P的结构中所含的磷相当于混合物总重量的一小部分，并加热以引起不溶解 在纤维结构中或之上。

    Phosphorus, nitrogen, bromine containing polymers and process for producing flame retardant textiles
    5.
    发明授权
    Phosphorus, nitrogen, bromine containing polymers and process for producing flame retardant textiles 失效
    含磷，氮，溴的聚合物和制造阻燃纺织品的方法

    公开(公告)号：US4067687A

    公开(公告)日：1978-01-10

    申请号：US652277

    申请日：1976-01-23

    申请人： Darrell J. Donaldson ,  George L. Drake, Jr. ,  John V. Beninate ,  Wilson A. Reeves ,  Donald J. Daigle

    发明人： Darrell J. Donaldson ,  George L. Drake, Jr. ,  John V. Beninate ,  Wilson A. Reeves ,  Donald J. Daigle

    IPC分类号： D06M15/431 ,  D06M15/673 ,  D06M1/00

    CPC分类号： D06M15/673 ,  D06M15/431 ,  Y10S428/921

    摘要： Textile treating compositions containing the elements phosphorus, nitrogen, and bromine and the processes for imparting flame resistance to organic fibrous materials have been prepared. This is accomplished by impregnating the textile treating compositions consisting of (1) tris(hydroxymethyl)phosphine mixed with nitrogenous compounds containing at least two members of the group hydrogen and methylol radicals (--CH.sub.2 OH) attached to trivalent nitrogen atoms, or (2) soluble methylol phosphine adducts which contain one or more methylol phosphine radicals (P--CH.sub.2 OH) prepared by reacting tris(hydroxymethyl)phosphine with an amide or amine which contains one or more hydrogens attached to a trivalent nitrogen with an organic bromine containing material with at least 10% bromine in the form of bromine atoms attached to carbon atoms, in proportions selected so that generally the phosphorus contained in structures of the group (--CH.sub.2).sub.3 P amount to a small portion of the total weight of the mixture, and heating to cause insolubilization in or on the fibrous structure.

    摘要翻译： 已经制备了含有磷，氮和溴元素的纺织品处理组合物和赋予有机纤维材料阻燃性的方法。 这是通过浸渍由（1）三（羟甲基）膦混合的纺织品处理组合物实现的，所述组合物与含有至少两个连接到三价氮原子的氢和羟甲基（-CH 2 OH）的成员的含氮化合物混合，或（2）可溶的 含有一个或多个羟甲基膦加成物的羟甲基膦加合物（P-CH 2 OH），其通过使三（羟甲基）膦与含有一个或多个与三价氮连接的氢的酰胺或胺与含有有机溴的材料与至少10 以溴原子连接碳原子形式的溴的比例按所选择的比例，使得通常基团（-CH 2）3 P的结构中所含的磷相当于混合物总重量的一小部分，并加热以引起不溶解 在纤维结构中或之上。