公开(公告)号：US09221853B2

公开(公告)日：2015-12-29

申请号：US13514464

申请日：2010-10-25

申请人： Wei Wang ,  Shuguang Zhou ,  Long Qin ,  Bufan Ren ,  Zhigang Qian ,  Tao Liu ,  Huiling She ,  Yaxian Zhang

发明人： Wei Wang ,  Shuguang Zhou ,  Long Qin ,  Bufan Ren ,  Zhigang Qian ,  Tao Liu ,  Huiling She ,  Yaxian Zhang

IPC分类号： A01N57/20 ,  C07F9/38 ,  C07C211/04 ,  A01N33/04

CPC分类号： C07F9/38 ,  A01N33/04 ,  A01N57/20 ,  C07B2200/13 ,  C07C211/04 ,  C07F9/3808 ,  A01N25/12

摘要： This invention provides the herbicidal active ingredient, a dimethylamine salt crystal of N-phosphonomethyl glycine (glyphosate), its preparation process and a solid formulation containing the crystalline dimethylamine salt of glyphosate as well as its application. Said preparation process comprises adding glyphosate and a suitable amount of solvent into a conventional reactor and introducing a dimethylamine gas for reaction, wherein the reaction temperature is controlled between 5 and 90° C. After the completion of the reaction, the temperature is reduced slowly to a certain value, a crystalline dimethylamine salt of glyphosate is precipitated (or precipitated after a crystal seed is added).

摘要翻译： 本发明提供除草活性成分，N-膦酰基乙基甘氨酸（草甘膦）的二甲胺盐结晶，其制备方法和含有草甘膦结晶二甲胺盐的固体制剂及其应用。 所述制备方法包括将草甘膦和适量的溶剂加入到常规反应器中并引入二甲胺气体进行反应，其中反应温度控制在5至90℃之间。反应完成后，将温度缓慢降低至 一定值，草甘膦的结晶二甲胺盐沉淀（或在加入晶种后沉淀）。

公开(公告)号：US20150307528A1

公开(公告)日：2015-10-29

申请号：US13514464

申请日：2010-10-25

申请人： Wei Wang ,  Shuguang Zhou ,  Long Qin ,  Bufan Ren ,  Zhigang Qian ,  Tao Liu ,  Huiling She ,  Yaxian Zhang

发明人： Wei Wang ,  Shuguang Zhou ,  Long Qin ,  Bufan Ren ,  Zhigang Qian ,  Tao Liu ,  Huiling She ,  Yaxian Zhang

IPC分类号： C07F9/38 ,  A01N57/20 ,  A01N33/04 ,  C07C211/04

CPC分类号： C07F9/38 ,  A01N33/04 ,  A01N57/20 ,  C07B2200/13 ,  C07C211/04 ,  C07F9/3808 ,  A01N25/12

摘要： This invention provides the herbicidal active ingredient, a dimethylamine salt crystal of N-phosphonomethyl glycine (glyphosate), its preparation process and a solid formulation containing the crystalline dimethylamine salt of glyphosate as well as its application. Said preparation process comprises adding glyphosate and a suitable amount of solvent into a conventional reactor and introducing a dimethylamine gas for reaction, wherein the reaction temperature is controlled between 5 and 90° C. After the completion of the reaction, the temperature is reduced slowly to a certain value, a crystalline dimethylamine salt of glyphosate is precipitated (or precipitated after a crystal seed is added).

摘要翻译： 本发明提供除草活性成分，N-膦酰基乙基甘氨酸（草甘膦）的二甲胺盐结晶，其制备方法和含有草甘膦结晶二甲胺盐的固体制剂及其应用。 所述制备方法包括将草甘膦和适量的溶剂加入到常规反应器中并引入二甲胺气体进行反应，其中反应温度控制在5至90℃之间。反应完成后，将温度缓慢降低至 一定值，草甘膦的结晶二甲胺盐沉淀（或在加入晶种后沉淀）。