METHOD OF SYNTHESIS OF HIGH DISPERSED SPHERICAL Y OR Nb DOPED LITHIUM TITANATE OXIDE USING TITANIUM TETRACHLORIDE AND LITHIUM HYDROXIDE
    1.
    发明申请
    METHOD OF SYNTHESIS OF HIGH DISPERSED SPHERICAL Y OR Nb DOPED LITHIUM TITANATE OXIDE USING TITANIUM TETRACHLORIDE AND LITHIUM HYDROXIDE 有权
    使用四氯化钛和氢氧化锂合成高分散球形Y或Nb掺杂的钛酸锂氧化物的方法

    公开(公告)号:US20140004346A1

    公开(公告)日:2014-01-02

    申请号:US13600691

    申请日:2012-08-31

    IPC分类号: H01B1/02 B32B5/16

    摘要: The present disclosure relates to a method of synthesis of Lithium Titanate Oxide used for a cathode of Lithium ion battery, the method comprising: (A) diluting TiCl4 with TiOCl2; (B) adding YCl3 or NbCl5 at the rate of 0.1˜2 mol % to Ti(mol); (C) forming a complex salt by dissolving to put at least one selected from a group consisting of Hydroxy propyl cellulose or Polyethylene glycol in a solvent, the Hydroxy propyl cellulose being a complexing agent and being a dispersing agent as well, whereas the Polyethylene glycol being a dispersing agent; (D) synthesizing a titanium precursor by adding an aqueous ammonia solution; (E) preparing Y or Nb doped titanium dioxide(TiO2) powder by heat-treating the synthetic product in a temperature of 500˜700° C.; and (F) mixing the Y or Nb doped TiO2 powder with LiOH.H2O and heat-treating the mixture in a temperature of 800˜900° C.

    摘要翻译: 本公开内容涉及用于锂离子电池阴极的钛酸锂氧化物的合成方法,该方法包括:(A)用TiO 2稀释TiCl 4; (B)以0.1〜2mol%的比例向Ti(mol)中加入YCl3或NbCl5; (C)通过溶解形成复合盐,将选自羟丙基纤维素或聚乙二醇的至少一种溶解于溶剂中,羟丙基纤维素为络合剂,为分散剂,而聚乙二醇 作为分散剂; (D)通过加入氨水溶液合成钛前体; (E)在500〜700℃的温度下对合成产物进行热处理制备Y或Nb掺杂的二氧化钛(TiO 2)粉末。 和(F)将Y或Nb掺杂的TiO 2粉末与LiOH·H 2 O混合并在800〜900℃的温度下进行热处理。

    METHOD OF MANUFACTURING UNIT CELL OF SOLID OXIDE FUEL CELL USING TRANSFER PROCESS
    2.
    发明申请
    METHOD OF MANUFACTURING UNIT CELL OF SOLID OXIDE FUEL CELL USING TRANSFER PROCESS 有权
    使用转移方法制造固体氧化物燃料电池单元的方法

    公开(公告)号:US20110135813A1

    公开(公告)日:2011-06-09

    申请号:US12963258

    申请日:2010-12-08

    IPC分类号: H01M8/00

    摘要: A method of manufacturing a unit cell of a solid oxide fuel cell using a transfer process, in which an anode, electrolyte, cathode and interconnect are deposited on a substrate using the transfer process when the unit cell of the solid oxide fuel cell having a variety of shapes, such as a planar type, a horizontal pipe type, a tubular type, a segmented type, and the like, is manufactured. In manufacture of solid oxide fuel cells having a variety of shapes according to lamination and arrangement of unit cells, the components of each unit cell, such as the anode, the cathode, the electrolyte, the interconnect, and the like, may be deposited in a desired shape using the transfer process through deposition or coating, so that the components of the unit cell having a large scale or a complicated structure can be deposited without limit in size and shape, the thickness of the components of the unit cell can be easily controlled depending on the number of stacked transfer paper sheets, and a coating film can be formed on a substrate at a lower cost.

    摘要翻译: 使用转印法制造固体氧化物型燃料电池的单电池的方法,其中当具有多种固体氧化物燃料电池的单电池时,使用转印工艺将阳极,电解质,阴极和互连物质沉积在基板上 的形状,例如平面型,水平管型,管状型,分段型等。 在根据单元电池的层压和布置制造具有各种形状的固体氧化物燃料电池时,可以将每个单元电池的元件(例如阳极,阴极,电解质,互连等)沉积在 使用通过沉积或涂覆的转印工艺的期望形状,使得可以在尺寸和形状上没有限制地沉积具有大尺寸或复杂结构的单元电池的部件,单元电池的部件的厚度可以容易地 根据堆叠的转印纸张的数量进行控制,并且可以以较低的成本在基板上形成涂膜。