Process for the preparation of magnetic powders based on .gamma.-Fe.sub.2
O.sub.3
    1.
    发明授权
    Process for the preparation of magnetic powders based on .gamma.-Fe.sub.2 O.sub.3 失效
    基于γ-Fe2O3制备磁粉的工艺

    公开(公告)号:US4224175A

    公开(公告)日:1980-09-23

    申请号:US29937

    申请日:1979-04-13

    IPC分类号: G11B5/706 C01G49/06

    CPC分类号: G11B5/70673

    摘要: A process is disclosed for obtaining acicular magnetic particles of .gamma.-Fe.sub.2 O.sub.3 modified with Fe.sup.++ and Co.sup.++ ions. The product thus obtained and magnetic tapes containing said product are also disclosed. A suspension of acicular .gamma.-Fe.sub.2 O.sub.3 in an aqueous solution of soluble Fe.sup.++ and Co.sup.++ salts is prepared. NH.sub.3 is then added in such quantity that the molar ratioNH.sub.3 /(Fe.sup.++ +Co.sup.++)is between 2.1 and 3, and the whole mass is then heated up to 100.degree.-200.degree. C. When the molar ratio Fe.sup.++ /Co.sup.++ is greater than about 2.5, it is necessary to operate in the presence of a metered quantity of oxygen or of an oxygen-containing gas; when the ratio is smaller or equal to about 2.5, the presence of a metered quantity of oxygen is optional.

    摘要翻译: 公开了一种获得用Fe ++和Co ++离子改性的γ-Fe2O3的针状磁性颗粒的方法。 由此获得的产品和含有所述产品的磁带也被公开。 制备针状γ-Fe2O3在可溶性Fe ++和Co ++盐水溶液中的悬浮液。 然后加入NH 3,使得NH 3 /(Fe +++ Co ++)的摩尔比在2.1和3之间,然后将整个物质加热至100℃-200℃。当Fe ++ / Co ++的摩尔比为 大于约2.5,需要在计量的氧气或含氧气体的存在下操作; 当该比例小于或等于约2.5时,计量的氧的存在是任选的。