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公开(公告)号：US20120322651A1
公开(公告)日：2012-12-20
申请号：US13576439
申请日：2011-01-28
IPC分类号： C07C29/152 , C07C29/154 , B23P23/00 , B01J37/00
CPC分类号： B01J8/0457 , B01J2208/00061 , B01J2208/00274 , B01J2208/00628 , B01J2208/025 , B01J2219/0004 , C07C29/1512 , C07C29/154 , Y02P20/52 , Y10T29/49716 , C07C31/04
摘要： Catalytic process for the preparation of methanol, with a plurality of serial synthesis stages, in which the severity of the reaction conditions, on the basis of the reaction temperature and/or the concentration of carbon monoxide in the synthesis gas, decreases from the first to the last reaction stage in flow direction, the first reaction stage having a first catalyst of low activity but high long-term stability, and the last reaction stage having a second catalyst of high activity but low long-term stability.
摘要翻译： 用于制备甲醇的催化方法，其中多个连续合成阶段，其中基于反应温度和/或合成气中一氧化碳浓度的反应条件的严重性从第一至第 在流动方向的最后反应阶段，第一反应阶段具有低活性但长期稳定性高的第一催化剂，最后反应阶段具有高活性但低长期稳定性的第二催化剂。
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公开(公告)号：US20120129958A1
公开(公告)日：2012-05-24
申请号：US13386098
申请日：2010-07-16
申请人： Andreas Bormann , Veronika Gronemann , Rainer Morgenroth , Jan Hagemann , Holger Schlichting , Philipp Marius Hackel
发明人： Andreas Bormann , Veronika Gronemann , Rainer Morgenroth , Jan Hagemann , Holger Schlichting , Philipp Marius Hackel
CPC分类号： C07C29/152 , C07C31/04
摘要： A method for producing methanol from a synthesis gas containing hydrogen and carbon oxides with a high content of inert components includes passing the synthesis gas through a synthesis reactor so as to catalytically convert a part of the carbon oxides to methanol. The methanol is separated from the obtained mixture from the reactor. The mixture liberated from methanol is separated into a cycle stream and a purge stream. The cycle stream is recirculated so as to form a synthesis circle and combined with a fresh gas stream including hydrogen and carbon oxides before being charged into the synthesis reactor. The purge stream is supplied to a secondary reactor so as to catalytically convert a further part of the hydrogen and carbon oxides to methanol. Further methanol is separated the obtained mixture including synthesis gas, inert components and methanol vapor.
摘要翻译： 从含有高含量惰性成分的氢和碳氧化物的合成气生产甲醇的方法包括使合成气通过合成反应器，以将一部分碳氧化物催化转化为甲醇。 将甲醇从所得反应器的混合物中分离。 从甲醇中释出的混合物被分离成循环流和净化流。 循环流再循环以形成合成圆，并且在包含氢和碳氧化物的新鲜气流之前被装入合成反应器中。 将吹扫流供给到二次反应器中，以将另一部分氢和碳氧化物催化转化成甲醇。 分离得到的混合物，包括合成气，惰性组分和甲醇蒸气。
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公开(公告)号：US09040594B2
公开(公告)日：2015-05-26
申请号：US13386098
申请日：2010-07-16
申请人： Andreas Bormann , Veronika Gronemann , Rainer Morgenroth , Jan Hagemann , Holger Schlichting , Philipp Marius Hackel
发明人： Andreas Bormann , Veronika Gronemann , Rainer Morgenroth , Jan Hagemann , Holger Schlichting , Philipp Marius Hackel
IPC分类号： C07C29/152 , B01J8/00
CPC分类号： C07C29/152 , C07C31/04
摘要： A method for producing methanol from a synthesis gas containing hydrogen and carbon oxides with a high content of inert components includes passing the synthesis gas through a synthesis reactor so as to catalytically convert a part of the carbon oxides to methanol. The methanol is separated from the obtained mixture from the reactor. The mixture liberated from methanol is separated into a cycle stream and a purge stream. The cycle stream is recirculated so as to form a synthesis circle and combined with a fresh gas stream including hydrogen and carbon oxides before being charged into the synthesis reactor. The purge stream is supplied to a secondary reactor so as to catalytically convert a further part of the hydrogen and carbon oxides to methanol. Further methanol is separated the obtained mixture including synthesis gas, inert components and methanol vapor.
摘要翻译： 从含有高含量惰性成分的氢和碳氧化物的合成气生产甲醇的方法包括使合成气通过合成反应器，以将一部分碳氧化物催化转化为甲醇。 将甲醇从所得反应器的混合物中分离。 从甲醇中释出的混合物被分离成循环流和净化流。 循环流再循环以形成合成圆，并且在包含氢和碳氧化物的新鲜气流之前被装入合成反应器中。 将吹扫流供给到二次反应器中，以将另一部分氢和碳氧化物催化转化成甲醇。 分离得到的混合物，包括合成气，惰性组分和甲醇蒸气。
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公开(公告)号：US20140031438A1
公开(公告)日：2014-01-30
申请号：US14111205
申请日：2012-03-22
IPC分类号： C07C29/152
CPC分类号： C07C29/152 , B01J19/245 , B01J2219/24 , C10J3/82 , C10J2300/0916 , C10J2300/093 , Y02E50/18 , Y10T29/49716 , C07C31/04
摘要： A method for producing methanol from inert-rich syngas includes installing a catalytic pre-reactor is upstream of the single or mufti-stage synthesis loop, a first part of the syngas being converted to methanol in the catalytic pre-reactor. Furthermore, an inert gas separation stage, for example a pressure swing adsorption system or a membrane system, is connected downstream of the synthesis loop, whereby a hydrogen-enriched syngas stream can be returned to the synthesis loop. In the processing of methane-rich syngas, the inert gas separation stage may also comprise an autothermal reformer in which methane is converted to carbon oxides and hydrogen, which are also returned into the synthesis loop.
摘要翻译： 从富惰性合成气生产甲醇的方法包括将催化预反应器安装在单级或多级合成回路的上游，第一部分合成气在催化预反应器中转化为甲醇。 此外，惰性气体分离阶段，例如变压吸附系统或膜系统，连接在合成回路的下游，由此富氢合成气流可返回合成回路。 在富甲烷合成气的处理中，惰性气体分离阶段还可以包括其中甲烷转化为碳氧化物和氢的自热重整器，其也返回到合成回路中。
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5.发明授权Process and plant for the production of methanol from synthesis gas rich in inerts 有权从合成气生产甲醇的工艺和装置富含惰性物质公开(公告)号：US09296672B2
公开(公告)日：2016-03-29
申请号：US14111205
申请日：2012-03-22
IPC分类号： C07C29/152
CPC分类号： C07C29/152 , B01J19/245 , B01J2219/24 , C10J3/82 , C10J2300/0916 , C10J2300/093 , Y02E50/18 , Y10T29/49716 , C07C31/04
摘要： A method for producing methanol from inert-rich syngas includes installing a catalytic pre-reactor is upstream of the single or mufti-stage synthesis loop, a first part of the syngas being converted to methanol in the catalytic pre-reactor. Furthermore, an inert gas separation stage, for example a pressure swing adsorption system or a membrane system, is connected downstream of the synthesis loop, whereby a hydrogen-enriched syngas stream can be returned to the synthesis loop. In the processing of methane-rich syngas, the inert gas separation stage may also comprise an autothermal reformer in which methane is converted to carbon oxides and hydrogen, which are also returned into the synthesis loop.
摘要翻译： 从富惰性合成气生产甲醇的方法包括将催化预反应器安装在单级或多级合成回路的上游，第一部分合成气在催化预反应器中转化为甲醇。 此外，惰性气体分离阶段，例如变压吸附系统或膜系统，连接在合成回路的下游，由此富氢合成气流可返回合成回路。 在富甲烷合成气的处理中，惰性气体分离阶段还可以包括其中甲烷转化为碳氧化物和氢的自热重整器，其也返回到合成回路中。
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公开(公告)号：US08629191B2
公开(公告)日：2014-01-14
申请号：US13121562
申请日：2009-07-29
IPC分类号： C07C27/00
CPC分类号： C07C29/152 , B01J8/067 , B01J2208/00274 , B01J2219/0004 , C07C31/04
摘要： For producing methanol from a synthesis gas containing hydrogen and carbon oxides the synthesis gas is passed through a first, water-cooled reactor in which a part of the carbon oxides is catalytically converted to methanol. The resulting mixture containing synthesis gas and methanol vapor is supplied to a second, gas-cooled reactor in which a further part of the carbon oxides is converted to methanol. Subsequently, methanol is separated from the synthesis gas, and synthesis gas is recirculated to the first reactor. The cooling gas flows through the second reactor cocurrent to the mixture withdrawn from the first reactor.
摘要翻译： 为了从含有氢和碳氧化物的合成气生产甲醇，合成气通过第一个水冷反应器，其中一部分碳氧化物被催化转化成甲醇。 将所得到的含有合成气和甲醇蒸汽的混合物供应到第二个气冷反应器中，其中另外一部分碳氧化物转化为甲醇。 随后，从合成气中分离出甲醇，合成气再循环至第一反应器。 冷却气体流过第二反应器并流至从第一反应器排出的混合物。
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公开(公告)号：US20110178188A1
公开(公告)日：2011-07-21
申请号：US13121562
申请日：2009-07-29
IPC分类号： C07C29/152
CPC分类号： C07C29/152 , B01J8/067 , B01J2208/00274 , B01J2219/0004 , C07C31/04
摘要： For producing methanol from a synthesis gas containing hydrogen and carbon oxides the synthesis gas is passed through a first, water-cooled reactor in which a part of the carbon oxides is catalytically converted to methanol. The resulting mixture containing synthesis gas and methanol vapor is supplied to a second, gas-cooled reactor in which a further part of the carbon oxides is converted to methanol. Subsequently, methanol is separated from the synthesis gas, and synthesis gas is recirculated to the first reactor. The cooling gas flows through the second reactor cocurrent to the mixture withdrawn from the first reactor.
摘要翻译： 为了从含有氢和碳氧化物的合成气生产甲醇，合成气通过第一个水冷反应器，其中一部分碳氧化物被催化转化成甲醇。 将所得到的含有合成气和甲醇蒸汽的混合物供应到第二个气冷反应器中，其中另外一部分碳氧化物转化为甲醇。 随后，从合成气中分离出甲醇，合成气再循环至第一反应器。 冷却气体流过第二反应器并流至从第一反应器排出的混合物。
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