公开(公告)号：US20090240083A1

公开(公告)日：2009-09-24

申请号：US12408899

申请日：2009-03-23

申请人： Huiyue Li ,  Jinghua Chen ,  Jiangwei Wu ,  Guirong Huang ,  Xinping Zhao ,  Kaiquan Wang

发明人： Huiyue Li ,  Jinghua Chen ,  Jiangwei Wu ,  Guirong Huang ,  Xinping Zhao ,  Kaiquan Wang

IPC分类号： C07C209/10

CPC分类号： C07C209/10 ,  C07C211/52

摘要： This invention is involved with a preparation method of 2,6-dichlor-4-trifluoromethyl aniline. With this process, 4-chlorotrifluoromethyl benzene is used as the starting material and subjected to halogenation reaction and ammoniation reaction and through separation of reaction products the desired 2,6-dichlor-4-trifluoromethyl aniline is obtained. In addition, ammonia is recovered from the surplus ammonia water in ammoniation reaction. This applied invention in characterized by simple process, cheap and easy-available raw materials, high reaction yield and friendly environment.

摘要翻译： 本发明涉及2,6-二氯-4-三氟甲基苯胺的制备方法。 通过该方法，使用4-氯三氟甲基苯作为原料，进行卤化反应和氨化反应，通过分离反应产物，得到所需的2,6-二氯-4-三氟甲基苯胺。 此外，在氨化反应中从多余的氨水中回收氨。 本发明的特点是工艺简单，原料价格便宜，反应产率高，环境友好。

公开(公告)号：US07777079B2

公开(公告)日：2010-08-17

申请号：US12408899

申请日：2009-03-23

申请人： Huiyue Li ,  Jinghua Chen ,  Jiangwei Wu ,  Guirong Huang ,  Xinping Zhao ,  Kaiquan Wang

发明人： Huiyue Li ,  Jinghua Chen ,  Jiangwei Wu ,  Guirong Huang ,  Xinping Zhao ,  Kaiquan Wang

IPC分类号： C07C209/10

CPC分类号： C07C209/10 ,  C07C211/52

摘要： This invention is involved with a preparation method of 2,6-dichloro-4-trifluoromethyl-aniline. With this process, p-Chlorobenzotrifluoride is used as the starting material and subjected to halogenation reaction and ammoniation reaction and through separation of reaction products the desired 2,6-dichloro-4-trifluoromethyl-aniline is obtained. In addition, ammonia is recovered from the surplus ammonia water in ammoniation reaction. This applied invention in characterized by simple process, cheap and easy-available raw materials, high reaction yield and friendly environment.

摘要翻译： 本发明涉及2,6-二氯-4-三氟甲基 - 苯胺的制备方法。 通过该方法，使用对氯三氟甲苯作为原料，进行卤化反应和氨化反应，通过反应产物的分离，得到所需的2,6-二氯-4-三氟甲基 - 苯胺。 此外，在氨化反应中从多余的氨水中回收氨。 本发明的特点是工艺简单，原料价格便宜，反应产率高，环境友好。