公开(公告)号：US06291622B1

公开(公告)日：2001-09-18

申请号：US09470533

申请日：1999-12-22

申请人： Jürgen Dröse ,  Hubertus Geisler ,  Wolfgang Hiersche ,  Klaus-Dieter Klein ,  Wilfried Knott ,  Andreas Mehrwald ,  Dagmar Windbiel

发明人： Jürgen Dröse ,  Hubertus Geisler ,  Wolfgang Hiersche ,  Klaus-Dieter Klein ,  Wilfried Knott ,  Andreas Mehrwald ,  Dagmar Windbiel

IPC分类号： C08G7706

CPC分类号： C08G77/46 ,  C08G77/38

摘要： A continuous process for preparing organomodified polysiloxanes by the transition metal-catalyzed addition of polysiloxanes containing SiH groups onto substances containing C—C multiple bonds, in particular a process for the continuous hydrosilylation of substances containing C—C multiple bonds, which comprises introducing the reactants, in the presence or absence of a homogeneous or heterogeneous catalyst, into a loop-like, heatable and coolable reaction circuit which has a static mixing element and/or a dynamic mixing element to mix starting materials and product formed, leaving the reaction mixture in the reaction circuit until a predetermined degree of conversion has been reached and subsequently transferring the reaction mixture still containing starting materials to a tube reactor to complete the reaction and taking it off via a receiver. In addition, a suitable industrial apparatus for carrying out the process of the invention is described.

摘要翻译： 通过过渡金属催化加成含有SiH基团的聚硅氧烷到含有多个CC的物质的物质，特别是含有CC多键的物质的连续氢化硅烷化方法，用于制备有机改性聚硅氧烷的连续方法，其包括在存在下引入反应物 或不存在均相或多相催化剂，形成环状，可加热和可冷却的反应回路，其具有静态混合元件和/或动态混合元件以混合起始材料和形成的产物，将反应混合物留在反应回路中直到 已经达到预定的转化率，随后将仍含有原料的反应混合物转移到管式反应器中以完成反应，并通过接收器将其取出。 此外，描述了用于实施本发明的方法的合适的工业设备。