Separation of 2,4-toluenediamine from an isomeric mixture of toluenediamines
    1.
    发明授权
    Separation of 2,4-toluenediamine from an isomeric mixture of toluenediamines 失效
    从甲苯二胺的异构体混合物中分离2,4-甲苯二胺

    公开(公告)号:US06469212B1

    公开(公告)日:2002-10-22

    申请号:US09531210

    申请日:2000-03-20

    IPC分类号: C07C20900

    CPC分类号: C07C209/86 C07C211/50

    摘要: A mixture comprised of about 60-85% of 2,4-toluenediamine (2,4-TDA) and about 15-40% of 2,6-toluenediamine (2,6-TDA) is melted, the temperature of the mixture is lowered to a 2,4-TDA nucleation temperature, and the temperature of the mixture is gradually reduced from the nucleation temperature to about 65 to about 70° C. The resultant mixture is in the form of a solids phase enriched in 2,4-TDA, and a novel and useful liquid phase enriched in 2,6-TDA. These phases are separated. Preferably the solids are further purified by “sweating” them and removing the sweated liquid impurities. The sweated liquid can be recycled together with another charge of a mixture comprised of 2,4-TDA and 2,6-TDA. 2,4-TDA can be produced with a purity of 96-99%.

    摘要翻译: 将由约60-85%的2,4-甲苯二胺(2,4-TDA)和约15-40%的2,6-甲苯二胺(2,6-TDA)组成的混合物熔化,混合物的温度为 降低至2,4-TDA成核温度,并且混合物的温度从成核温度逐渐降低至约65至约70℃。所得混合物为富含2,4-二甲酸的固体相的形式, TDA,以及富含2,6-TDA的新型有用的液相。 这些阶段是分开的。 优选地,通过将​​它们“出汗”并除去出汗的液体杂质来进一步纯化固体。 可以将出汗的液体与另一种由2,4-TDA和2,6-TDA组成的混合物一起再循环。 可以生产纯度为96-99%的2,4-TDA。

    Timing ball
    2.
    发明授权

    公开(公告)号:US10668348B1

    公开(公告)日:2020-06-02

    申请号:US16435471

    申请日:2019-06-08

    申请人: Jason G. Jones

    发明人: Jason G. Jones

    IPC分类号: A63B69/22 A63B69/20 A63B71/02

    摘要: A striking apparatus for all fighting art forms such as boxing to improve a user's fighting skills. The striking apparatus includes a timing ball having a link disposed thereon; an elongated adjustable rope; a swivel mounted to a swivel plate, the swivel plate being mounted to a backboard; the backboard being optionally attached to a frame; the link disposed on the timing ball being attached to the elongated adjustable rope, the rope being attached to the swivel; and the timing ball configured to be struck by the knuckles of a user's fist. Another embodiment of the invention includes a punching apparatus station for all fighting art forms which generally includes the same configuration as the striking apparatus referenced-above. Importantly, the striking apparatus advantageously is a cross between a speed bag, a double end bag, and a maze ball but is beneficially more effective than all three.

    Timing ball
    3.
    发明授权

    公开(公告)号:US10357701B2

    公开(公告)日:2019-07-23

    申请号:US15439088

    申请日:2017-02-22

    申请人: Jason G. Jones

    发明人: Jason G. Jones

    IPC分类号: A63B69/22 A63B69/20 A63B71/02

    摘要: A striking apparatus for all fighting art forms such as boxing to improve a user's fighting skills. The striking apparatus includes a timing ball having a link disposed thereon; an elongated adjustable rope; a swivel mounted to a swivel plate, the swivel plate being mounted to a backboard; the backboard being attached to a frame; the link disposed on the timing ball being attached to the elongated adjustable rope, the rope being attached to the swivel; and the timing ball configured to be struck by the knuckles of a user's fist. Another embodiment of the invention includes a punching apparatus station for all fighting art forms which generally includes the same configuration as the striking apparatus referenced-above. Importantly, the striking apparatus advantageously is a cross between a speed bag, a double end bag, and a maze ball but is beneficially more effective than all three.

    Timing Ball
    4.
    发明申请
    Timing Ball 审中-公开

    公开(公告)号:US20170252628A1

    公开(公告)日:2017-09-07

    申请号:US15439088

    申请日:2017-02-22

    申请人: Jason G. Jones

    发明人: Jason G. Jones

    IPC分类号: A63B69/20

    摘要: A striking apparatus for all fighting art forms such as boxing to improve a user's fighting skills. The striking apparatus includes a timing ball having a link disposed thereon; an elongated adjustable rope; a swivel mounted to a swivel plate, said swivel plate being mounted to a backboard; the backboard being attached to a frame; the link disposed on the timing ball being attached to the elongated adjustable rope, said rope being attached to said swivel; and the timing ball configured to be struck by the knuckles of a user's fist. Another embodiment of the invention includes a punching apparatus station for all fighting art forms which generally includes the same configuration as the striking apparatus referenced-above. Importantly, the striking apparatus advantageously is a cross between a speed bag, a double end bag, and a maze ball but is beneficially more effective than all three.