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1.发明授权Method of preparing a poly (arylene ether) and a poly (arylene ether) prepared thereby 有权制备由其制备的聚（亚芳基醚）和聚（亚芳基醚）的方法公开(公告)号：US06437084B1
公开(公告)日：2002-08-20
申请号：US09683037
申请日：2001-11-12
申请人： Joop Birsak , Hugo Gerard Eduard Ingelbrecht , David Parrillo , Mukund Parthasarathy , Probjot Singh
发明人： Joop Birsak , Hugo Gerard Eduard Ingelbrecht , David Parrillo , Mukund Parthasarathy , Probjot Singh
IPC分类号： C08G6538
CPC分类号： C08G65/44
摘要： A method of preparing a poly(arylene ether) includes oxidatively coupling a monohydric phenol in a reaction solution at a reaction temperature that exceeds the cloud point temperature of the reaction solution. The oxidative coupling occurs in the presence of a metal complex catalyst, and when the catalyst includes an amine ligand, the method facilitates incorporation of the amine ligand into the poly(arylene ether) resin. The amine-incorporated poly(arylene ether) resins prepared by the method are useful in the preparation of higher molecular weight poly(arylene ether) resins and compatibilized blends of poly(arylene ether) resins with other thermoplastics.
摘要翻译： 制备聚（亚芳基醚）的方法包括在超过反应溶液的浊点温度的反应温度下将反应溶液中的一元酚氧化偶联。 氧化偶联发生在金属络合物催化剂的存在下，当催化剂包括胺配体时，该方法便于将胺配体引入聚（亚芳基醚）树脂中。 通过该方法制备的加入胺的聚（亚芳基醚）树脂可用于制备高分子量聚（亚芳基醚）树脂和聚（亚芳基醚）树脂与其它热塑性塑料的相容混合物。
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2.发明授权Method of preparing a poly(arylene ether), and a poly(arylene ether) prepared thereby 有权制备聚（亚芳基醚）的方法和由其制备的聚（亚芳基醚）公开(公告)号：US06407200B1
公开(公告)日：2002-06-18
申请号：US09681895
申请日：2001-06-21
IPC分类号： C08G6538
摘要： A method of preparing a poly(arylene ether) includes oxidatively polymerizing a monohydric phenol in solution, concentrating the solution by removing a portion of the solvent to form a concentrated solution having a cloud point, Tcloud, and combining the concentrated solution with an anti-solvent to precipitate the poly (arylene ether), wherein the concentrated solution has a temperature of at least about (Tcloud−10° C.) immediately before it is combined with the anti-solvent. The method reduces the formation of undesirably fine particles in the product poly(arylene ether).
摘要翻译： 制备聚（亚芳基醚）的方法包括使溶液中的一元酚氧化聚合，通过除去溶剂的一部分浓缩溶液以形成具有浊点Tcloud的浓缩溶液，并将浓缩溶液与抗 - 溶剂以沉淀聚（亚芳基醚），其中浓缩溶液在其与抗溶剂组合之前具有至少约（Tcloud-10℃）的温度。 该方法减少了产物聚（亚芳基醚）中不期望的细颗粒的形成。
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3.发明授权Method of preparing a poly(arylene ether), and a poly(arylene ether) prepared thereby 有权制备聚（亚芳基醚）的方法和由其制备的聚（亚芳基醚）公开(公告)号：US06444779B1
公开(公告)日：2002-09-03
申请号：US09683806
申请日：2002-02-19
IPC分类号： C08G6538
摘要： A method of preparing a poly(arylene ether) includes oxidatively polymerizing a monohydric phenol in solution, concentrating the solution by removing a portion of the solvent to form a concentrated solution having a cloud point, Tcloud, adjusting the temperature of the concentrated solution to at least about (Tcloud−10° C.), and combining the concentrated solution with an anti-solvent to precipitate the poly (arylene ether). The method reduces the formation of undesirably fine particles in the product poly(arylene ether).
摘要翻译： 制备聚（亚芳基醚）的方法包括使溶液中的一元酚氧化聚合，通过除去一部分溶剂浓缩溶液，形成具有浊点的浓缩溶液Tcloud，将浓缩溶液的温度调节至 至少约（Tcloud-10℃），并将浓缩溶液与抗溶剂组合以沉淀聚（亚芳基醚）。 该方法减少了产物聚（亚芳基醚）中不期望的细颗粒的形成。
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公开(公告)号：US06469128B1
公开(公告)日：2002-10-22
申请号：US09682210
申请日：2001-08-07
IPC分类号： C08G6538
摘要： A process for producing a poly(arylene ether) resins includes oxidatively coupling a monohydric phenol in the presence of a solvent and a catalyst to form a soluble poly(arylene ether) and an insoluble poly(arylene ether), separating the soluble poly(arylene ether) and the insoluble poly(arylene ether), and recycling the soluble poly(arylene ether). The process is particularly useful for synthesizing poly(arylene ether) copolymers in which the monomer compositions of soluble and insoluble copolymers may vary.
摘要翻译： 一种制备聚（亚芳基醚）树脂的方法包括在溶剂和催化剂存在下使一元酚氧化偶合形成可溶性聚（亚芳基醚）和不溶性聚（亚芳基醚），将可溶性聚（亚芳基） 醚）和不溶性聚（亚芳基醚），并再循环可溶性聚（亚芳基醚）。 该方法对于合成其中可溶性和不溶性共聚物的单体组成可能变化的聚（亚芳基醚）共聚物特别有用。
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公开(公告)号：US06860966B2
公开(公告)日：2005-03-01
申请号：US10005934
申请日：2001-11-12
申请人： David Parrillo , Probjot Singh
发明人： David Parrillo , Probjot Singh
摘要： A method of removing substantially all solvent from a solution containing a polyphenylene ether polymer resin with little by-product formation (less than 250 ppm) is provided. The method employs a wiped thin film evaporator with a cylindrical heating chamber operating under conditions that satisfy the relationships defined by Equations I and II. 5.3*1024RLδ exp(−24123/T)/m
摘要翻译： 提供了从含有少量副产物形成的聚苯醚聚合物树脂（小于250ppm）的溶液中除去基本上所有溶剂的方法。 该方法采用具有圆柱形加热室的擦拭薄膜蒸发器，其工作条件满足方程式I和II定义的关系。最大化方式，其中进料速率（m）和固体百分比（C）的值被选择以提供最大值 根据方程m * C = Q确定的输出值Q，聚苯醚产物的熔体粘度在圆柱形加热室的工作温度下小于50,000厘泊。
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公开(公告)号：US08080156B2
公开(公告)日：2011-12-20
申请号：US12538606
申请日：2009-08-10
IPC分类号： C10G31/00
CPC分类号： C10G31/06 , C10G25/00 , C10G53/08 , C10G2300/201 , C10G2300/205
摘要： Methods and apparatus relate to removal of mercury from crude oil. Such removal relies on transferring mercury from a liquid hydrocarbon stream to a natural gas stream upon contacting the liquid hydrocarbon stream with the natural gas stream. Processing of the natural gas stream after used to strip the mercury from the liquid hydrocarbon stream removes the mercury from the natural gas stream.
摘要翻译： 方法和装置涉及从原油中去除汞。 这种去除依赖于在液体烃流与天然气流接触时将汞从液态烃流转移到天然气流中。 用于从液态烃流中除去汞后的天然气流的处理从天然气流中除去汞。
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公开(公告)号：US20100032344A1
公开(公告)日：2010-02-11
申请号：US12174816
申请日：2008-08-11
IPC分类号： C10G17/00
CPC分类号： C10G25/00 , B01D53/64 , B01D2256/24 , B01D2257/602 , B01D2259/401 , E21B43/34
摘要： A process for decreasing the level of elemental mercury contained in a crude oil at the well site by separating the crude oil stream into a gaseous hydrocarbon stream containing hydrocarbons, mercury and water, and a liquid hydrocarbon stream containing hydrocarbons and elemental mercury; removing mercury from the gaseous hydrocarbon stream in a mercury removal unit, thereby forming a treated gas stream; contacting a recycle gas stream comprising a portion of the treated gas stream with at least a portion of the liquid hydrocarbon stream for transfer of at least a portion of the elemental mercury contained in the liquid hydrocarbon stream to the recycle gas stream; thereby forming a mercury rich gas stream, and a treated liquid hydrocarbon stream; and passing the mercury rich gas stream, along with the gaseous hydrocarbon stream, to the mercury removal unit, is disclosed.
摘要翻译： 通过将原油流分离成含有烃，汞和水的气态烃流以及含有烃和元素汞的液态烃流，来降低井场中原油中含有的元素汞含量的方法; 在汞去除单元中从气态烃流中除去汞，从而形成经处理的气流; 使包含一部分经处理的气流的再循环气流与至少一部分液态烃流接触，以将液态烃流中所含的至少一部分元素汞转移至循环气流; 从而形成富含汞的气流和经处理的液态烃流; 并且将富汞气流与气态烃流一起传递到除汞单元。
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公开(公告)号：US20100032345A1
公开(公告)日：2010-02-11
申请号：US12538606
申请日：2009-08-10
IPC分类号： C10G31/00
CPC分类号： C10G31/06 , C10G25/00 , C10G53/08 , C10G2300/201 , C10G2300/205
摘要： Methods and apparatus relate to removal of mercury from crude oil. Such removal relies on transferring mercury from a liquid hydrocarbon stream to a natural gas stream upon contacting the liquid hydrocarbon stream with the natural gas stream. Processing of the natural gas stream after used to strip the mercury from the liquid hydrocarbon stream removes the mercury from the natural gas stream.
摘要翻译： 方法和装置涉及从原油中去除汞。 这种去除依赖于在液体烃流与天然气流接触时将汞从液态烃流转移到天然气流中。 用于从液态烃流中除去汞后的天然气流的处理从天然气流中除去汞。
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