Toners for use in electrophotography and production thereof
    2.
    发明授权
    Toners for use in electrophotography and production thereof 失效
    用于电子照相和其生产的调色剂

    公开(公告)号:US5328795A

    公开(公告)日:1994-07-12

    申请号:US501136

    申请日:1990-03-29

    IPC分类号: G03G9/08

    摘要: There is disclosed a method of producing a toner particles for use in electrophotography which comprises: suspending a radical polymerizable monomer which contains a colorant and a charge controlling agent therein in an aqueous phase; suspension polymerizing the monomer to provide spherical polymer particles of 1-30 .mu.m in diameter; treating the suspension containing the polymer particles with a continuous, wet type, agitation mill, to deform the polymer particles.A further method of producing toner particles is disclosed which comprises: producing spherical polymer particles by suspension polymerization of a monomer; making finely divided triboelectric or electroconductive particles or both onto the surface of the polymer particles; and then mechanically pressing the polymer particles to deform the polymer particles as well as to fix the particles on the surface of the polymer particles.A still further method of producing toner particles is disclosed which comprises: producing spherical polymer particles of 20-300 .mu.m in diameter by suspension polymerization of a monomer; and then crushing and classifying the polymer particles into toners of 1-30 .mu.m in size preferably after deforming the polymer particles.

    摘要翻译: 公开了一种生产用于电子照相术的调色剂颗粒的方法,包括:将含有着色剂的自由基聚合性单体和电荷控制剂悬浮在水相中; 悬浮聚合单体以提供直径为1-30μm的球形聚合物颗粒; 用连续的湿式搅拌机处理含有聚合物颗粒的悬浮液,使聚合物颗粒变形。 公开了制备调色剂颗粒的另一种方法,其包括:通过单体的悬浮聚合制备球形聚合物颗粒; 将精细分裂的摩擦电或导电颗粒或两者都制成聚合物颗粒的表面; 然后机械压制聚合物颗粒以使聚合物颗粒变形,并将颗粒固定在聚合物颗粒的表面上。 公开了制备调色剂颗粒的另一种方法,其包括:通过单体的悬浮聚合制备直径为20-300μm的球形聚合物颗粒; 然后将聚合物颗粒粉碎并分级成尺寸为1-30μm的调色剂,优选在使聚合物颗粒变形之后。

    Suspension polymerization process for producing electrophotographic
toners
    3.
    发明授权
    Suspension polymerization process for producing electrophotographic toners 失效
    用于生产电子照相色调剂的悬浮聚合方法

    公开(公告)号:US4904560A

    公开(公告)日:1990-02-27

    申请号:US212651

    申请日:1988-06-28

    IPC分类号: G03G9/08 G03G9/087

    摘要: A process for producing toners for use in electrophotography which comprises: stirring a mixture of a radical polymerizable liquid monomer and carbon black in the presence of a peroxide polymerization initiator, thereby to disperse the carbon black uniformly and minutely in the monomer; adding an azobisnitrile polymerization initiator to the resultant monomer composition; suspension polymerizing the monomer in an aqueous medium; and recovering and drying the resultant spherical polymer particles.In a preferred process, the suspension polymerization is carried out in an aqueous medium which contains polyvinyl alcohol as a suspending agent, and after the polymerization, the polyvinyl alcohol remaining on the polymer particles is saponified or nitrated to produce a toner with a higher quality.