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    3-AMINOMETHYL-1-CYCLOHEXYLAMINE, AND METHOD FOR THE PRODUCTION THEREOF
    1.
    发明申请
    3-AMINOMETHYL-1-CYCLOHEXYLAMINE, AND METHOD FOR THE PRODUCTION THEREOF 审中-公开
    3-氨基甲基-1-环己基氨基胺及其生产方法

    公开(公告)号：US20110124919A1

    公开(公告)日：2011-05-26

    申请号：US13055595

    申请日：2009-07-13

    申请人： Martin Ernst ,  Kirsten Dahmen ,  Alfred Oftring

    发明人： Martin Ernst ,  Kirsten Dahmen ,  Alfred Oftring

    IPC分类号： C07C211/49

    CPC分类号： C07C211/36 ,  C07B2200/09 ,  C07C2601/14

    摘要： The present invention relates to 3-aminomethyl-1-cyclohexylamine and to a process for preparation thereof by a) reacting cyclohexenone with hydrogen cyanide in the presence of a basic catalyst, b) reacting the cyclohexanonenitrile obtained in stage a) with ammonia in the presence of an imine formation catalyst, and c) reacting the 3-cyanocyclohexylimine-containing reaction mixture obtained in stage b) with hydrogen and ammonia over hydrogenation catalysts.The present invention further relates to the use of 3-aminomethyl-1-cyclohexylamine as a hardener for epoxy resins, as an intermediate in the preparation of diisocyanates, as a starter in the preparation of polyetherols and/or as a monomer for polyamide preparation.

    摘要翻译： 本发明涉及3-氨基甲基-1-环己基胺及其制备方法，其通过以下步骤a）使环己烯酮与氰化氢在碱性催化剂存在下反应，b）在步骤a）中得到的环己腈与氨在存在下反应 的亚胺形成催化剂，和c）使步骤b）中获得的含3-氰基环己基亚胺的反应混合物与氢气和氨在氢化催化剂上反应。 本发明还涉及3-氨基甲基-1-环己胺作为环氧树脂的硬化剂的用途，作为制备二异氰酸酯的中间体，作为制备聚乙烯醇和/或作为聚酰胺制备的单体的起始物。

    Method for producing ethylenediamine
    5.
    发明授权
    Method for producing ethylenediamine 有权
    乙二胺的制备方法

    公开(公告)号：US07915454B2

    公开(公告)日：2011-03-29

    申请号：US12529107

    申请日：2008-02-28

    申请人： Alfred Oftring ,  Kirsten Dahmen ,  Randolf Hugo ,  Thilo Hahn ,  Katrin Baumann ,  Johann-Peter Melder

    发明人： Alfred Oftring ,  Kirsten Dahmen ,  Randolf Hugo ,  Thilo Hahn ,  Katrin Baumann ,  Johann-Peter Melder

    IPC分类号： C07C209/48

    CPC分类号： C07C209/48 ,  C07C211/10

    摘要： The invention relates to a process for preparing ethylenediamine by hydrogenation of aminoacetonitrile over a catalyst, wherein the hydrogenation is carried out in a solution comprising aminoacetonitrile, water in a proportion of from 0 to 60% by weight and a solvent and the aminoacetonitrile comprised in the solution is fed into the reaction vessel at a rate which is not greater than the rate at which the aminoacetonitrile reacts with hydrogen in the hydrogenation.

    摘要翻译： 本发明涉及一种通过氨基乙腈在催化剂上氢化制备乙二胺的方法，其中氢化是在包含氨基乙腈的溶液中，以0至60重量％的比例的水和溶剂和包含在其中的氨基乙腈 溶液以不大于氨基乙腈在氢化中与氢反应的速率进料到反应容器中。

    Method for producing ethyleneamines from untreated AAN
    10.
    发明授权
    Method for producing ethyleneamines from untreated AAN 失效
    从未经处理的AAN生产乙撑胺的方法

    公开(公告)号：US07960590B2

    公开(公告)日：2011-06-14

    申请号：US12529101

    申请日：2008-02-28

    申请人： Kirsten Dahmen ,  Alfred Oftring ,  Randolf Hugo ,  Thilo Hahn ,  Katrin Baumann ,  Johann-Peter Melder

    发明人： Kirsten Dahmen ,  Alfred Oftring ,  Randolf Hugo ,  Thilo Hahn ,  Katrin Baumann ,  Johann-Peter Melder

    IPC分类号： C07C209/48

    CPC分类号： C07C209/48 ,  C07C211/10

    摘要： The invention relates to a process for preparing an ethylene amine mixture, which comprises the following steps: a) crude AAN which is largely free of formaldehyde cyanohydrin (largely FACH-free) is heated at a temperature of from 50 to 150° C. to give an amino nitrile mixture comprising aminoacetonitrile (AAN) and from 5 to 70% by weight of iminodiacetonitrile (DAN), b) hydrogenation of the amino nitrile mixture obtained in step a) in the presence of a catalyst. Ethylenediamine (EDA) and/or diethylenetriamine (DETA) and also, if appropriate, further ethylene amines can be isolated from the ethylene amine mixtures obtained.

    摘要翻译： 本发明涉及一种制备乙烯胺混合物的方法，其包括以下步骤：a）将大部分不含甲醛氰醇（基本上不含FACH的）的粗AAN在50至150℃的温度下加热至 得到包含氨基乙腈（AAN）和5-70重量％亚氨基二乙腈（DAN）的氨基腈混合物，b）在催化剂存在下氢化步骤a）中得到的氨基腈混合物。 乙二胺（EDA）和/或二亚乙基三胺（DETA）以及如果合适的话，还可以从获得的乙烯胺混合物中分离另外的亚乙基胺。