公开(公告)号：US20080132722A1

公开(公告)日：2008-06-05

申请号：US10586065

申请日：2005-01-13

申请人： Massimo Morbidelli ,  Marco Mazzotti ,  Adalbert Prior ,  Joachim Prior ,  Frank Lang

发明人： Massimo Morbidelli ,  Marco Mazzotti ,  Adalbert Prior ,  Joachim Prior ,  Frank Lang

IPC分类号： C07C69/34 ,  B01D15/08 ,  C07C39/16

CPC分类号： B01D15/1892 ,  B01J8/0257 ,  B01J8/0285 ,  B01J2208/00212 ,  Y02P20/582

摘要： Disclosed is a method for producing at least one chemical reaction product by chemically reacting one or several reactants that is/are optionally dissolved in one or several solvents and is/are supplied as a feed stream by bringing the same in contact with a heterogeneous catalyst in a continuously operated fixed-bed reactor which is filled with a particle bed, a continuous annular chromatograph (CAC) that is filled with the particle bed being used as a fixed-bed reaction in which the at least one reaction product is formed and purified while the at least one purified reaction product as well as optionally provided secondary products and/or non-reacted reactants are withdrawn at a different, predetermined azimuthal position of the annular chromatograph, respectively. The inventive method is characterized in that only one type of particle material is used in a single particle bed as both a formation catalyst and a chromatographic medium for purifying the at least one reaction product in the particle bed.

摘要翻译： 公开了一种通过化学反应一种或几种反应物来生产至少一种化学反应产物的方法，所述反应物任选地溶解在一种或多种溶剂中，并通过使其与非均相催化剂接触而作为进料流供给 用颗粒床填充的连续操作的固定床反应器，填充有颗粒床的连续环状色谱仪（CAC），其用作固定床反应，其中形成和纯化至少一种反应产物，同时 分别在环状色谱仪的不同的预定方位位置取出至少一种纯化的反应产物以及任选提供的第二产物和/或未反应的反应物。 本发明的方法的特征在于，在单颗粒床中仅使用一种类型的颗粒材料作为地层催化剂和用于纯化颗粒床中的至少一种反应产物的色谱介质。

公开(公告)号：US07686958B2

公开(公告)日：2010-03-30

申请号：US10586065

申请日：2005-01-13

申请人： Massimo Morbidelli ,  Marco Mazzotti ,  Adalbert Prior ,  Joachim Prior ,  Frank Lang

发明人： Massimo Morbidelli ,  Marco Mazzotti ,  Adalbert Prior ,  Joachim Prior ,  Frank Lang

IPC分类号： B01D15/08 ,  C07C39/16

CPC分类号： B01D15/1892 ,  B01J8/0257 ,  B01J8/0285 ,  B01J2208/00212 ,  Y02P20/582

摘要： Disclosed is a method for producing at least one chemical reaction product by chemically reacting one or several reactants that is/are optionally dissolved in one or several solvents and is/are supplied as a feed stream by bringing the same in contact with a heterogeneous catalyst in a continuously operated fixed-bed reactor which is filled with a particle bed, a continuous annular chromatograph (CAC) that is filled with the particle bed being used as a fixed-bed reaction in which the at least one reaction product is formed and purified while the at least one purified reaction product as well as optionally provided secondary products and/or non-reacted reactants are withdrawn at a different, predetermined azimuthal position of the annular chromatograph, respectively. The inventive method is characterized in that only one type of particle material is used in a single particle bed as both a formation catalyst and a chromatographic medium for purifying the at least one reaction product in the particle bed.

摘要翻译： 公开了一种通过化学反应一种或几种反应物来生产至少一种化学反应产物的方法，所述反应物任选地溶解在一种或多种溶剂中，并通过使其与非均相催化剂接触而作为进料流供给 用颗粒床填充的连续操作的固定床反应器，填充有颗粒床的连续环状色谱仪（CAC），其用作固定床反应，其中形成和纯化至少一种反应产物，同时 分别在环状色谱仪的不同的预定方位位置取出至少一种纯化的反应产物以及任选提供的第二产物和/或未反应的反应物。 本发明的方法的特征在于，在单颗粒床中仅使用一种类型的颗粒材料作为地层催化剂和用于纯化颗粒床中的至少一种反应产物的色谱介质。