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公开(公告)号:US20200062657A1
公开(公告)日:2020-02-27
申请号:US16466066
申请日:2017-05-10
Applicant: Nanjing University of Technology
Inventor: Wanqin JIN , Jiawei ZHU , Zhengkun LIU
IPC: C04B35/622 , C04B35/26 , C04B26/28 , C04B26/10
Abstract: The invention relates to a method for preparing a composite metal oxide hollow fibre. A certain stoichiometry of composite metal oxide raw material and a polymer binding agent are added to an organic solvent, and mixed mechanically to obtain an evenly dispersed spinning solution having a suitable viscosity. After defoaming treatment, the spinning solution is extruded through a spinneret and, after undergoing a certain dry spinning process, enters an external coagulation bath; during this period, a phase inversion process occurs and composite metal oxide hollow fibre blanks are formed. The blanks are immersed in the external coagulation bath and the organic solvent is displaced; after natural drying, the blanks undergo a heat treatment process; during this period, polymer burn off, in situ reaction, and in situ sintering processes occur to obtain the composite metal oxide hollow fibre.