公开(公告)号：US20150162634A1

公开(公告)日：2015-06-11

申请号：US14622644

申请日：2015-02-13

Applicant: National Central University

Inventor： Sheng-Wei LEE ,  Kan-Rong LEE ,  Jing-Chie LIN ,  Chuan LI ,  Chung-Jen TSENG ,  Jeng-Kuei CHANG ,  Shian-Ching JANG ,  I-Ming HUNG ,  Chi-Shiung HSI ,  Sheng-Long LEE ,  Yen-Jiun CHIANG ,  Yu-Shuo HUANG

IPC: H01M8/12 ,  C04B35/64 ,  C04B35/01 ,  C04B35/624

CPC classification number: H01M8/1246 ,  C04B35/01 ,  C04B35/624 ,  C04B35/64 ,  H01M8/1253 ,  H01M8/126 ,  H01M2008/1293 ,  H01M2300/0074 ,  H01M2300/0077 ,  Y02E60/525 ,  Y02P70/56

Abstract: The preparation method of electrolytes provided by the present invention involves applications of a first solid oxide powder and a second solid oxide powder, both of which are prepared by using a sol-gel process and a calcination process. Each of the first and second solid oxide powders is a Perovskite-type oxide. After the first and second solid oxide powders are readily mixed, they are compressed into a pellet and then sintered to prepare the afore-mentioned electrolytes for SOFC. It is found in the present invention that by mixing and compressing different solid oxide powders, the solid oxide powder having smaller particle size can fill into the gaps of the other solid oxide powder. After the pellet is sintered, the density of the product is significantly improved.

Abstract translation: 由本发明提供的电解质的制备方法涉及第一固体氧化物粉末和第二固体氧化物粉末的应用，二者均通过使用溶胶 - 凝胶法和煅烧法制备。 第一固体氧化物粉末和第二固体氧化物粉末都是钙钛矿型氧化物。 在第一和第二固体氧化物粉末容易混合之后，将它们压制成颗粒，然后烧结以制备上述用于SOFC的电解质。 在本发明中发现，通过混合和压缩不同的固体氧化物粉末，具有较小粒度的固体氧化物粉末可以填充到另一种固体氧化物粉末的间隙中。 颗粒烧结后，产品的密度显着提高。