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公开(公告)号：US20160052946A1
公开(公告)日：2016-02-25
申请号：US14888802
申请日：2014-04-30
申请人： PETHMARK AB
摘要： The present invention discloses a composition comprising a compound of formula I and a deuterated solvent. The deuterated solvent is miscible with water in any proportion at a temperature of 20 to 25° C. and comprises less than 5% residual 1H-isotopes. The concentration of the compound of formula I may advantageously be determined by 1H-QNMR. Methods of production of the composition and salts of compounds of formula I, as well as related analogs and novel reagents and intermediates for the production thereof, are also described.
摘要翻译： 本发明公开了包含式I化合物和氘代溶剂的组合物。 氘代溶剂在20至25℃的温度下以任何比例与水混溶，并且包含少于5％的残余1H-同位素。 式I化合物的浓度可有利地由1H-QNMR确定。 还描述了制备式I化合物的组合物和盐的方法，以及相关的类似物和新的试剂及其生产中间体。
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公开(公告)号：US09499572B2
公开(公告)日：2016-11-22
申请号：US14888802
申请日：2014-04-30
申请人： Pethmark AB
摘要： The present invention discloses a composition comprising a compound of formula I and a deuterated solvent. The deuterated solvent is miscible with water in any proportion at a temperature of 20 to 25° C. and comprises less than 5% residual 1H-isotopes. The concentration of the compound of formula I may advantageously be determined by 1H-QNMR. Methods of production of the composition and salts of compounds of formula I, as well as related analogs and novel reagents and intermediates for the production thereof, are also described.
摘要翻译： 本发明公开了包含式I化合物和氘代溶剂的组合物。 氘代溶剂在20至25℃的温度下以任何比例与水混溶，并且包含小于5％的残余1H-同位素。 式I化合物的浓度可有利地由1H-QNMR确定。 还描述了制备式I化合物的组合物和盐的方法，以及相关的类似物和新的试剂及其生产中间体。
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公开(公告)号：US20170052132A1
公开(公告)日：2017-02-23
申请号：US15251764
申请日：2016-08-30
申请人： Pethmark AB
IPC分类号： G01N24/08
CPC分类号： G01N24/08
摘要： The present invention discloses a composition comprising a compound of formula I and a deuterated solvent. The deuterated solvent is miscible with water in any proportion at a temperature of 20 to 25° C. and comprises less than 5% residual 1H-isotopes. The concentration of the compound of formula I may advantageously be determined by 1H-QNMR. Methods of production of the composition and salts of compounds of formula 1, as well as related analogs and novel reagents and intermediates for the production thereof, are also described.
摘要翻译： 本发明公开了包含式I化合物和氘代溶剂的组合物。 氘代溶剂在20至25℃的温度下以任何比例与水混溶，并且包含少于5％的残余1H-同位素。 式I化合物的浓度可有利地由1H-QNMR确定。 还描述了制备式1化合物的组合物和盐的方法，以及相关的类似物和新的试剂及其生产中间体。
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