公开(公告)号：US20100284901A1

公开(公告)日：2010-11-11

申请号：US12811664

申请日：2009-03-06

申请人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Tae Hee Shin ,  Deok Yun Kim ,  Sun Ki Seo ,  Rae Sung Chung ,  Do Sun Baik

发明人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Tae Hee Shin ,  Deok Yun Kim ,  Sun Ki Seo ,  Rae Sung Chung ,  Do Sun Baik

IPC分类号： C01B15/023 ,  C09K3/00

CPC分类号： C01B15/023

摘要： The present invention relates to a method for the preparation of hydrogen peroxide through a continuous process, extracting hydrogen peroxide produced from reduction and oxidation of a working solution and recycling the oxidized working solution back to the reduction process, wherein the composition of the working solution, i.e. the composition of 2-alkylanthraquinone and 2-tetrahydroalkylanthraquinone, is optimized to increase the solubility of the quinones and to improve the reaction rate. The working solution comprises 2-alkylanthraquinone, 2-tetrahydroalkylanthraquinone and an organic solvent, wherein 65-95 mol % of the alkyl group of 2-alkylanthraquinone and 2-tetrahydroalkylanthraquinone is amyl and the remaining 5-35 mol % of the alkyl group is ethyl, and the molar ratio of 2-alkylanthraquinone to 2-tetrahydroalkylanthraquinone is from 4:6 to 1:9.

摘要翻译： 本发明涉及通过连续方法制备过氧化氢的方法，提取由还原和氧化工作溶液产生的过氧化氢，并将氧化的工作溶液再循环回还原过程，其中工作溶液的组成， 即2-烷基蒽醌和2-四氢烷基蒽醌的组成被优化以增加醌的溶解度并提高反应速率。 工作溶液包括2-烷基蒽醌，2-四氢烷基蒽醌和有机溶剂，其中65-95摩尔％的2-烷基蒽醌和2-四氢烷基蒽醌的烷基是戊基，剩余的5-35摩尔％的烷基是乙基 ，2-烷基蒽醌与2-四氢烷基蒽醌的摩尔比为4：6〜1：9。

公开(公告)号：US08158100B2

公开(公告)日：2012-04-17

申请号：US12811664

申请日：2009-03-06

申请人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Tae Hee Shin ,  Deok Yun Kim ,  Sun Ki Seo ,  Rae Sung Chung ,  Do Sun Baik

发明人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Tae Hee Shin ,  Deok Yun Kim ,  Sun Ki Seo ,  Rae Sung Chung ,  Do Sun Baik

IPC分类号： C01B15/023

CPC分类号： C01B15/023

摘要： The present invention relates to a method for the preparation of hydrogen peroxide through a continuous process, extracting hydrogen peroxide produced from reduction and oxidation of a working solution and recycling the oxidized working solution back to the reduction process, wherein the composition of the working solution, i.e. the composition of 2-alkylanthraquinone and 2-tetrahydroalkylanthraquinone, is optimized to increase the solubility of the quinones and to improve the reaction rate. The working solution comprises 2-alkylanthraquinone, 2-tetrahydroalkylanthraquinone and an organic solvent, wherein 65-95 mol % of the alkyl group of 2-alkylanthraquinone and 2-tetrahydroalkylanthraquinone is amyl and the remaining 5-35 mol % of the alkyl group is ethyl, and the molar ratio of 2-alkylanthraquinone to 2-tetrahydroalkylanthraquinone is from 4:6 to 1:9.

摘要翻译： 本发明涉及通过连续方法制备过氧化氢的方法，提取由还原和氧化工作溶液产生的过氧化氢，并将氧化的工作溶液再循环回还原过程，其中工作溶液的组成， 即2-烷基蒽醌和2-四氢烷基蒽醌的组成被优化以增加醌的溶解度并提高反应速率。 工作溶液包括2-烷基蒽醌，2-四氢烷基蒽醌和有机溶剂，其中65-95摩尔％的2-烷基蒽醌和2-四氢烷基蒽醌的烷基是戊基，剩余的5-35摩尔％的烷基是乙基 ，2-烷基蒽醌与2-四氢烷基蒽醌的摩尔比为4：6〜1：9。

公开(公告)号：US08877091B2

公开(公告)日：2014-11-04

申请号：US11993622

申请日：2005-09-23

申请人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Young Ran Lee

发明人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Young Ran Lee

IPC分类号： A62D3/00 ,  A62D9/00 ,  C01B15/00 ,  C01B15/12 ,  C09K3/00 ,  D06L3/00 ,  D06L3/02 ,  D06L3/04 ,  C11D3/02 ,  C11D7/42 ,  C11D17/00 ,  C11D13/00 ,  C11D3/00 ,  C11D3/386 ,  C11D7/00 ,  C11D1/00 ,  C11D10/00 ,  C11D3/43 ,  D06L1/04 ,  C11D3/39 ,  C11D1/83

CPC分类号： D06L1/04 ,  C11D1/83 ,  C11D3/3947 ,  C11D3/43 ,  C11D17/0013 ,  D06L4/12 ,  D06L4/15 ,  D06L4/17

摘要： This invention relates to a novel non-aqueous liquid oxygen bleach composition prepared by dispersing solid peroxygen compound in the liquid in which the content of an anhydrous non-polar organic solvent and a non-ionic and anionic surfactant is controlled. The composition is formed in a high viscous paste or a gel-type suspension and can be used as a multi-purpose composition, for example, the bleach and stain remover of clothes and the cleanser of bathroom and kitchen since they have a chemical/physical stability of no loss of available oxygen, an excellent bleaching and cleaning ability due to their alkaline pH range, no change of viscosity or no phase separation during the storage and so on.

摘要翻译： 本发明涉及通过将固体过氧化合物分散在其中控制无水非极性有机溶剂和非离子和阴离子表面活性剂的含量的液体中制备的新型非水液氧漂白组合物。 该组合物形成为高粘度糊状物或凝胶型悬浮液，并且可以用作多用途组合物，例如衣物的漂白和去污剂以及浴室和厨房的清洁剂，因为它们具有化学/物理 稳定性不损失可用氧气，由于其碱性pH范围，优异的漂白和清洁能力，粘度无变化或储存期间无相分离等优点。

公开(公告)号：US20100155659A1

公开(公告)日：2010-06-24

申请号：US11993622

申请日：2005-09-23

申请人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Young Ran Lee

发明人： Se In Yang ,  Kyung Keun Yoo ,  Yong Il Kim ,  Young Ran Lee

IPC分类号： D06L3/02

CPC分类号： D06L1/04 ,  C11D1/83 ,  C11D3/3947 ,  C11D3/43 ,  C11D17/0013 ,  D06L4/12 ,  D06L4/15 ,  D06L4/17

摘要： This invention relates to a novel non-aqueous liquid oxygen bleach composition prepared by dispersing solid peroxygen compound in the liquid in which the content of an anhydrous non-polar organic solvent and a non-ionic and anionic surfactant is controlled. The composition is formed in a high viscous paste or a gel-type suspension and can be used as a multi-purpose composition, for example, the bleach and stain remover of clothes and the cleanser of bathroom and kitchen since they have a chemical/physical stability of no loss of available oxygen, an excellent bleaching and cleaning ability due to their alkaline pH range, no change of viscosity or no phase separation during the storage and so on.

摘要翻译： 本发明涉及通过将固体过氧化合物分散在其中控制无水非极性有机溶剂和非离子和阴离子表面活性剂的含量的液体中制备的新型非水液氧漂白组合物。 该组合物形成为高粘度糊状物或凝胶型悬浮液，并且可以用作多用途组合物，例如衣物的漂白和去污剂以及浴室和厨房的清洁剂，因为它们具有化学/物理 稳定性不损失可用氧气，由于其碱性pH范围，优异的漂白和清洁能力，粘度无变化或储存期间无相分离等优点。