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公开(公告)号：US06566520B2
公开(公告)日：2003-05-20
申请号：US09291524
申请日：1999-04-14
IPC分类号： C07D40100
CPC分类号： C12N15/8297 , C07C69/00 , C07C2603/00 , C07D215/56
摘要： A method for the preparation and purification of compounds using a novel support, a tetrabenzo [a, c, g, i]-fluorene group (Tbf) comprising reacting a building block (A) containing a Tbf group (Tbf-A), with a second building block (B), to afford an intermediate compound (Tbg-A-B) followed by purifying the intermediate compound by adsorption on a carbon support, removing the intermediate compound from the support with a solvent and repeating the previous reactions using the required number of building blocks to synthesize the compounds followed by removal of the Tbf group to afford the desired compounds.
摘要翻译： 使用新型载体四丁苯并[a，c，g，i] - 芴基（Tbf）制备和纯化化合物的方法，包括使含有Tbf基团（Tbf-A）的结构单元（A）与 第二构建块（B），得到中间体化合物（Tbg-AB），然后通过在碳载体上吸附纯化中间体化合物，用溶剂从载体中除去中间体化合物，并使用所需数量重复以前的反应 的组合物合成化合物，然后除去Tbf基团，得到所需化合物。
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公开(公告)号：US5977400A
公开(公告)日：1999-11-02
申请号：US48166
申请日：1998-03-25
IPC分类号： C07C69/00 , C07D215/56 , C12N15/82 , C07C69/76 , C07D215/16 , C07D401/00
CPC分类号： C12N15/8297 , C07C69/00 , C07D215/56 , C07C2103/00
摘要： A method for the preparation and purification of compounds using a novel support, a tetrabenzo[a,c,g,i]fluorene group (Tbf) comprising reacting a building block (A) containing a Tbf group (Tbf-A), with a second building block (B), to afford an intermediate compound (Tbg-A-B) followed by purifying the intermediate compound by adsorption on a carbon support, removing the intermediate compound from the support with a solvent and repeating the previous reactions using the required number of building blocks to synthesize the compounds followed by removal of the Tbf group to afford the desired compounds.
摘要翻译： 一种使用新型载体，四苯并[a，c，g，i]芴基（Tbf）制备和纯化化合物的方法，包括使含有Tbf基团（Tbf-A）的结构单元（A）与 第二组合物（B），得到中间体化合物（Tbg-AB），然后通过在碳载体上吸附纯化中间体化合物，用溶剂从载体中除去中间体化合物，并使用所需数量的 合成化合物，然后除去Tbf基团，得到所需化合物。
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