公开(公告)号：US07611548B2

公开(公告)日：2009-11-03

申请号：US10660715

申请日：2003-09-12

申请人： Shyue-Ming Jang ,  Sheng Yang ,  Bang-I Liou ,  Jun-Yi Chen ,  Long-Shuenn Jean ,  Chun-Te Tsai ,  Chiu-Tung Huang

发明人： Shyue-Ming Jang ,  Sheng Yang ,  Bang-I Liou ,  Jun-Yi Chen ,  Long-Shuenn Jean ,  Chun-Te Tsai ,  Chiu-Tung Huang

IPC分类号： B01D7/00

CPC分类号： B01D7/00

摘要： A vertical and a horizontal vacuum sublimation apparatus with high efficiency and processes thereof are provided, especially for the materials with high melting point and low vapor pressure. The vertical sublimation purification apparatus comprises a sublimation channel body, a material rack, a heating evaporation device, a condensation device, an incubating device, and a product scratching device. The horizontal sublimation purification apparatus comprises a sublimation channel body, a material carrier, a heating evaporation device, and two end pipes. The apparatuses of the present invention can be applied to the mass production of high purity chemicals, and are capable of sublimating and purifying OLED illumination layer materials including Alq3, NPB and CuPc, which have high melting temperature and low vapor pressure.

摘要翻译： 提供了一种高效率的垂直和水平真空升华装置及其工艺，特别是对于具有高熔点和低蒸气压的材料。 垂直升华净化装置包括升华通道体，材料架，加热蒸发装置，冷凝装置，孵育装置和产品刮擦装置。 水平升华净化装置包括升华通道体，材料载体，加热蒸发装置和两个端部管。 本发明的装置可以应用于大量生产高纯度化学品，并且能够升华和净化具有高熔点温度和低蒸气压的Alq3，NPB和CuPc的OLED照明层材料。

公开(公告)号：US20050047979A1

公开(公告)日：2005-03-03

申请号：US10660715

申请日：2003-09-12

申请人： Shyue-Ming Jang ,  Sheng Yang ,  Bang-I Liou ,  Jun-Yi Chen ,  Long-Shuenn Jean ,  Chun-Te Tsai ,  Chiu-Tung Huang

发明人： Shyue-Ming Jang ,  Sheng Yang ,  Bang-I Liou ,  Jun-Yi Chen ,  Long-Shuenn Jean ,  Chun-Te Tsai ,  Chiu-Tung Huang

IPC分类号： B01D7/00 ,  B01D7/02

CPC分类号： B01D7/00

摘要： A vertical and a horizontal vacuum sublimation apparatus with high efficiency and processes thereof are provided, especially for the materials having high melting point and low vapor pressure. The vertical sublimation purification apparatus comprises a sublimation channel body, a material rack, a heating evaporation device, a condensation device, an incubating device and a product scratching device. The horizontal sublimation purification apparatus comprises a sublimation channel body, a material carrier, a heating evaporation device and two end pipes. The apparatuses of the present invention can be applied on high purity chemicals from mass production, and are capable of sublimating and purifying OLED illumination layer materials including ALq3, NPB and CuPc, which have high melting temperature and low vapor pressure.

摘要翻译： 提供了一种高效率的垂直和水平真空升华装置及其工艺，特别是对于具有高熔点和低蒸气压的材料。 垂直升华净化装置包括升华通道体，材料架，加热蒸发装置，冷凝装置，孵育装置和产品刮擦装置。 水平升华净化装置包括升华通道体，材料载体，加热蒸发装置和两个端部管。 本发明的装置可以应用于批量生产的高纯度化学品，并且能够升华和净化具有高熔点温度和低蒸气压的ALQ3，NPB和CuPc的OLED照明层材料。