Cellulose acetates and process for producing the cellulose acetates
    1.
    发明授权
    Cellulose acetates and process for producing the cellulose acetates 有权
    乙酸纤维素和乙酸纤维素的生产方法

    公开(公告)号:US06803458B2

    公开(公告)日:2004-10-12

    申请号:US10239628

    申请日:2002-09-20

    IPC分类号: C08B306

    CPC分类号: C08B3/06

    摘要: The present invention provides a cellulose acetate satisfying at least one requirement selected from the following requirements (A), (B) and (C), provided that the case where (B) alone is satisfied is excluded. Requirement (A): Bright spotty matters in sizes of 20 &mgr;m or more are not more than 20 units/mm3. Requirement (B): Blocking constant (K) is not more than 60. Requirement (C): The ratio (G′/G″) of storage modulus (G′) to loss modulus (G″) at a measuring frequency of 0.016 Hz is not more than 0.2.

    摘要翻译: 本发明提供满足以下要求(A),(B)和(C)中至少一个要求的乙酸纤维素乙酸酯,只要满足(B)的情况即被排除。要求(A):亮点 尺寸为20um或更大的物质不超过20单位/ mm 3。要求(B):阻塞常数(K)不大于60.要求(C):比例(G'/ G“ 在0.016Hz的测量频率下的储能模量(G')与损耗模量(G“)不大于0.2。

    Cellulose triacetates and methods for producing the cellulose triacetates
    2.
    发明授权
    Cellulose triacetates and methods for producing the cellulose triacetates 有权
    三乙酸纤维素和纤维素三乙酸酯的制备方法

    公开(公告)号:US06683174B1

    公开(公告)日:2004-01-27

    申请号:US09831454

    申请日:2001-05-08

    IPC分类号: C08B306

    CPC分类号: C08B3/06

    摘要: The present invention provides a cellulose triacetate which exhibits a satisfactory filtration performance Thus, the present invention provides a cellulose triacetate whose occlusion constant (K) determined by the following method is 70 or less. Method: the cellulose triacetate is dissolved in a solvent mixture of methylene chloride/methanol (9/1 w/w) to form a 16% by weight (as a solid concentration) solution, which is then filtered under a constant pressure at the filtration pressure of 3 kg/cm2 and the temperature of 25° C. using a muslin filter to determine a filtered volume with the lapse of time, from which the slope of a linear curve represented by t/V−t (wherein t is a filtration time (sec) and V is a filtered volume (ml)) is calculated to obtain an occlusion constant (K) where K=slope×2×104.

    摘要翻译: 本发明提供一种显示出令人满意的过滤性能的三醋酸纤维素。因此,本发明提供一种三乙酸纤维素,其通过以下方法确定的遮蔽常数(K)为70以下。 方法:将三乙酸纤维素溶解在二氯甲烷/甲醇(9/1w / w)的溶剂混合物中以形成16重量%(作为固体浓度)溶液,然后在恒定压力下过滤 压力为3kg / cm 2,温度为25℃,用棉布过滤器确定过滤体积随时间的推移,由t / Vt表示的线性曲线的斜率(其中t为 计算过滤时间(秒),V为过滤体积(ml)),得到K = slopeex2×10 4的遮蔽常数(K)。