公开(公告)号：US11612936B2

公开(公告)日：2023-03-28

申请号：US17275198

申请日：2020-03-27

Applicant: University of Science and Technology Beijing

Inventor： Fang Yang ,  Yanru Shao ,  Yang Zhou ,  Zhimeng Guo ,  Yanli Sui ,  Qian Qin ,  Cunguang Chen

IPC: B22F9/30 ,  B22F3/16 ,  C23C16/08 ,  C23C16/442 ,  C23C16/448 ,  B22F1/16 ,  B22F1/145 ,  B33Y10/00 ,  B33Y70/00

Abstract: A method for preparing an oxygen-free passivated titanium or titanium-alloy powder product by means of gas-solid fluidization is provided. The new method includes placing the metal halide and the titanium powder which meet formula requirements into a gasifier and a fluidized bed reactor respectively; heating the gasifier to gasify the metal halide, and introducing dry argon and halide gas into the fluidized bed reactor; opening the fluidized bed, heating the fluidized bed, fluidizing the titanium powder after the introduction of the argon and the metal halide gas, and cooling the product to obtain the titanium powder subjected to oxygen-free passivation using metal chloride; molding the oxygen-free passivated titanium powder into a green body with powder metallurgy technology; and sintering the green body in vacuum or argon atmosphere according to the molding technology, and after temperature rise treatment, performing a densification sintering operation to obtain a high-performance titanium product component.