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    Non-uniformly substituted phthalocyanine compositions preparation methods, and electrophotographic elements
    2.
    发明授权
    Non-uniformly substituted phthalocyanine compositions preparation methods, and electrophotographic elements 失效
    非均匀取代的酞菁组合物制备方法和电子照相元件

    公开(公告)号：US5773181A

    公开(公告)日：1998-06-30

    申请号：US448056

    申请日：1995-05-23

    申请人： Michel F. Molaire ,  Jeanne Ellen Kaeding ,  William Tod Gruenbaum

    发明人： Michel F. Molaire ,  Jeanne Ellen Kaeding ,  William Tod Gruenbaum

    IPC分类号： C09B67/04 ,  C09B67/12 ,  C09B67/22 ,  C09B67/50 ,  G03G5/06

    CPC分类号： C09B67/0026 ,  C09B67/0002 ,  C09B67/0016 ,  C09B67/0035 ,  G03G5/0696

    摘要： Phthalocyanine compositions and prepartion methods. In a method, first, a phthalocyanine mixture is synthesized that has a plurality of differently substituted phthalocyanines selected from the group consisting of compounds having the general structure: ##STR1## M represents a pair of hydrogen atoms or a covalent or coordinate bonded moiety including a metal atom. Each T substituent is independently selected from the group consisting of H, F, Cl, Br, I, and alkyl having from 1 to 18 carbons. There are at least two different T substituents. The smallest T substituent has a van der Waal's radius that differs from the radius of the largest T substituent by less than about 50 percent of the radius of the smallest substituent. The amorphousness of the phthalocyanine mixture is then imcreased. The amorphous mixture is then contacted with organic solvent having a gamma.sub.c hydrogen bonding parameter of less than 8.0. Prior to the contacting, the amorphous mixture is excluded from contact with organic solvent having a gamma.sub.c hydrogen bonding parameter greater than 9.0.

    摘要翻译： 酞菁组合物和制备方法。 在一种方法中，首先，合成具有多个不同取代的酞菁的酞菁混合物，其选自具有以下通式结构的化合物：M表示一对氢原子或共价键或键合部分，包括 金属原子。 每个T取代基独立地选自H，F，Cl，Br，I和具有1至18个碳的烷基。 存在至少两个不同的T取代基。 最小的T取代基具有与最大T取代基的半径不同的范德华半径小于最小取代基半径的约50％。 然后增加酞菁混合物的无定形性。 然后将无定形混合物与具有小于8.0的gammac氢键参数的有机溶剂接触。 在接触之前，将无定形混合物排除与具有大于9.0的gammac氢键参数的有机溶剂的接触。