摘要:
A process for preparing isoflurane (1-chloro-2,2,2-trifluoroethyl difluoromethyl ether) by reacting PFE (2,2,2-trifluoroethyl difluoromethyl ether) with chlorine in the presence of ultraviolet light and added water, at a low temperature and/or at a high conversion.
摘要:
The invention provides a process for the preparation of fluorinated alkanesulfonic acid anhydrides by contacting alkanesulfonic acids with phosphorus pentoxide, the phosphorus pentoxide being provided as a dispersion in an inert oil. The invention also provides novel fluorinated alkanesulfonic acid anhydrides including 2-hydrotetrafluoroethanesulfonic acid anhydride.
摘要:
A process for the production of trialkylsilyl (fluorosulfonyl)difluoroacetate by contacting (fluorosulfonyl)difluoroacetyl fluoride with siloxane. The amount of (fluorosulfonyl)difluoroacetic acid by-product in trialkylsilyl(fluorosulfonyl)difluoroacetate is reduced by contacting said mixture with trialkylsilyl halide.
摘要:
A process for preparing hexafluoroacetone comprising the reaction of 2-chloro-1,1,1,3,3,3-hexafluoropropane [R226da] with oxygen in the presence of actinic light.
摘要:
A grease made by combining polychlorotrifluoroethylene oil with a thickening agent comprising polychlorotrifluoroethylene (PCTFE) polymer. The thickening agent is made by polymerizing chlorotrifluoroethylene [R-1113] in the presence of a telogen, which is 2,2-dichloro-1,1,1-trifluoroethane[R-123] or a homolog thereof, namely CF3—CF2—CHCl2, CF3—CF2—CF2—CHCl2, and CF3—CF2—CF2—CF2—CHCl2.
摘要:
A process for the production of trialkylsilyl (fluorosulfonyl)difluoroacetate by contacting (fluorosulfonyl)difluoroacetyl fluoride with siloxane. The amount of (fluorosulfonyl)difluoroacetic acid by-product in trialkylsilyl(fluorosulfonyl)difluoroacetate is reduced by contacting said mixture with trialkylsilyl halide.
摘要:
In a fire extinguisher containing a halogenated hydrocarbon extinguishant, the improvement wherein said extinguishant comprises at least one of 2-bromo-1,1,1,2-tetrafluoroethane and 2-bromo-2-chloro-1,1,1-trifluoroethane. These compounds will eventually decompose in the atmosphere so as not to present a hazard to the ozone layer.