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    PROCESS FOR PREPARING SUBSTITUTED PYRIDONE COMPOUNDS
    3.
    发明申请
    PROCESS FOR PREPARING SUBSTITUTED PYRIDONE COMPOUNDS 有权
    制备取代的吡咯烷酮化合物的方法

    公开(公告)号：US20040006234A1

    公开(公告)日：2004-01-08

    申请号：US10185597

    申请日：2002-06-27

    Applicant: Xerox Corporation

    Inventor： James D. Mayo ,  James M. Duff ,  Rina Carlini ,  Roger E. Gaynor ,  George Liebermann

    IPC: C07D213/08 ,  C07D211/84

    CPC classification number: C07D213/69 ,  C07D213/85 ,  Y10S534/02

    Abstract: Disclosed is a process for preparing substituted pyridone compounds which comprises (a) admixing in the absence of a solvent (1) an amine of the formula R1nullNH2 wherein R1 is an alkyl group, an aryl group, an arylalkyl group, or an alkylaryl group, and (2) a first ester of the formula 1 wherein R2 is an electron withdrawing group and R3 is an alkyl group; (b) heating the mixture containing the amine and the first ester to form an intermediate compound of the formula 2 (c) admixing the intermediate compound with (1) a base and (2) a second ester of the formula 3 wherein R4 is an alkyl group, an aryl group, an arylalkyl group, or an alkylaryl group and R5 is an alkyl group, said second ester being present in a molar excess relative to the intermediate compound, said base being present in a molar excess relative to the intermediate compound, and (d) heating the mixture containing the intermediate compound, the second ester, and the base to form a pyridone compound of the formula 4 or a salt thereof. Also disclosed is a process for preparing diazopyridone colorants which comprises preparing a pyridone compound by the above process and reacting the pyridone compound with a diazonium salt to form a diazopyridone compound.

    Abstract translation: 公开了一种制备取代的吡啶酮化合物的方法，其包括（a）在不存在溶剂的情况下混合（1）式R 1 -NH 2的胺，其中R 1是烷基，芳基，芳基烷基或烷基芳基 基团，和（2）下式的第一个酯其中R2是吸电子基团，R3是烷基; （b）加热含有胺和第一酯的混合物以形成式（c）的中间体化合物，其将中间体化合物与（1）碱和（2）下式的第二酯混合，其中R 4是烷基 芳基，芳基烷基或烷基芳基，R 5为烷基，所述第二酯相对于中间体化合物以摩尔过量存在，所述碱相对于中间体化合物以摩尔过量存在，和 （d）加热含有中间体化合物，第二酯和碱的混合物以形成下式的吡啶酮化合物或其盐。 还公开了制备重氮吡啶酮着色剂的方法，其包括通过上述方法制备吡啶酮化合物并使吡啶酮化合物与重氮盐反应以形成重氮吡啶酮化合物。

    Ink compositions containing phthalocyanines
    4.
    发明申请
    Ink compositions containing phthalocyanines 失效
    含有酞菁的油墨组合物

    公开(公告)号：US20030172841A1

    公开(公告)日：2003-09-18

    申请号：US10072210

    申请日：2002-02-08

    Applicant: Xerox Corporation

    Inventor： Donald R. Titterington ,  Michael B. Meinhardt ,  Jeffrey H. Banning ,  James D. Mayo ,  James M. Duff ,  Roger E. Gaynor ,  Harold R. Frame

    IPC: C09D011/12

    CPC classification number: C09D11/34

    Abstract: Disclosed is a phase change ink composition comprising a phase change ink carrier and a colorant compound of the formula 1 wherein M is an atom or group of atoms capable of bonding to the central cavity of a phthalocyanine molecule, wherein axial ligands optionally can be attached to M. Also disclosed are printing processes using the phase change inks.

    Abstract translation: 公开了一种相变油墨组合物，其包含相变油墨载体和下式的着色剂化合物，其中M是能够键合到酞菁分子的中心空穴的原子或原子团，其中轴向配体任选地可以连接到M 还公开了使用相变油墨的印刷方法。

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